Waltron 9165 User Manual

Luminescent dissolved oxygen analyzer
Table of Contents

Advertisement

Quick Links

EXPERTS IN WATER CHEMISTRY SINCE 1903
9165 Luminescent Dissolved Oxygen Analyzer
User Manual
Document 101-063-B.1

Advertisement

Table of Contents
loading
Need help?

Need help?

Do you have a question about the 9165 and is the answer not in the manual?

Questions and answers

Subscribe to Our Youtube Channel

Summary of Contents for Waltron 9165

  • Page 1 EXPERTS IN WATER CHEMISTRY SINCE 1903 9165 Luminescent Dissolved Oxygen Analyzer User Manual Document 101-063-B.1...
  • Page 2: Waltron Customer Commitment

    It is Waltron’s commitment to provide the customer with timely and accurate technical service and support. Waltron fully expects the customer to be satisfied with the quality, performance, and cost of this product. If there are any questions or concerns regarding this product, please feel free to contact Waltron at (908)-534-5100.
  • Page 3: Safety

    • Follow all regulations and warning labels when disposing of chemicals. Do not mix chemicals. To obtain analyzer safety information or Safety Data Sheets (SDS), please contact Waltron or visit the website at www.waltron.net Waltron User Manual 101-063-B.1...
  • Page 4: Warranty Agreement

    If, within one year from the date of shipment, the customer experiences any equipment defects or is not satisfied with the analyzer manufacturing, Waltron will repair, or at its option, replace any defective part(s) free of charge. This warranty requires that the defective part(s) be returned to Waltron with shipping charges prepaid.
  • Page 5: Checklist Of Materials

    Checklist of Materials CHECKLIST OF MATERIALS • In order to ensure customer satisfaction, Waltron does its best to provide adequate and timely packaging and shipping services. Please perform the following after receiving a shipment: • Inspect all shipping containers upon receipt and record any visible damage. If there are any outward signs of damage, please retain all containers and packages for inspection by carrier.
  • Page 6: Table Of Contents

    Sensor Spot..........................13 Measurement Principle ...................... 13 3 Installation ..................15 Content of the Delivery ......................15 Pre-Installation .......................... 15 Mounting the 9165 ........................16 Assembling the Sensor ......................17 Sample Connections ........................ 18 Electrical Connections ......................19 3.6.1 Transmitter Connections ..................19 3.6.2...
  • Page 7 Replacing the SENSOR SPOT ................44 9 Deactivating, Storage and Transport ..........46 Deactivating ..........................46 Storage............................46 Transport ........................... 46 10 Spare Parts ..................47 11 Appendix A: GNU General Public License ........49 Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 8: List Of Figures

    ........................14 oxygen (2)..............14 Figure 2.5: Optical sensor depiction......16 Figure 3.1: Dimensions of the 9165 transmitter for wall mounting.......16 Figure 3.2: Dimensions of the 9165 sensor mounting bracket............17 Figure 3.3: Fitting the sensor into the flowcell................18 Figure 3.5: Sample Connections.
  • Page 9: List Of Tables

    Table 3.7: Connector 5: I/O Cable..................20 Table 4.2: Configurable settings for the analog outputs..........35 Table 10.1: Consumable Parts Listing................47 Table 10.2: Spare Parts Listing.................... 48 Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 10: Overview

    Ø 84 x 240, excluding plug Transmitter W178 x H278 x D90 Weight Sensor 2.2 kg Transmitter 1.8 kg -probes per 4 max. Transmitter * The accuracy from the 9165 is determined at 20° C Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 11: Intended Use

    The 9165 must be connected to a sample line. The connections to the flowcell are ¼” Swagelok fittings. The dissolved oxygen must be measured in a full, flowing sample line. Using the sensor in a pipe that is not full or taking the measurement while the product is not flowing will cause errors.
  • Page 12: Precautionary Measures And Safety Instructions

    During CIP/cleaning, the outside of the instrument may become hot. The sensor will turn itself off automatically when the inside of the sensor reaches a temperature of 65C. Do not touch the outside of the instrument. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 13: Introduction

    Introduction 2 INTRODUCTION ANALYZER OVERVIEW The 9165 has two main sections: 1. Transmitter 2. Sensor Housing Transmitter Display User Interface Transmitter Connections Sensor Housing Flowcell Sample Inlet Sample Outlet Figure 2.1: Analyzer overview. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 14: Sensor

    Temperature Well Figure 2.2: Sensor Head. SENSOR SPOT The 9165 Sensor Spot is recognizable by its hexagonal shape. Figure 2.3: 9165 Sensor Spot. MEASUREMENT PRINCIPLE The O measurement is based on measuring the luminescence of a layer that is sensitive to oxygen.
  • Page 15: Figure 2.4: Luminescence In The Absence Of Oxygen (1) And In The Presence Of

    The oxygen content is calculated using the time difference between the exposure to the blue light and the molecules lighting up (phase shift) and the product temperature. Figure 2.5: Optical sensor depiction. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 16: Installation

    3 INSTALLATION CONTENT OF THE DELIVERY The 9165 is calibrated, checked and tested by Waltron before shipment and the instrument is, therefore, ready for immediate use. It is not necessary to calibrate the instrument again before it is used for the first time.
  • Page 17: Mounting The 9165

    Installation MOUNTING THE 9165 The 9165 can be mounted on a wall or a flat surface using the dimensions shown in the figure below. Figure 3.1: Dimensions of the 9165 transmitter for wall mounting. Figure 3.2: Dimensions of the 9165 sensor mounting bracket.
  • Page 18: Assembling The Sensor

    The sensor housing and transmitter are fully assembled to the mounting plate. The figure below shows how the sensor properly fits into the flowcell. Figure 3.3: Fitting the sensor into the flowcell. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 19: Sample Connections

    Sample Outlet Sample Inlet Figure 3.5: Sample Connections. Figure 3.6: Sample Connection Dimensions. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 20: Electrical Connections

    Power Cable Panel Mount USB USB Drive POWER CABLE 3.6.2 Table 3.2: Connector 1: Power supply range: 90V AC – 230V AC. Pin No. Type Wire color Black Neutral White Brown/Blue Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 21: I/O Cable

    Passive or 24V DC White/Green Relay 3+ Passive or 24V DC Brown/Green Relay 3- Passive or 24V DC White/Yellow Relay 4+ Passive or 24V DC Yellow/Brown Relay 4- Passive or 24V DC White/Gray SPARE Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 22: Non-Powered Relay Configuration

    Connector J6 of the main electronics board should be wired as shown in Figures 3.8 and 3.9. Note that this is the default configuration. Figure 3.8: J6 Connector on Main Board for Relay Configuration. Figure 3.9: Non-Powered relay configuration of J6. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 23: Powered Relay Configuration

    When the relay toggles, it sends 24v to the relay/alarm outside of the analyzer and returns to ground. Figure 3.10: Powered Relay Configuration of J6; Relay #1 only. Figure 3.10: Powered Relay Configuration of J6; All Relays. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 24: Preparation And Start-Up

    Installation PREPARATION AND START-UP Power can be supplied to the analyzer after all the cables have been connected. The 9165 will initialize automatically once the power is turned on. Hard materials, such as woodchip and/or grindings, may damage the 9165 measuring head.
  • Page 25: User Interface

    4 USER INTERFACE CONTROL BUTTONS The transmitter faceplate contains a full touchscreen which allows the user to navigate through the interface and communicate with the analyzer. Figure 4.1: Transmitter with display screen. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 26: Display Screen

    3 seconds. The status of the O measurement is displayed on the bottom left of the individual sensor area. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 27: Shortcut Menu

    While all screens will display, they may not be interactive without first logging in. Figure 4.3: Menu Screen. OPERATING MODES The possible sesnsor operating modes of the 9165 are as follows: MEASURING Depending on the number of sensors that have been connected and properly addressed, the respective number of sensor screens will display.
  • Page 28: User Levels

    The software will automatically switch back to the Operator level after 10 minutes. This cannot be altered. SETTINGS The 9165 is highly configurable with multipe user option. All screens for these settings are availsble through the menu. Waltron User Manual 101-063-B.1...
  • Page 29: Sensor Setup Screen

    The bottom of the screen will appear with the addresses of the sensors detected and allow for easy switching between sensors in this screen. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 30: Calibration Screen

    Due to minimal drifting associated with optical technology, regular calibration other than 0% is not required. User must be logged in to make changes.For detailed instructions on sensor calibrations please see (Section 4.5.7). Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 31: Alarm Setup Screen

    Alarm will reactivate upon re-entering conditions for established alarm. The bottom of the screen will appear with the addresses of the sensors detected and allow for easy switching between sensors in this screen. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 32: Analog Outputs Screen

    4 mA • 50%: 12 mA • 100%: 20 mA The bottom of the screen will appear with the available output channels and allows for easy switching between outputs in this screen. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 33: Relay Outputs Screen

    The bottom of the screen will appear with the available relay channels and allows for easy switching between outputs in this screen. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 34: Address Setup Screen

    Note: Should a sensor not have an established address, the field will remain blank. Tapping an address will write to the new sensor, but will require that the transmitter conduct a soft restart. This will happen automatically. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 35: Device Setup Screen

    Tapping this button will cause “Writing to USB” to appear breifly. After writing is complete it will revert to “Export Data” Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 36: Analog Outputs

    ANALOG OUTPUTS 4.5.8 The 9165 offers four analog outputs that can be configured as desired from the analog outputs screen. The O2 and temperature settings depend on the unit that has been selected on the sensor settings screen. The range is not changed automatically if the unit is changed.
  • Page 37: Relay Outputs

    RELAY OUTPUTS 4.5.10 The 9165 comes with four available relay output that can be independantly configured to any or all of the sensor alarms. Relay options: • Normaly Open or Normally Closed •...
  • Page 38: Operation

    Operation 5 OPERATION GENERAL INFORMATION Prior to using the 9165 for online measurement, be sure that all installation and start-up procedures have been properly followed. MEASUREMENT The 9165 will start measurements once the sensors are connected, properly addressed and the sensors are put into online mode.
  • Page 39: Exporting Data

    Operation EXPORTING DATA Measurement data is stored internal by the 9165 for a period of one month. After which, old data is trimmed. NOTE: This is an automatic function that references the Real Time Clock (RTC) of the processor. Changing the date/time settings of the RTC can cause the processor to trim / retain data.
  • Page 40: Calibration

    24 hours a day, seven days a week. If a shorter sample time is used, the sensor will reach 1 million light exposures sooner and will, therefore, require calibration sooner. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 41: One Point Gas Calibration

    ≤ 0.001%. The use of nitrogen or carbon dioxide with a purity of 99.9990% (Class 5.0) is reccomended. • The inside of the 9165 must be dry during calibration with a gas. Rinse the 9165 for approx. 15 minutes with N , CO or oil-free compressed air.
  • Page 42 14. Reconnect sample lines and restore sample flow to the sensor. 15. Ensure that the sensor is placed back into online measurement mode. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 43: Calibration With Two Gases

    1% or 2% O can be used for this. • The inside of the 9165 must be dry during calibration with a gas. Rinse the 9165 for approx. 15 minutes with N , CO or oil-free compressed air. During the calibration process, the % is used.
  • Page 44: Cleaning And Maintenance

    Cleaning and Maintenance 7 CLEANING AND MAINTENANCE INSPECTION Whenever possible, it is recommended to inspect the 9165 for the following and correct if necessary: • Make sure there is no dirt or dust on the instrument. • Check whether the plugs and cables have been inserted correctly.
  • Page 45: Troubleshooting And Repair

    REPAIR AND MAINTENANCE Before performing any maintenance on the 9165, make sure the instrument is disconnected from the power supply during assembly and disassembly so that there is no risk of an electric shock.
  • Page 46 Screw the coating holder back on to the sensor, return the sensor to the mounting plate, and calibrate the sensor. Apply Loctite 572 Never unscrew or loose the temperature sensor. Warning! Unscrewing the temperature sensor will void the warranty. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 47: Deactivating, Storage And Transport

    The instrument must be stored in a dry location and be protected against mechanical and/or chemical damage. If the 9165 is not going to be used for a long time, the instrument must be thoroughly rinsed with water to clean it. The instrument must then be emptied, flushed with air and dried.
  • Page 48: 10 Spare Parts

    O-ring 20x2.5 (Sensor Head) K5000-011 LDO Zero Point Calibration Kit K6000-101 Zero Water (4-pack with rubber beaker) K6000-121 Zero Point Calibration Gas, 105L K6000-110 High Point (1%) Calibration Gas, 105L K6000-111 Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 49: Table 10.2: Spare Parts Listing

    K5000-042 Flowcell with Sample Fittings K5000-103 LDO Sensor Bracket K5000-008A Regulator, Fixed Flow, Calibration Gas 105L Cylinder K6000-115 Connection Hose, LDO Calibration Kit K6000-117 Tube Connection Fitting, LDO Calibration Kit K6000-118 Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 50: 11 Appendix A: Gnu General Public License

    GPL to prohibit the practice for those products. If such problems arise substantially in other domains, we stand ready to extend this provision to those domains in future versions of the GPL, as needed to protect the freedom of users. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 51 The “System Libraries” of an executable work include anything, other than the work as a whole, that (a) is included in the normal form of packaging a Major Component, but which is not part of that Major Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 52 Conveying Verbatim Copies. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 53 License, on a durable physical medium customarily used for software interchange, for a price no more than your reasonable cost of physically performing this conveying of source, or (2) access to copy the Corresponding Source from a network server at no charge. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 54 (and with an implementation available to the public in source code form), and must require no special password or key for unpacking, reading or copying. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 55 You may not propagate or modify a covered work except as expressly provided under this License. Any attempt otherwise to propagate or modify it is void, and will automatically terminate your rights under this License (including any patent licenses granted under the third paragraph of section 11). Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 56 License, of making, using, or selling its contributor version, but do not include claims that would be infringed only as a consequence of further modification of the contributor version. For purposes of this Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 57 Program, the only way you could satisfy both those terms and this License would be to refrain entirely from conveying the Program. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 58 OF DATA OR DATA BEING RENDERED INACCURATE OR LOSSES SUSTAINED BY YOU OR THIRD PARTIES OR A FAILURE OF THE PROGRAM TO OPERATE WITH ANY OTHER PROGRAMS), EVEN IF SUCH HOLDER OR OTHER PARTY HAS BEEN ADVISED OF THE POSSIBILITY OF SUCH DAMAGES. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...
  • Page 59 Program, unless a warranty or assumption of liability accompanies a copy of the Program in return for a fee. Waltron User Manual 101-063-B.1 9165 Luminescent Dissolved Oxygen Analyzer...

Table of Contents