Waltron 9065 User Manual

Luminescent dissolved oxygen analyzer
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EXPERTS IN WATER CHEMISTRY SINCE 1903
9065 Luminescent Dissolved Oxygen Analyzer
User Manual
Revision 2.05

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Table of Contents
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Summary of Contents for Waltron 9065

  • Page 1 EXPERTS IN WATER CHEMISTRY SINCE 1903 9065 Luminescent Dissolved Oxygen Analyzer User Manual Revision 2.05...
  • Page 2: Waltron Customer Commitment

    It is Waltron’s commitment to provide the customer with timely and accurate technical service and support. Waltron fully expects the customer to be satisfied with the quality, performance, and cost of this product. If there are any questions or concerns regarding this product, please feel free to contact Waltron at (908)-534-5100.
  • Page 3: Safety

     Follow all regulations and warning labels when disposing of chemicals. Do not mix chemicals. To obtain analyzer safety information or Safety Data Sheets (SDS), please contact Waltron or visit the website at www.waltron.net Waltron User Manual...
  • Page 4: Warranty Agreement

    If, within one year from the date of shipment, the customer experiences any equipment defects or is not satisfied with the analyzer manufacturing, Waltron will repair, or at its option, replace any defective part(s) free of charge. This warranty requires that the defective part(s) be returned to Waltron with shipping charges prepaid.
  • Page 5: Checklist Of Materials

    Checklist of Materials CHECKLIST OF MATERIALS  In order to ensure customer satisfaction, Waltron does its best to provide adequate and timely packaging and shipping services. Please perform the following after receiving a shipment:  Inspect all shipping containers upon receipt and record any visible damage. If there are any outward signs of damage, please retain all containers and packages for inspection by carrier.
  • Page 6: Table Of Contents

    Preparation and Start-Up ....................21 4 User Interface ..................22 Control Buttons ......................22 Display Screen ......................23 Operating Modes ......................23 User Level ........................24 Configuration ......................25 4.5.1 Units ........................25 4.5.2 Info ........................26 4.5.3 Date ........................26 Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 7 Replacing the Coating Holder ................42 9 Deactivating, Storage and Transport ..........44 Deactivating ........................44 Storage ........................44 Transport ........................44 10 Spare Parts ..................45 Appendix A: Formulas ................47 Appendix B: Software Structure ............48 Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 8: List Of Figures

    (2)........................14 Figure 2.5: Optical sensor depiction................ 14 Figure 3.1: Dimensions of the 9065 mounting plate for wall mounting....16 Figure 3.2: Dimensions of the 9065 sensor mounting bracket....... 16 Figure 3.3: Fitting the sensor into the flowcell............17 Figure 3.4: Sensor orientation relative to flow direction.
  • Page 9: List Of Tables

    Table 4.1: Configurable sensor settings..............26 Table 4.2: Configurable settings for the analog outputs......... 28 Table 4.3: Configurable Alarm Settings..............29 Table 4.4: Alarm Output Summary................30 Table 10.1: Spare Parts Listing.................. 45 Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 10: Overview

    Optional 24 V DC, 25 W Installation Sensor One or Two Sensor Configurations Transmitter Standard Wall-mounted Optional Panel-mounted IP class Sensor IP67 Transmitter IP67 Dimensions Sensor Ø 84 x 240, excluding plug Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 11: Intended Use

    The 9065 must be connected to a sample line. The connections to the flowcell are ¼” (6mm) Swagelok fittings. The dissolved oxygen must be measured in a full, flowing sample line. Using the sensor in a pipe that is not full or taking the measurement while the product is not flowing will cause errors or will it cause damage to the device.
  • Page 12: Safety

    During CIP/cleaning, the outside of the instrument may become hot. The sensor will turn itself off automatically when the inside of the sensor reaches a temperature of 65C. Do not touch the outside of the instrument. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 13: Introduction

    Introduction 2 INTRODUCTION ANALYZER OVERVIEW The 9065 has two main sections: 1. Transmitter 2. Sensor Housing Transmitter Display User Interface Transmitter Connections Sensor Housing Flowcell Sample Inlet Sample Outlet Figure 2.1: Analyzer overview. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 14: Sensor

    Coatingholder Temperature Figure 2.2: 25 mm Sensor. COATINGHOLDER The 9065 coatingholder is recognizable by its hexagonal shape. Figure 2.3: 9065 Coatingholder. MEASUREMENT PRINCIPLE The O measurement is based on measuring the luminescence of a layer that is sensitive to oxygen.
  • Page 15: Figure 2.4: Luminescence In The Absence Of Oxygen (1) And In The Presence Of

    The oxygen content is calculated using the time difference between the exposure to the blue light and the molecules lighting up (phase shift) and the product temperature. The sensor in the 9065 is located behind the inlet and before the throttle.
  • Page 16: Installation

    3 INSTALLATION CONTENT OF THE DELIVERY The 9065 is calibrated, checked and tested by Waltron before shipment and the instrument is, therefore, ready for immediate use. It is not necessary to calibrate the instrument again before it is used for the first time.
  • Page 17: Mounting The 9065

    Installation MOUNTING THE 9065 The 9065 can be mounted on a wall or a flat surface using the dimensions shown in the figure below. 8” 7/16” 33.5” 32.2” 5” Figure 3.1: Dimensions of the 9065 mounting plate for wall mounting.
  • Page 18: Assembling The Sensor

    The sensor can be located a cable distance of up to 15 meters from the transmitter. Figure 3.3: Fitting the sensor into the flowcell. Flow Direction Figure 3.4: Sensor orientation relative to flow direction. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 19: Sample Connections

    Sample Inlet Sample Outlet Figure 3.5: Sample Connections. Figure 3.6: Sample Connection Dimensions. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 20: Electrical Connections

    Table 3.2: Connector 1: Power supply range: 90V AC – 230V AC. Pin No. Type Wire color Phase Brown Neutral Blue Yellow/green Table 3.3: Connector 1: Power supply 24V DC. Pin No. Type Wire color + 24V DC Ground Black Yellow/green Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 21: Rs-232 Communication Cable

    Logging sensor 1 Blue 20 mA-output 2 Out-20mA Logging sensor 2 24V input 1 Input 24V Sensor 1 on/off Black 24V input 2 Input 24V Sensor 2 on/off Purple Not connected Grey/pink Shielding ground Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 22: Preparation And Start-Up

    Figure 3.8: An example of the I/O connections. PREPARATION AND START-UP Power can be supplied to the analyzer afternall the cables have been connected. The 9065 will initialize automatically once the power is turned on. Hard materials, such as woodchip and/or grindings, may damage the 9065 measuring head.
  • Page 23: User Interface

    The down arrow also allows the user to select various sub-menus and options. Start Button The start button is used to toggle the sensor measurement mode between online measurement and standby mode. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 24: Display Screen

    The status of the O measurement is displayed on the bottom line. OPERATING MODES The possible operating modes of the 9065 are as follows: INIT Directly after the start up sequence from the control box the INIT-message will appear at the bottom of the screen.
  • Page 25: User Level

    The measurement cell will be calibrated when the Calibration mode is activated. During calibration mode it is not possible to take a measurement. USER LEVEL The default settings can be changed to the preferred user settings before the 9065 is used for the first time. The 9065 has two operator levels: ...
  • Page 26: Configuration

    3. The following sections outline the settings that can be configured by the user. UNITS 4.5.1 The 9065 allows the user to select the display units for the O measurement and temperature values. To change the display units: 1. In the Configuration menu, use the cursor keys to select ‘Units’ and confirm the selection by pressing the Enter button.
  • Page 27: Info

    User Interface INFO 4.5.2 This screen displays the software version and the 9065 serial number. DATE 4.5.3 The arrow buttons can be used to change the date. The day can be changed by pressing the Enter button. By pressing the Enter button again, it is possible to alter the month and the year. Press the Enter button again to return to the Configuration menu.
  • Page 28: Sample Application

    ANALOG OUTPUTS 4.5.9 The 9065 offers two analog outputs that can be configured as desired. After selecting and confirming ‘Config. Output’, the corresponding settings for the unit will be displayed automatically. The settings depend on the unit that has been selected in ‘Units’. The range will be altered accordingly if the unit is changed.
  • Page 29: Alarm Settings

    4. Press the Enter button to return to the Alarm settings menu. 5. Use the cursor keys to select the Return sign and press the Enter button to return to the Configuration menu. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 30: Alarm Outputs

    Extra (Alarm) for Sensor 2 (A4): If the O value of sensor 2 is greater than this value, then output A4 is zero. The same conditions apply here as for the O extra alarm for sensor 1. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 31: Table 4.4: Alarm Output Summary

    Temp < > min./max. > O alarm > O extra Sensor error/fault x The output becomes zero immediately (the relay cuts out due to the alarm function). . The state of the relay remains unchanged. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 32: Operation

    (see Section 5.4). LOCAL AND REMOTE OPERATION Before the 9065 is used for the first time, all of the desired parameter configurations must be set locally at the transmitter. It is then possible to choose remote or local operation. Once remote operation is chosen the transmitter can no longer be controlled locally (loss of start/stop capabilities).
  • Page 33 A maximum of 50 alarms is saved in this menu, including the date and time. The user cannot alter this menu. With a full memory the oldest alarm will be deleted and replaced by the most recent. Reset: The Reset menu can be used to delete all stored measurements. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 34: Calibration

    The zero-point calibration should be carried out using a gas with a certified oxygen content of ≤ 0.001%. The use of nitrogen or carbon dioxide with a purity of 99.9990% (Class 5.0) is reccomended. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 35 Calibration  The inside of the 9065 must be dry during calibration with a gas. Rinse the 9065 for approx. 15 minutes with N , CO or oil-free compressed air. During the calibration process, the % unit or the % a.s. unit must be used. Since the oxygen sensor measures the oxygen partial pressure, the oxygen content measured in the gas during the calibration process depends on the atmospheric pressure.
  • Page 36 13. Press Enter again and calibration is now in progress. A message will display on the screen indicating that the calibration is in progress. 14. After approximiately 1 ½ minutes, the message on the display will change to say Calibration Step Successful; Press any key. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 37: Calibration With Two Gases

    ≤ 0.001%. The use of nitrogen or carbon dioxide with a purity of 99.9990% (Class 5.0) is reccomended.  The high calibration point for the sensor must be calibrated with an accuracy of ± 1% Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 38 4% or 1% O be used for this.  The inside of the 9065 must be dry during calibration with a gas. Rinse the 9065 for approx. 15 minutes with N , CO or oil-free compressed air. During the calibration process, the % unit or the % a.s.
  • Page 39: Check Calibration

    1. Connect the calibration gas to the calibration beaker and enter the current air pressure. 2. The current O value will be shown in “Actual O value”. During a calibration check, never use “Store calibration.” NOTE: Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 40: Calibrating The Analog Outputs

    This is how the output is calibrated. 8. After the outputs have been calibrated, select ‘Store calibration’ to save the settings in the 9065 memory. Select the Return option to return to the previous menu. The calibration data for the previous calibration will be kept if you return to the previous menu without selecting ‘Store...
  • Page 41: Cleaning And Maintenance

    Cleaning and Maintenance 7 CLEANING AND MAINTENANCE INSPECTION Whenever possible, it is recommended to inspect the 9065 for the following and correct if necessary:  Make sure there is no dirt or dust on the instrument.  Check whether the plugs and cables have been inserted correctly.
  • Page 42: Troubleshooting And Repair

    Reset 9065 Broken wire communication Cool down the sensor Cable Thermal shutdown sensor (> 65°C) symbol appears The sensor has taken more The sensor must be recalibrated. in the display than 1,000,000 measurements. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 43: Repair And Maintenance

    Troubleshooting and Repair REPAIR AND MAINTENANCE Before performing any maintenance on the 9065, make sure the instrument is disconnected from the power supply during assembly and disassembly so that there is no risk of an electric shock. REPLACING THE COATING HOLDER 8.3.1...
  • Page 44 6. Screw the coating holder back on to the sensor, return the sensor to the mounting plate, and calibrate the sensor. Never unscrew or loose the temperature sensor. Warning! Unscrewing the temperature sensor will void the warranty. Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 45: Deactivating, Storage And Transport

    The instrument must be stored in a dry location and be protected against mechanical and/or chemical damage. If the 9065 is not going to be used for a long time, the instrument must be thoroughly rinsed with water to clean it. The instrument must then be emptied, flushed with air and dried.
  • Page 46: 10 Spare Parts

    Spare Parts 10 SPARE PARTS If you order spare parts, we kindly request you to include all the information given below.  Serial number of the 9065  Description  Part number Table 10.1: Spare Parts Listing. Description Part No.
  • Page 47 CD-rom with PC software for reading data to PC, Incl RS-232 cable On request Swagelok connector ¼” P1000-106 25 mm Orbisphere adapter K5000-029 LDO Sensor Bracket K5000-008 Set plug 25 mm sensor K5000-030 Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 48: Appendix A: Formulas

    APPENDIX A: FORMULAS Converting the temperature units: Temperature T (° C) = (T (° F)-32)*5/9 Conversion of O units: The 9065 can be set to various oxygen units, where the instrument then makes the following conversions: 20,95   saturation With Tm : Temperature in °...
  • Page 49: Appendix B: Software Structure

    Sensor 1 & 2 Measurement screen ↓ Measurement values Sensor 1 trend graph Sensor 1 Detailed values Sensor 1 Shortcut Measurement values Sensor 2 trend graph Sensor 2 Detailed values Sensor 2 Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 50 Units Info Configuration Sensor settings Main menu Analogue outputs Alarm settings Calibration sensor 1 Calibration Fixed calibration sensor 1 sensor 1 Calibrations Calibration Calibration sensor 2 sensor 2 Fixed calibration sensor 2 Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...
  • Page 51 Operating hours Display O graph s2 Extremes Display temperature graph s2 Logbook Calibrations History 1 Sensor1 History 2 Sensor1 Alarms History 3 Sensor1 History 1 Sensor2 Reset History 2 Sensor2 History3 Sensor2 Waltron User Manual 9065 Luminescent Dissolved Oxygen Analyzer...

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