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Linkam Scientific Instruments CCR1000 User Manual

Catalyst cell reactor
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Linkam Scientific Instruments
CCR1000
Catalyst Cell Reactor
USER GUIDE

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Summary of Contents for Linkam Scientific Instruments CCR1000

  • Page 1 Linkam Scientific Instruments CCR1000 Catalyst Cell Reactor USER GUIDE...

  • Page 2: Table Of Contents

    Load Sample Filter ...................... 12 Warning ......................12 Important Note Before Heating Sample ............12 Load Sample into Sample Holder ................. 13 Load Sample Holder into CCR1000 ................14 Appendix .......................... 15 Spares and Accessories ....................15 Contacts Details ........................ 16...

  • Page 3: Before Setting Up Your Equipment

    Before Setting Up Your Equipment Please register your products by going to www.linkam.co.uk and click on the product/software registration button. You will need to register your equipment with us to:  Activate your warranty and technical support  Access the online setup videos ...

  • Page 4: Important Notice

    Use a small quantity of isopropyl alcohol with a soft cloth and gently wipe the surface. Pressure Warning The CCR1000 has been tested to 5bar pressure using 22mm quartz windows of 1mm thickness. Windows must always be inspected with magnifying lens to check there are no microscopic cracks or scratches before using the stage under pressure.

  • Page 5: Safety Precautions

    Safety Precautions Read this guide before using the equipment. Save these instructions for later use. Follow all warnings and instructions which may be placed on the programmer or stage. If for any reason the mains fuse needs to be replaced then it must be replaced by one of the same type and rating as shown in the equipment ratings.

  • Page 6: Introduction

    A high pressure outlet valve can be connected to various gas analysis equipment. All materials used in the CCR1000 stage have been carefully selected to be as un-reactive as possible.

  • Page 7: Mounting Stage To Microscope With Dovetail Substage

    Mounting Stage to Microscope with Dovetail Substage The CCR1000 is designed to work with an up- Curved Clamps Set 9548 right microscope using reflected light only. The following description is for mounting the stage on to microscopes which have a circular dovetail substage assembly.

  • Page 8: Set Up The Ccr1000

    Set Up the CCR1000 Please check that all of the following parts have been supplied with the CCR1000. 1. CCR1000 2. Green Temperature Sensor Cable 3. Power Cable 4. Stage Connection Lead Electrical Cable Connectors Plug in the green Temperature Sensor cable to stage.

  • Page 9: Connection To T95 System Controller

    Connection To T95 System Controller From the stage: connect the green Temperature Sensor cable to the Stage Socket (1) and connect the Stage Connection Lead to Stage Connection Socket (2). Refer to the T95-LinkPad Manual for more de- tails.

  • Page 10: Connect The Ecp Water Circulator Pump

    Use a flow rate of less than 50cc/min. Pressure Warning The CCR1000 has been tested to 5 bar pressure using 22mm quartz windows of 1mm thickness. Windows must always be inspected with magni- fying lens to check there are no microscopic cracks or scratches before using the stage under pressure.

  • Page 11: Load A Sample

    This will allow the tool to grip the outer diameter of the sample holder. Lift the tool vertically away from the CCR1000. If the sample holder is lifted out at an angle it could break.

  • Page 12: Load Sample Filter

    600ºC before doing a sample run. Either heat the fabric in an autoclave or using the CCR1000. Remove the lid window and run gas through the stage during the heating phase. This is so that any dust or debris in the stage or fabric filter is burned off and car- ried away before start of experiment.

  • Page 13: Load Sample Into Sample Holder

    Load Sample into Sample Holder Place the Sample Loading Base (1) on a flat sur- face and hold the Sample Holder (2) above it. Gently press and rotate the Sample Holder into the central hole in the sample loading base until resistance is felt.

  • Page 14: Load Sample Holder Into Ccr1000

    Load Sample Holder into CCR1000 Carefully pick up the top of the Sample Holder and hold it over the heater assembly. Very carefully lower the Sample Holder into the heater assembly. Rotate the sample holder to make sure that it is axially aligned with the heater assembly.

  • Page 15: Appendix

    Here is a list of spares you may require in the future. Contact your Linkam representative for other spare parts that are not listed below. Part No. Part Name Part Description 9848 CCR1000 KIT Replacement Spares Kit CCR-SLK Sample Loading Kit CCR-CC Ceramic Cloth for Sample Loading (6x3.5cm) x4...

  • Page 16: Contacts Details

    Linkam Scientific Instruments Ltd Tel: +44(0)1737 363 476 Fax: +44(0)1737 363 480 Email: support@linkam.co.uk Unit 8 Epsom Downs Metro Centre Waterfield, Tadworth, Surrey, KT20 5LR, UK www.linkam.co.uk Version: 1.05.29.10...

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