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TripleTOF 5600 Plus
SCIEX TripleTOF 5600 Plus Spectrometer Manuals
Manuals and User Guides for SCIEX TripleTOF 5600 Plus Spectrometer. We have
1
SCIEX TripleTOF 5600 Plus Spectrometer manual available for free PDF download: System User's Manual
SCIEX TripleTOF 5600 Plus System User's Manual (131 pages)
Brand:
SCIEX
| Category:
Laboratory Equipment
| Size: 1 MB
Table of Contents
Table of Contents
3
1 Operational Precautions and Limitations
7
General Safety Information
7
Regulatory Compliance
7
Australia and New Zealand
7
Canada
8
Europe
8
United States
8
International
9
Electrical Precautions
9
AC Mains Supply
9
Protective Earth Conductor
10
Chemical Precautions
10
Ventilation Precautions
11
Environmental Precautions
12
Electromagnetic Environment
13
Decommissioning and Disposal
14
Qualified Personnel
14
Laboratory Conditions
14
Operating Conditions
14
Performance Specifications
15
Equipment Use and Modification
15
Contact Us
16
Technical Support
16
Documentation Symbols and Conventions
16
Related Documentation
17
2 Principles of Operation
18
System Overview
18
Hardware Overview
18
Panel Symbols
21
Theory of Operation
22
Data Handling
23
3 Operating Instructions Hardware
24
Start up the System
24
Shut down the System
25
Adjust the Integrated Syringe Pump Position
26
Reset the Syringe Pump
29
4 Operating Instructions Sample Workflows
31
5 Operating Instructions Hardware Profiles and Projects
34
Hardware Profiles
34
Create a Hardware Profile
34
Add Devices to a Hardware Profile
39
Troubleshoot Hardware Profile Activation
41
Projects and Subprojects
42
Create Projects and Subprojects
42
Create Subprojects
44
Copy Subprojects
44
Switch between Projects and Subprojects
44
Installed Project Folders
45
Back up the API Instrument Folder
46
Recover the API Instrument Folder
46
6 Tune and Calibrate
47
Optimize the Mass Spectrometer
47
About the Verifying or Adjusting Performance Dialog
48
Results Summary
48
7 Operating Instructions Acquisition Methods
50
Create an Acquisition Method Using the Acquisition Method Editor
50
Add an Experiment
51
Add a Period
51
Copy an Experiment into a Period
52
Copy an Experiment Within a Period
52
Create an Acquisition Method Using the Method Wizard
52
Scan Techniques
53
Single Mass Spectrometry
53
Quadrupole-Based Single Mass Spectrometry
53
Time-Of-Flight Single Mass Spectrometry
54
Tandem Mass Spectrometry
54
Product Ion Mass Spectrometry
54
Precursor Ion Mass Spectrometry
54
About Spectral Data Acquisition
54
Parameters
55
8 Operating Instructions Batches
60
Set Queue Options
60
Add Sets and Samples to a Batch
62
Submit a Sample or Set of Samples
65
Set up Sample Calibration
65
Change Sample Order
66
Acquire Data
66
Set Sample Locations in the Batch Editor
67
Select Vial Positions Using the Locations Tab (Optional)
67
Stop Sample Acquisition
68
Batch Editor Right-Click Menu
69
Queue States and Device Status
70
Queue States
70
View Instrument and Device Status Icons
71
Queue Right-Click Menu
72
9 Operating Instructions Analyze and Explore Data
74
Open Data Files
74
Navigate between Samples in a Data File
75
View Experimental Conditions
75
Show Data in Tables
76
Show ADC Data
78
Show Basic Quantitative Data
79
Chromatograms
79
Show Tics from a Spectrum
80
Show a Spectrum from a TIC
81
About Generating Xics
82
Generate an XIC Using a Selected Range
82
Generate an XIC Using the Maximum Peak
83
Generate an XIC Using Base Peak Masses
83
Extract Ion by Selecting Masses
83
Generate Bpcs
84
Generate Xwcs
86
DAD Data
86
Generate Twcs
87
Adjust the Threshold
87
Chromatogram Panes
88
Spectra Panes
89
Graphical Data Processing
89
Graphs
90
Manage Data
90
Zoom in on the Y-Axis
92
Zoom in on the X-Axis
92
10 Service and Maintenance Information
93
Recommended Maintenance Schedule
93
Clean the Surfaces
95
Clean the Front-End
95
Symptoms of Contamination
96
Required Materials
96
Cleaning Best Practices
97
Prepare the Mass Spectrometer
98
Clean the Curtain Plate
99
Clean the Front of the Orifice Plate
101
Put the Mass Spectrometer Back in Service
101
Empty the Source Exhaust Drain Bottle
101
Inspect the Roughing Pump Oil Level
103
Replace the Mass Spectrometer Cooling Fans Filter
104
Storage and Handling
106
11 Mass Spectrometer Troubleshooting
107
A Recommended Calibration Ions
110
B Exact Masses and Chemical Formulas
113
C Toolbar Icons
116
D Glossary of Symbols
125
E Glossary of Warnings
130
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