SCIEX 3200 QTRAP Mass Spectrometer Manuals

Manuals and User Guides for SCIEX 3200 QTRAP Mass Spectrometer. We have 1 SCIEX 3200 QTRAP Mass Spectrometer manual available for free PDF download: System User's Manual

SCIEX 3200 QTRAP System User's Manual (114 pages)

Brand: SCIEX | Category: Laboratory Equipment | Size: 1 MB

Table of Contents
3
Operational Precautions and Limitations
7
General Safety Information
7
Documentation Symbols and Conventions
7
Regulatory Compliance
8
Australia and New Zealand
8
Canada
8
Europe
8
United States
9
International
9
Electrical Precautions
10
Mains Supply
10
Protective Earth Conductor
10
Chemical Precautions
11
System Safe Fluids
12
Ventilation Precautions
13
Physical Precautions
14
Environmental Precautions
14
Electromagnetic Environment
14
Decommissioning and Disposal
16
Qualified Personnel
16
Laboratory Conditions
17
Safe Environmental Conditions
17
Performance Specifications
17
Equipment Use and Modification
17
Principles of Operation
19
System Overview
19
Hardware Overview
20
Ion Source Overview
26
Theory of Operation
32
Ion Source Installation
34
Prepare for Installation
34
Install the Probe
35
Connect the Ion Source Tubing
36
Install the Ion Source on the Mass Spectrometer
36
Inspect for Leaks
38
Ion Source Optimization
39
Sample Introduction
39
Method
39
Flow Rate
40
Turboionspray Probe Optimization
40
Flow Rate and Ion Source Temperature
41
Set up the System
41
Prepare the System
41
Set the Starting Conditions
42
Optimize the Turboionspray Probe Position
42
Optimize Source and Gas Parameters and Voltage
44
Optimize the Turbo Heater Temperature
44
APCI Probe Optimization
45
Optimization Tips
45
Operating Instructions
47
Start up the System
47
Syringe Pump
48
Adjust the Integrated Syringe Pump Position
48
Diverter Valve
48
Plumb the Diverter Valve in Injector Mode
49
Plumb the Diverter Valve in Diverter Mode
50
Shut down and Vent the System
52
Operating Instructions - User Workflows
53
Service and Maintenance Information - Mass Spectrometer
55
Recommended Maintenance Schedule
55
Clean the Surfaces
57
Clean the Front-End
58
Symptoms of Contamination
58
Required Materials
58
Cleaning Best Practices
59
Prepare the Mass Spectrometer
61
Clean the Curtain Plate
62
Clean the Front of the Orifice Plate
63
Put the Mass Spectrometer Back in Service
63
Empty the Source Exhaust Drain Bottle
63
Inspect the Roughing Pump Oil Level
66
Storage and Handling
67
Service and Maintenance - Ion Source
68
Ion Source Handling
69
Remove the Ion Source
70
Clean the Ion Source Surfaces
71
Clean the Probe
71
Remove the Probe
72
Replace the Electrode
72
Replace the Corona Discharge Needle
74
Replace the Sample Tubing
76
Storage and Handling
76
Mass Spectrometer Troubleshooting
77
A Calibration Ions and Solutions
82
B Principles of Operation - Ion Source
84
Electrospray Ionization Mode
84
APCI Mode
85
APCI Ionization Region
88
C Ion Source Optimization
90
Turboionspray Probe Optimization
90
Set up the System
91
Prepare the System
91
APCI Probe Optimization
91
Set up the System
92
Prepare the System
92
Set the Starting Conditions
93
Optimize Source and Gas Parameters
93
Adjust the Position of the Corona Discharge Needle
94
Optimize the APCI Probe Position
94
Optimize the Nebulizer Current
96
Optimize the APCI Probe Temperature
96
D Source Parameters and Voltages
98
Turboionspray Probe Parameters
98
APCI Probe Parameters
99
Parameter Descriptions
100
Probe Position
102
Solvent Composition
102
E Glossary of Symbols
104
F Glossary of Warnings
110
Contact Us
113
Customer Training
113
Online Learning Center
113
SCIEX Support
113
Cybersecurity
113
Documentation
113

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