Contents Parts list Setup diagram Order of connections Setup instructions USB2 cable installation The two first steps for every measurement Integration time Specifications Taking measurements Three tips for SpectraWiz Spectral modes and applications Detailed control bar descriptions System indicators Menu descriptions Model PS-100R with carrying case and reflectance wand...
files, and man- uals Fiber-optic cable, 2 meters USB2 cable Cosine-corrected head Rechargeable 5V output battery Leveling plate 12V output wall mount power supply for recharging battery Reflectance wand 5 V output wall mount power supply for spectroradiometer Apogee carrying-case...
Setup Diagram CAUTION: Do not use Power the force to bend the fiber spectroradiometer with optic cable. It will break. 5 V power supplies only. The 12 V adapter is for recharging the battery only. Attach fiber- optic cable here: For use with reflectance wand Cosine- attach fiber-optic cable here:...
Setup Instructions 1. SpectraWiz Installation Load your CD or USB drive and install the SpectraWiz Software. Different versions of SpectraWiz are available and are stored in separate folders according to your computer’s operating system. Choose the “SETUP” application from the appropriate folder. For Windows XP, select D:\SpectraWiz for Win 2k-NT-XP Ver 4.1, SETUP.
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4. SpectraWiz Setup Run the SpectraWiz software. The dialogue box below, “SpectraWiz Spectro Hardware Setup“, will appear. The correct detector type is “CCD 2048” and the “USB2EPP cable” option should also be checked. These are the only two options you should have selected. Exit Setup. Click on the setup menu and select Unit Calibration Coefficients.
USB2 Cable Installation 1. Disconnect the internet connection to your PC (Do not allow windows to connect to Windows Up- date). 2. Power the spectroradiometer. 3. Connect the USB2 cable to the spectroradiometer and one of the USB ports on your PC. This will prompt the following wizard: 4.
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The First Two Steps For Every Measurement 1. Set Detector Integration Time The detector integration time is like the shutter speed on a camera. It controls the amount of light reaching the detector. An integration time that is too high exposes the detector beyond its range and saturates the readings you will view.
Integration Time About the Integration Time The current integration time is displayed on the status bar at the bottom of the screen (e.g. Time: 100ms). This is the amount of time (in milliseconds) that the spectroradiometer records for a single measurement.
Specifications PS-100 PS-200 Wavelength range 350 to 1000 nm 300 to 850 nm Base unit size 15.5 × 9.5 × 4 cm 15.5 × 11 × 8 cm Base unit mass 500 g 900 g Detector 2048 pixel, 14 x 200µm microelement array Linear range 0-2.1 absorbance units (<0.5%)
Taking Measurements This section will very briefly tell how to make basic measurements. See “Spectral Modes and Applica- tions” on page 15 for more details. Irradiance / Photon Flux ����� ������ �������� ���������� �� ������ ��������� ���� Determine the integration time and save a dark scan as described above. Make sure temperature compensation is on: Setup Temperature Compensation...
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Reflectance / Transmittance �� ����������������� �� ����������������� ������������ ����� ���������� ����� ������ ������ ����� ����� ����� ����� ����� ������ ����� ������ ��� ����� �� ���� ����������� �������� ���� �� ������ ������ ���������� ����� Determine the integration time and save a dark scan. Save a reference scan using the reflectance standard as shown above left.
files for the Spectroradiometer you will not be using to swUV.ini and sw1UV.icf. Apogee suggests making separate folders (e.g. NIR Cal Files and UV Cal Files) inside the SpectraWiz folder to help to keep them separate. Change the names of the files but not the exten- sion.
Spectral Modes And Applications Reflectance, Transmittance, And Absorbance Measurements Reflectance and transmittance are measured as percent of the incident incoming radiation and are both measured using transmission mode: View Transmission. Absorbance is a measure of optical density and is measured using absorbance mode: View Absorbance.
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Overlaying Multiple Spectra To overlay multiple saved spectral traces: Open and navigate to the files folder. hold down the shift key (for contiguous files) or the control key (for noncontiguous files) to select multiple files before clicking “open.” Each spectral trace is graphed in a different color. Excel is capable of importing files created by SpectraWiz.
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Applications The Apps menu allows color monitoring, solution concentration predictions, and irradiance and wavelength calibration. Cielab This CIELAB application performs color measurement using the International Commission on Illumination (CIE) techniques. The application provides a chromaticity diagram for irradiance and a spectrocolorimeter function for reflectance.
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(see page 9). For the best results using a reflectance probe, use a fixture that holds the tip at the same distance from each sample. Apogee carries such a probe with a built in light source.
Detailed Control Bar Descriptions Move Data Cursor / Seek Peek When you click on either button, a vertical line appears on the graph of your spectrum. At the bottom of the screen, the intensity of the spectrum and the wavelength of the vertical line are reported. The line can be moved to the right or the left by clicking on these buttons.
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X Zoom Info / Y Zoom Enable Zooms out to fit the entire wavelength range supported by the spectrometer in use. Holding down the left mouse button and dragging between the wavelengths of interest will zoom in. This function also fits the y-scale to the visible spectral trace.
System Indicators The system indicators are displayed in the status panel at the bottom of your screen. From left to right, the system indicators are as follows: View Mode (SCOPE->) controlled under the ‘View’ menu Wavelength (Wave: 541.1 nm) – controlled by peak right and peak left icons Pixel number (Pix: 553) Y-value at the specified wavelength (Val: 680.053) Integration time (Time: 500 ms) –...
Menu Descriptions The File menu contains the save, Export, open, print setup, print, and exit commands. • Detector Integration Time: may be adjusted manually to allow more precise integration time adjustments than the slide bar. • Number of Scans: SpectraWiz automatically averages a user-defined number of scans for each reading.
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This allows a visual estimate of variance in a sample over time. Graph trace as 1st derivative or 2nd derivative allows the examination of spectral derivatives, which are used in many studies to remove background from spectral applications. techsupport@apogee-inst.com...
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Apogee Instruments, Inc. 708 W 1800 N Ste. 1A Logan, UT 84321 Phone: 435-792-4700 Fax: 435-787-8268 admin@apogee-inst.com...
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