Monitoring system for the automatic, continuous measurement and dosing control of chlorine based on the dpd colorimetric method apha 4500 cl-g and on
en iso 7393-2 (116 pages)
AMU-II Pharmacon Safety Instructions Operator’s Manual This document describes the main steps for instrument setup, operation and maintenance. Safety Instructions General The instructions included in this section explain the potential risks associated with instrument operation and provide important safety practices designed to minimize these risks.
AMU-II Pharmacon Safety Instructions 1.1. Warning Notices The symbols used for safety-related notices have the following meaning: DANGER Your life or physical wellbeing are in serious danger if such warn- ings are ignored. Follow the prevention instructions carefully. WARNING Severe injuries or damage to the equipment can occur if such warnings are ignored.
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AMU-II Pharmacon Safety Instructions Warning Signs The warning signs in this manual have the following meaning: Electrical shock hazard Corrosive Harmful to health Flammable Warning general Attention general A-96.150.691 / 041021...
AMU-II Pharmacon Safety Instructions 1.2. General Safety Regulations Legal The user is responsible for proper system operation. All precautions must be followed to ensure safe operation of the instrument. Requirements Spare Use only official Swan spare parts and disposables. If other parts are used during the normal warranty period, the manufacturer’s warranty...
The conductivity is a parameter for the total quantity of ions present in the solution. range The AMU-II Pharmacon transmitter is used together with the two- electrode inline sensors Pharmacon NPT or Pharmacon SAN for applications in purified water (PW) ...
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AMU-II Pharmacon Product Description Alarm relays Two potential-free contacts (one normally open and one normally closed). Summary alarm indication for programmable alarm values and instrument faults. Normally open contact: closed during normal operation, open on error and power loss.
AMU-II Pharmacon Product Description 2.2.2 Swansensor Pharmacon Two-electrode conductivity sensor for the inline measurement of purified water and water for injection. Available in two different models: Swansensor Pharmacon SAN, with sanitary flange Swansensor Pharmacon NPT, with NPT ¾” thread Swansensor Polished surface, no dead volume.
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AMU-II Pharmacon Product Description Dimensions Total length: 153 mm Insertion length: 85 mm dia. 24 mm / (0,95 in) dia. 50.5 mm / (1 1/2“) dia. 16 mm / (0,63 in) A-96.150.691 / 041021...
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AMU-II Pharmacon Product Description Swansensor Polished surface, no dead volume. Equipped with fixed cable (~30cm, PTFE) with M16 male plug. Pharmacon The sensor is accompanied with the following certificates: Cell constant Material specification Inspection certificate according to EN 10204 (surface roughness with SS Pharmacon NPT).
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AMU-II Pharmacon Product Description Dimensions Total length: 102 mm Insertion length: 29 mm SW 28 mm / 1,26 in 9 mm / 0.35 in 3/4 NPT 29 mm / 1.14 in dia. 12.7 mm / 0.5 in A-96.150.691 / 041021...
AMU-II Pharmacon Installation 3.2. Electrical Connections Connection diagram CAUTION Use only the terminals shown in this diagram, and only for the mentioned purpose. Use of any other terminals will cause short circuits with possible corresponding consequences to material and personnel.
Mains cable according to standards IEC 60227 or IEC 60245; flammability rating FV1 Mains equipped with an external switch or circuit-breaker – near the instrument – easily accessible to the operator – marked as interrupter for AMU-II Pharmacon 3.4. Sensor Terminals: see Connection diagram, p.
AMU-II Pharmacon Installation 3.6. Input Note: Use only potential-free (dry) contacts. Terminals 16/8 For programming see Program List and Explanations, p. 3.7. Relay Contacts 3.7.1 Alarm Relay Note: Max. load 100 mA/50 V Alarm output for system errors. For error codes see Error List, p.
AMU-II Pharmacon Installation 3.8. Signal Output 1 and 2 (Current Outputs) Note: Max. burden 510 Ω If signals are sent to two different receivers, use signal isolator (loop isolator). Signal output 1: Terminals 12 (+) and 11 (-) Signal output 2: Terminals 13 (+) and 11 (-) For programming see Program List and Explanations, p.
AMU-II Pharmacon Installation 3.9. Interface Options The functionality of the AMU-II Pharmacon can be expanded with one of the following interface options: RS485 with Modbus or Profibus protocol HART USB 3.9.1 Installation WARNING Electrical shock hazard Before opening the housing, disconnect the AMU-II transmitter from the power supply.
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AMU-II Pharmacon Installation To install an interface option, proceed as follows: 1 Switch power off. 2 Loosen the four screws at the back of the AMU-II transmitter and remove the backplate. 3 Pull the mainboard [B] completely out of the housing.
AMU-II Pharmacon Installation 3.9.2 USB Option C USB stick Pushbutton Blue LED Menu item Calling up the <Operation>/<Eject USB Stick> menu item performs the following actions: the calibration history and the event history are copied to the USB stick, ...
AMU-II Pharmacon Installation 3.9.3 RS485 Option Menu items After the RS485 option has been installed, the <Installation>/ <Interface> menu item becomes visible. Select Modbus RTU or Profibus as protocol. Terminating On the last RS485 interface in the network, move the switch to the position marked “Ron”...
AMU-II Pharmacon Installation 3.10. RS232 Interface The RS232 interface is located on the back of the AMU-II transmitter. Use the USB to RS232 interface converter available from Swan. Downloading To use the functions provided via the RS232 interface, the SwanTerminal program is required, which can be downloaded from SwanTerminal www.swan.ch.
AMU-II Pharmacon Installation 3.11. Install the Swansensor Pharmacon SAN Swansensor Pharmacon SAN Clamp Gasket T-Pipe Pipe To install the Swansensor Pharmacon SAN into a pipe flange pro- ceed as follows: 1 Make sure that the surface of the T-Piece flange [D] is clean.
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AMU-II Pharmacon Installation Recommended Installation The flow direction should be towards the sensor tip. This avoids air or solids becoming trapped in the sensor. Vertical installation is pos- sible if the pipe is always full and no air can be trapped between the electrodes.
AMU-II Pharmacon Installation 3.12. Install the Swansensor Pharmacon NPT Teflon tape Swansensor Pharmacon NPT Flange To install the Swansensor Pharmacon NPT into a pipe flange pro- ceed as follows: 1 Wrap 7 turns of teflon tape around the sensor thread.
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AMU-II Pharmacon Installation Recommended Installation The flow direction should be towards the sensor tip. This avoids air or solids becoming trapped in the sensor. Vertical installation is pos- B C D E sible if the pipe is always full and no air can be trapped between the electrodes.
AMU-II Pharmacon Instrument Setup Instrument Setup 1 Switch on power. 2 Let the instrument run-in for 1 h. 4.1. Programming Menu 5.1.2 (activate if required) parameters Set Operating mode to ON Set the Limit according your requirements. Sensor Program all sensor parameters in Menu 5.1.3 <Installation>/<Sensors>/<Sensor parameters>:...
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AMU-II Pharmacon Instrument Setup Temp. Menu 5.1.4 Compensation Choose between: none Coefficient Neutral salts High-purity water Strong acids Strong bases Ammonia, Ethanolamine Morpholine Quality Menu 5.1.5 (Activate if required). assurance Set the Level according to your requirements, details see Quality As- surance of the Instrument, p.
AMU-II Pharmacon Operation Operation 5.1. Keys to exit a menu or command (rejecting any changes) to move back to the previous menu level to move DOWN in a menu list and to decrease digits to move UP in a menu list and to increase digits...
AMU-II Pharmacon Operation 5.2. Display 15:20:18 0.178 μS 0.092 μS 9.5 l/h 25.4°C A RUN normal operation HOLD input closed or cal delay: Instrument on hold (shows status of signal outputs). input closed: control/limit is interrupted (shows status of signal outputs).
AMU-II Pharmacon Operation 5.3. Software Structure Main Menu Messages Diagnostics Maintenance Operation Installation Menu Messages 1 Messages Reveals pending errors as well as an event history Pending Errors (time and state of events that have occurred at an Message List earlier point of time).
AMU-II Pharmacon Operation 5.4. Changing Parameters and values Changing The following example shows how to set the Q-Flow sensor: parameters 1 Select the parameter you want to Sensors 5.1.1 change. Flow None 2 Press <Enter> Sensor parameters Temp. Compensation Quality Assurance...
AMU-II Pharmacon Maintenance Maintenance 6.1. Maintenance Schedule As required Clean sensor. If a test resistor is available, perform a transmitter test. 6.2. Stop of Operation for Maintenance Shut off power of the instrument. A-96.150.691 / 041021...
AMU-II Pharmacon Maintenance 6.3. Cleaning the Sensor The Swansensor Pharmacon NPT/SAN is largely maintenance free. Depending on the application, however, the sensor may become contaminated, which can lead to problems. If the sensor is contaminated proceed as follows to clean the sensor.
AMU-II Pharmacon Maintenance 6.4. Alarm Function According to USP<645> Display Set the display to show all available conductivity values, i.e: tc: Temperature compensated conductivity uc: Uncompensated conductivity usp: Conductivity Limit at given temperature The setpoint of the USP limit can be modified from 100% to 20% (<Installation>/<Sensors>/<USP parameters>).
Every SWAN on-line instrument is equipped with integrated, autono- mous quality assurance functions to survey the plausibility of each measurement. For AMU-II Pharmacon these are: continuous monitoring of the temperature inside the transmitter case. periodic accuracy test with ultra high precision resistors Further a manual, menu driven inspection procedure can be carried out using a certified reference instrument.
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AMU-II Pharmacon Maintenance Tab. 8-1 Limits and interval for AMU-II Pharmacon max. deviation max. deviation min. inspection Quality Level temperature [°C] result [%] interval 0: Off 0.5 °C 10.0 % 1: Trend annual 0.4 °C 5.0 % 2: Standard quarterly 0.3 °C...
AMU-II Pharmacon Maintenance 6.6.1 Activate SWAN Quality Assurance Procedure Enable quality assurance procedure at each instrument by selecting the quality level in menu 5.1.5, p. 58, Quality Assurance <Installation>/<Sensors>. The corresponding submenus are then activated. Note: The activation is necessary the first time only.
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AMU-II Pharmacon Maintenance Example: The reference instrument, AMI Inspector Pharmacon, is connected up-stream to the in-line sensor Pharmacon at a sampling point (grab sampling via sample). sampling point Reference instrument Sample outlet from reference Sample line instrument Sample inlet to reference...
AMU-II Pharmacon Maintenance 6.6.4 Carry Out Comparison Measurement 1 Navigate to menu <Maintenance>/<Quality Assurance>. 2 Press [Enter]. 3 Follow the dialog on the Display. 4 Carry out pre test preparations Con- Quality Assurance 3.4.5 nect instruments. - carry out preparations...
AMU-II Pharmacon Maintenance 6.6.5 Completion of the Measurement 1 Close the flow regulating valve of the AMI Inspector. 2 Disconnect the AMI Inspector by removing the tubes. 3 Shut down the AMI Inspector. 6.7. Longer Stop of Operation Shut off power of the instrument.
AMU-II Pharmacon Error List Error List Error Non-fatal Error. Indicates an alarm if a programmed value is exceeded. Such Errors are marked E0xx. Fatal Error (blinking symbol) Control of dosing devices is interrupted. The indicated measured values are possibly incorrect.
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AMU-II Pharmacon Error List Error Description Corrective action – check process E001 Cond. Alarm high – check program value 5.3.1.1, p. 63 – check process E002 Cond. Alarm low – check program value 5.3.1.1, p. 63 – check sample temperature E007 Sample Temp.
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AMU-II Pharmacon Error List Error Description Corrective action – See If Fault Yes is programmed in Menu E024 Input active 5.3.4, p. 68 – call service E026 IC LM75 – call service E030 EEprom Frontend – call service E031 Calibration Recout –...
AMU-II Pharmacon Program Overview Program Overview For explanations about each parameter of the menus see Program List and Explanations, p. Menu 1 Messages informs about pending errors and mainte- nance tasks and shows the error history. Password protection possible. No settings can be modified.
AMU-II Pharmacon Program Overview 8.2. Diagnostics (Main Menu 2) Identification Designation * Menu numbers AMU-II Pharmacon 2.1* Version V6.21 – 05/18 Factory Test 2.1.3.1* Instrument 2.1.3* Motherboard Front End Operating Time 2.1.4.1* Years / Days / Hours / Minutes / Seconds 2.1.4*...
AMU-II Pharmacon Program Overview 8.3. Maintenance (Main Menu 3) Transmitter Test 3.1.5* * Menu numbers Mount Test 3.1* (Progress) Simulation 3.2.1* Alarm Relay 3.2* 3.2.2* Relay 1 3.2.3* Relay 2 3.2.4* Signal Output 1 Signal Output 2 3.2.5* Set Time (Date), (Time) 3.3*...
AMU-II Pharmacon Program List and Explanations Program List and Explanations 1 Messages 1.1 Pending Errors 1.1.5 Provides the list of active errors with their status (active, acknowl- edged). If an active error is acknowledged, the alarm relay opens again. Cleared errors are moved to the Message list.
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AMU-II Pharmacon Program List and Explanations 2.2.1.5 QA History: Review QA values (Number, Date, Time, Deviation Conductivity, Deviation Temperature, Status of QA check) of the last quality assurance procedures. 2.2.2 Miscellaneous: 2.2.2.1 Case Temp: Shows the actual temperature [°C] inside the transmit- ter.
AMU-II Pharmacon Program List and Explanations 3 Maintenance 3.1 Transmitter Test 3.1.5 Follow the commands on the screen. Transmitter Test, p. 39 3.2 Simulation To simulate a value or a relay state, select alarm relay, relay 1/2, signal output 1/2...
AMU-II Pharmacon Program List and Explanations 4.2 Relay Contacts 5.3 Relay Contacts, p. 62 4.3 Logger The instrument is equipped with an internal logger. The logger data can be downloaded to a PC using the built-in RS232 interface. The logger can save approx. 1500 data records. Records consist of: Date, time, alarms, measured value, measured value uncompensat- ed, temperature, flow.
AMU-II Pharmacon Program List and Explanations 5.1.3 Sensor parameters: 5.1.3.1 Cell Constant: Enter the cell constant (ZK). It is printed on the label of the used sensor. Range: 0.005000–11.00 cm 5.1.3.2 Temperature Correction: Enter the temperature correction (DT). It is printed on the label of the used sensor.
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AMU-II Pharmacon Program List and Explanations 5.2.1.3-5.2.2.3 Function: Define if the signal output is used to transmit a process val- ue or to drive a control unit. Available functions are: Linear, bilinear or logarithmic for process values. As process values, p. 59 ...
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AMU-II Pharmacon Program List and Explanations 5.2.x.40 Scaling: Enter beginning and end point (Range low & high) of the linear or logarithmic scale. In addition, the midpoint for the bilinear scale. Parameter Conductivity: 5.2.1.40.10 Range low: 0 µS–300 mS 5.2.1.40.20 Range high: 0 µS–300 mS...
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AMU-II Pharmacon Program List and Explanations Ziegler-Nichols method for the optimization of a PID controller: Response to maximum control output = 1.2/a Tangent on the inflection point = 2L Time = L/2 The point of intersection of the tangent with the respective axis will result in the parameters a and L.
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AMU-II Pharmacon Program List and Explanations 5.2.1.43 Control Parameters: if Parameters = Sample flow 5.2.1.43.12 Setpoint Range: 0 –50 l/h 5.2.1.43.22 P-Band: Range: 0 –50 l/h 5.2.1.43 Control Parameters: if Parameters = Cond. uc. 5.2.1.43.13 Setpoint Range: 0 S–300 mS 5.2.1.43.23...
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AMU-II Pharmacon Program List and Explanations Program alarm levels, hysteresis values and delay times for the fol- lowing parameters. Alarm Conductivity Sample Flow Sample Temp. Case Temp. high Case Temp. low 5.3.1.1 Alarm Conductivity 5.3.1.1.1...
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AMU-II Pharmacon Program List and Explanations 5.3.1.3 Sample temperature: Define the measuring value, which should issue an alarm high respectively low. 5.3.1.3.1 Alarm High: If the sample temperature rises above the programmed value E007 is issued. Range: 30–200 °C 5.3.1.3.x Alarm Low: If the sample temperature falls below the programmed value E008 is issued.
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AMU-II Pharmacon Program List and Explanations 5.3.2.1 Function = Limit upper/lower: When the relays are used as upper or lower limit switches, program the following: 5.3.2.20 Parameter: select a process value 5.3.2.300 Setpoint: If the measured value rises above respectively falls below the set-point, the relay is activated.
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AMU-II Pharmacon Program List and Explanations 5.3.2.32 Settings: Choose the respective actuator: Time proportional Frequency Motor valve 5.3.2.32.1 Actuator = Time proportional Examples of metering devices that are driven time proportional are solenoid valves, peristaltic pumps. Dosing is controlled by the operating time.
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AMU-II Pharmacon Program List and Explanations 5.3.2.24 Mode: Operating mode (interval, daily, weekly) 5.3.2.24 Interval 5.3.2.340 Interval: The interval can be programmed within a range of 1–1440 min. 5.3.2.44 Run Time: Enter the time the relay stays closed. Range: 5–6000 sec.
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AMU-II Pharmacon Program List and Explanations 5.3.2.7 Output/Control: see Interval 5.3.2.24 weekly The relay contact can be closed at one or several days, of a week. The daily starting time is valid for all days. 5.3.2.342 Calendar: 5.3.2.342.1 Start time: The programmed start time is valid for each of the pro- grammed days.
AMU-II Pharmacon Program List and Explanations 5.3.4.3 Output/Control: (relay or signal output): Controller continues normally. Cont. Controller continues on the last valid value. Hold Controller is switched off. 5.3.4.4 Fault: No message is issued in pending error list and the alarm relay does not close when input is active.
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AMU-II Pharmacon Program List and Explanations 5.4.4.1 Administrator: The administrator owns all rights and has access to all menus. Only an administrator can assign user rights for the users 1 to 4. Name: Admin predefined, not changeable Function: Administrator predefined, not changeable 5.4.4.1.3...
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AMU-II Pharmacon Program List and Explanations 5.5 Interface Select one of the following communication protocols. Depending on your selection, different parameters must be defined. 5.5.1 Protocol: Profibus 5.5.20 Device address: Range: 0–126 5.5.30 ID No.: Range: Analyzer; Manufacturer; Multivariable 5.5.40...
AMU-II Pharmacon Default Values Default Values Operation: Sensors Filter Time Const.: ................10 s Hold after Cal.:................300 s Alarm Relay .................same as in Installation Signal Output .................same as in Installation Relay 1/2 .................same as in Installation Input .................same as in Installation Logger Logger Interval:................
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AMU-II Pharmacon Default Values Case temp. high:................ 65 °C Case temp. low: ................0 °C Relay 1/2 Function: ................Limit upper Parameter: ...............Conductivity Setpoint:..................30 mS Hysteresis: ................10.0 µS Delay:................... 30 s If Function = Control upw. or dnw: Parameter: ...............Conductivity Settings: Actuator: .............
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Swan Products - Analytical Instruments for: Swan is represented worldwide by subsidiary companies and distributors and cooperates with independent representatives all over the world. For contact in- formation, please scan the QR code. Swan Analytical Instruments ∙ CH-8340 Hinwil www.swan.ch ∙ swan@swan.ch AMU-II Pharmacon...