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Summary of Contents for Metrohm 736 GP Titrino
- Page 1 CH-9101 Herisau/Switzerland Phone ++41 71 53 85 85 ++41 71 53 89 01 736 GP Titrino Short instructions for use 8.736.1023 95.12 Ti/pr 736 GP Titrino, Short instructions for use...
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Page 2: Table Of Contents
2.9 Mode TIP, parameters ............22 2.10 Calculations ..............23 3. Other functions ..............25 3.1 Method memory..............25 3.2 Sample data, keys <smpl data> and <silo> ...... 27 3.3 Configuration, key <configuration> ........28 Index ..................29 736 GP Titrino, Short instructions for use... -
Page 3: Getting Started
Other inquiries of the "auxiliaries" group are not of interest at date 1997-12-16 the moment. Exit the inquiries with <QUIT>. Press <QUIT> once again to exit the inquiries of the <configuration> key. 2 x <QUIT> 736 GP Titrino: Getting started... - Page 4 Signs in the Titrino dialog: > Title of inquiry groups, e.g. ">auxiliaries" Values can be chosen by the key <select>, e.g. "dialog:" Signs that are used in the instructions for use <> sign for "key", e.g. <select> 736 GP Titrino: Getting started...
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Page 5: Development Of A Method
Now stop it with <STOP>. The second line shows the equivalence point found, e.g.: 2.083 ml pH 7.64 If more than one equivalence point has been found, the sec- ond equivalence point can be viewed with <enter> 736 GP Titrino: Getting started... - Page 6 Entry of the calculation constants <C-fmla> Press <C-fmla>. The constants which have been used in the formula are requested: 0.1 <enter> C01: Concentration of your titrant = 0.1 mol/L. C02: Molar mass of HCI = 36.47 g/mol 36.47 <enter> 736 GP Titrino: Getting started...
- Page 7 Use a ";" as delimiter between the report blocks. If you <select> wish to print out a curve and a full result report, enter "curve;full". report:curve;full Confirm the entry with <enter> and quit the inquiries <enter> with <QUIT> <QUIT> 736 GP Titrino: Getting started...
- Page 8 If several stop criteria have been set, the one that is reached stop pH first, applies. 11.5 <enter> Confirm the input with <enter> and quit the inquiry with 2 x <QUIT> <QUIT>. Try another titration with this method. 736 GP Titrino: Getting started...
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Page 9: Storing Methods
Blank D0 Chloride D0 Diazo D0 Ipol Br-Index D0 Ca-Mg D0 EDTA-NTA D0 Metals D0 Perox.No D0 HCl D0 remaining bytes 7330 ------------ dosing unit, that is being used method mode and name measured quantity 736 GP Titrino: Getting started... - Page 10 Confirm this function with the key <enter> and give a name for the backup directory. directory: If you wish to overwrite an existing directory, choose a name with <select>. name + <enter> The backup will be effected. 736 GP Titrino: Getting started...
- Page 11 "user Acid Tit.NaOH Tit.HCl meth." W-Liquor bytes: 620 directory: KF Titr. TarTiter H2OTiter Blank_KF the directory "KF Titr." KF-Blank contains 5 methods bytes: 808 remaining bytes on card: 121892 ------------ 736 GP Titrino: Getting started...
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Page 12: Working With Several Dosing Units
D1 is be- ing used. DET pH Start the method. <START> After the titration "D1a" appears in the display. "a" means DET pH "active", the dosing unit D1 is now active. 736 GP Titrino: Getting started... - Page 13 (e.g. for cleaning). Choose the function <START> "empty" with the key <select> and start with <START>. Attention: With the function "empty", liquid will be expelled! <QUIT> Quit the selection of dosing units with <QUIT>. 736 GP Titrino: Getting started...
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Page 14: Titration, Dosing And Measuring Modes
• sluggish electrode response. Note: The reagent feeding algo- Applications rithm is based on measured data. The curve should therefore not deviate markedly from S-shape. 736 GP Titrino: Titration, dosing and measuring modes... - Page 15 • activity determinations, e.g. does not change during a of enzymes. determination series. • kinetic investigations (first • If an excess of titrant must order kinetics). be avoided. • KFT: Determinations of water contents. 736 GP Titrino: Titration, dosing and measuring modes...
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Page 16: Mode Det And Met, Parameters
0.00...±20.00, OFF resp. Up to 9 fix EP's. U: 0...±2000 mV, OFF Evaluation of pK or half neutralization pK/HNP: ON, OFF potential (HNP). Preselections for the sequence see DOS, >preselections page 19 736 GP Titrino: Titration, dosing and measuring modes... -
Page 17: Mode Set, Parameters
Request of identifications after start. req.ident: id1, id1 & 2, all, OFF Request of sample size after start. req.smpl size: value, unit, all, OFF Pulse output on I/O line L6. activate pulse: first, all, cond., OFF 736 GP Titrino: Titration, dosing and measuring modes... -
Page 18: Mode Kft, Parameters
Request of identifications after start. req.ident: id1, id1 & 2, all, OFF Request of sample size after start. req.smpl size: value, unit, all, OFF Pulse output on I/O line L6. activate pulse: first, all, cond., OFF 736 GP Titrino: Titration, dosing and measuring modes... -
Page 19: Mode Stat, Parameters
C5X). Up to 9 fix V's. 0...999 999 s, OFF Interpolation of times at fixed volume fix time 1 0.01...1, OFF rations of the end volume (→ C6X). Up to 9 fix times. 736 GP Titrino: Titration, dosing and measuring modes... - Page 20 & 2, all, OFF Request of sample size after start. req.smpl size: Value, unit, all, OFF Display of rate. display rate: ON, OFF Pulse output on I/O line L6. activate pulse: ON, OFF 736 GP Titrino: Titration, dosing and measuring modes...
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Page 21: Mode Dos, Parameters
Request of identifications after start. req.ident: id1, id1 & 2, all, OFF Request of sample size after start. req.smpl size: value, unit, all, OFF Pulse output on I/O line L6. activate pulse: ON, OFF 736 GP Titrino: Titration, dosing and measuring modes... -
Page 22: Mode Doc, Parameters
& 2, all, OFF Request of sample size after start. req.smpl size: value, unit, all, OFF Display of rate. display rate: ON, OFF Pulse output on I/O line L6. activate pulse: ON, OFF 736 GP Titrino: Titration, dosing and measuring modes... -
Page 23: Mode Meas And Cal, Parameters
8 ASCII characters sample changer cal: Calibration with Sample Changer. ON, OFF activate pulse: Pulse output on I/O line L6. all, first, OFF Statistics calculation see at DET, page 14. >statistics 736 GP Titrino: Titration, dosing and measuring modes... -
Page 24: Mode Tip, Parameters
Selection of the measured quantity for meas.mode: pH, U, I(pol), U(pol), T, OFF <meas/hold>. Measuring input for pH and U. meas.input: 1, 2, diff. Temperature for the compensation of the temperature -170.0...500.0 °C pH values. 736 GP Titrino: Titration, dosing and measuring modes... -
Page 25: Calculations
Allocations for statistics. >mean Enter mean number and result RSX, EPX, MN?= RSX, EPX, CXX or CXX. Allocations of temporary variables for >temporary variables calculations under TIP. C7?= RSX, EPX, CXX 736 GP Titrino: Titration, dosing and measuring modes... - Page 26 C23 Sample size -999 999...1...999 999 smpl size Unit of sample size g, mg, ml, ul, pc, no unit or up to smpl unit: 5 ASCII characters 736 GP Titrino: Titration, dosing and measuring modes...
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Page 27: Other Functions
- - Memory Card store store store store Single method Single method recall recall recall recall Working memory: Working memory: method data of last analysis sample data 736 GP Titrino: Other functions... - Page 28 10 characters Card formatting. >format Card labeling. card label up to 8 characters Confirm formatting. format: ON, OFF Date for changing the card battery. >change battery date YYYY-MM-DD 736 GP Titrino: Other functions...
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Page 29: Sample Data, Keys
Determination results will be stored as save lines: ON, OFF C24 or C25 in the silo memory according to the allocations in the methods, see page 23. 736 GP Titrino: Other functions...And -
Page 30: Configuration, Key
0.1...2.0...9.9 mm Length of the aspiration tube. len.asp.tub. 1.0...25.0...999.9 cm Diameter of the aspiration tube. diam.asp.tub. 0.1... 2.0...9.9 mm Dosing rate. dos.rate DX 0.01...150 ml/min, max. Filling rate. fill rate DX 0.01...150 ml/min, max. 736 GP Titrino: Other functions... -
Page 31: Index
Weight..........5 - Development ......3 - Recalling........8 - Storing ........7 Modes .......... 12ff - Selection........3 - Survey ........12 Operands ........4, 24 Parameters ........14ff pH Stat ..........17 Printing..........5 736 GP Titrino: Index...
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