SCIEX 5500 Series Mass Spectrometer Manuals

Manuals and User Guides for SCIEX 5500 Series Mass Spectrometer. We have 1 SCIEX 5500 Series Mass Spectrometer manual available for free PDF download: System User's Manual

SCIEX 5500 Series System User's Manual (195 pages)

Brand: SCIEX | Category: Laboratory Equipment | Size: 3 MB

Table of Contents
3
Chapter 1 Operational Precautions and Limitations

8
- General Safety Information
  8
- Regulatory Compliance
  8
  - Australia and New Zealand
    8
  - Canada
    9
  - Europe
    9
  - United States
    9
  - International
    10
- Electrical Precautions
  10
  - AC Mains Supply
    10
  - Protective Earth Conductor
    11
- Chemical Precautions
  11
  - System Safe Fluids
    12
- Ventilation Precautions
  13
- Environmental Precautions
  14
  - Electromagnetic Environment
    14
  - Decommissioning and Disposal
    15
- Qualified Personnel
  16
- Laboratory Conditions
  16
  - Operating Conditions
    16
  - Performance Specifications
    16
- Equipment Use and Modification
  17
- Contact Us
  17
- Technical Support
  18
- Documentation Symbols and Conventions
  18
- Related Documentation
  19
Chapter 2 Principles of Operation

20
- System Overview
  20
Chapter 3 Operating Instructions Sample Workflows

36
Chapter 4 Operating Instructions Hardware

45
Chapter 5 Operating Instructions Hardware Profiles and Projects

55
- Hardware Profiles
  55
- Projects and Subprojects
  62
Chapter 6 Tune and Calibrate

66
Chapter 7 Automatic Optimization

69
Chapter 8 Operating Instructions Acquisition Methods

84
Chapter 9 Operating Instructions Analyze and Process Quantitative Data

90
- Quantitative Analysis
  90
- Peak Review and Manual Integration of Peaks
  98
  - Review Peaks
    98
  - Manually Integrate Peaks
    103
  - Peak Review Right-Click Menu
    104
- Calibration Curves
  105
  - View Calibration Curves
    105
  - Overlay Calibration Curves
    107
  - Calibration Curve Right-Click Menu
    107
- Sample Statistics
  108
  - View the Statistics for Standards and Qcs
    108
- Compare Results between Batches
  109
Chapter 10 Operating Instructions Analyze and Explore Data

110
- Open Data Files
  110
- Navigate between Samples in a Data File
  110
- View Experimental Conditions
  111
- Show Data in Tables
  112
- Show ADC Data
  114
- Show Basic Quantitative Data
  115
- Chromatograms
  116
- Show Tics from a Spectrum
  117
- Show a Spectrum from a TIC
  117
- About Generating Xics
  118
- Generate Bpcs
  121
- Generate Xwcs
  123
- Generate DAD Data
  123
- Generate Twcs
  124
- Adjust the Threshold
  124
- Chromatogram Panes
  125
- Spectra Panes
  126
- Graphical Data Processing
  126
- Graphs
  127
  - Manage Data
    127
  - Zoom in on the Y-Axis
    129
  - Zoom in on the X-Axis
    129
Chapter 11 Reporter Software

130
- Analyst Reporter User Interface
  131
- Generate Reports
  133
Chapter 12 Operating Instructions Batches

135
- Set Queue Options
  135
- Create and Submit a Batch
  136
  - Add Sets and Samples to a Batch
    136
  - Equilibrate the System
    139
  - Submit a Sample or Set of Samples
    140
- Change Sample Order
  140
- Acquire Data
  140
- Set Sample Locations in the Batch Editor
  141
- Select Vial Positions Using the Locations Tab (Optional)
  142
- Set Quantitation Details in the Batch Editor (Optional)
  143
- Stop Sample Acquisition
  143
- Import Batch Files
  144
  - Build a Batch as a Text File
    144
  - Import a Batch from a Text File
    144
- Batch Editor Right-Click Menu
  145
- Queue States and Device Status
  146
  - Queue States
    146
  - View Instrument and Device Status Icons
    147
  - Queue Right-Click Menu
    148
Chapter 13 Service and Maintenance Information

150
- Recommended Maintenance Schedule
  150
- Clean the Surfaces
  152
- Clean the Front-End
  152
  - Symptoms of Contamination
    153
  - Required Materials
    153
  - Cleaning Best Practices
    154
  - Prepare the Mass Spectrometer
    155
  - Clean the Curtain Plate
    156
  - Clean the Front of the Orifice Plate
    157
  - Put the Mass Spectrometer Back in Service
    157
- Inspect the Roughing Pump Oil Level
  158
- Empty the Source Exhaust Drain Bottle
  158
- Storage and Handling
  160
Chapter 14 Mass Spectrometer Troubleshooting

161
Appendix A Operating Instructions Manual Compound Optimization

164
- About Manual Compound Optimization
  164
- About Scan Types
  165
- Manually Optimize an Analyte
  165
- Manually Optimize the Ion Source and Gas Parameters
  171
  - Prepare the Ion Source
    171
  - Optimize the Ion Source Parameters
    171
- Advanced Parameters
  172
  - Optimize AF2
    172
  - About Collision Energy Spread (CES)
    173
Appendix B 5500 Series System Parameters

174
Appendix C Calibration Ions and Solutions

177
Appendix D Toolbar Icons

180
Appendix E Glossary of Symbols

189
Appendix F Glossary of Warnings

194

SCIEX Categories

Laboratory Equipment Portable Generator Medical Equipment Control Unit Analytical Instruments

More SCIEX Manuals

SCIEX 5500 Series Mass Spectrometer Manuals

SCIEX 5500 Series System User's Manual (195 pages)

Table of Contents

Chapter 1 Operational Precautions and Limitations

Chapter 2 Principles of Operation

Chapter 3 Operating Instructions Sample Workflows

Chapter 4 Operating Instructions Hardware

Chapter 5 Operating Instructions Hardware Profiles and Projects

Chapter 6 Tune and Calibrate

Chapter 7 Automatic Optimization

Chapter 8 Operating Instructions Acquisition Methods

Chapter 9 Operating Instructions Analyze and Process Quantitative Data

Chapter 10 Operating Instructions Analyze and Explore Data

Chapter 11 Reporter Software

Chapter 12 Operating Instructions Batches

Chapter 13 Service and Maintenance Information

Chapter 14 Mass Spectrometer Troubleshooting

Appendix A Operating Instructions Manual Compound Optimization

Appendix B 5500 Series System Parameters

Appendix C Calibration Ions and Solutions

Appendix D Toolbar Icons

Appendix E Glossary of Symbols

Appendix F Glossary of Warnings

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