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Sciex NanoSpray Manuals
Manuals and User Guides for Sciex NanoSpray. We have
1
Sciex NanoSpray manual available for free PDF download: Operator's Manual
Sciex NanoSpray Operator's Manual (92 pages)
Ion Source
Brand:
Sciex
| Category:
Laboratory Equipment
| Size: 6 MB
Table of Contents
Table of Contents
3
1 Operational Precautions and Limitations
6
Operational Precautions and Hazards
6
Chemical Precautions
7
System Safe Fluids
8
Laboratory Conditions
9
Operating Conditions
9
Performance Specifications
9
Equipment Use and Modification
10
Contact Us
10
Related Documentation
11
Technical Support
11
Laser Safety Information
11
Laser Classification
11
Scheduled Maintenance
12
Specifications
12
Labels on the Ion Source
12
2 Ion Source Overview
14
3 Ion Source Components
15
Camera and Illuminator
16
Ion Source Head
18
X-Y-Z Positioning Unit
18
Positioning Rails
19
Nanospray ® Interface Components
20
Optiflow TM Interface Components
20
Requirements
22
Gases
22
Solvents
22
4 Nanospray ® III Head Assembly and Installation
23
Assemble the Nanospray III Head
24
Remove the Nanospray III Head
26
Prepare the Sprayer Fitting
28
Insert the Emitter Tip
30
Install the Nanospray III Head on the Bracket
31
Connect the Sample Line
32
Adjust the Illuminator and Camera
34
Adjust and Focus the Camera
34
Adjust the Illuminator
36
Inspect for Leaks
40
5 Optimize the Nanospray III Head
42
6 Ion Source Maintenance
44
Remove the Ion Source
45
Install the Ion Source
46
Change Ion Sources
48
Change to a Different Ion Source (Optiflow TM Interface Components)
49
Change to the Nanospray ® Ion Source (Optiflow TM Interface
49
Components)
49
Change to a Different Ion Source (Nanospray ® Interface Components)
49
Change to the Nanospray ® Ion Source (Nanospray ® Interface
50
Components)
50
Change the Interface Components
50
Install the Optiflow TM Interface Components
50
Interface
51
Remove the Interface Components
52
Interface
52
Interface
53
Install the Interface Components
54
Interface
55
Remove the Monitor
56
Remove the Monitor from the 4500, 5500, 6500, 6500
56
Systems
56
Remove the Monitor from the 3200 and 4000 Series Systems
57
Install the Monitor
57
Install the Monitor 4500, 5500, 6500, 6500
57
And Tripletof ® Systems
57
Install the Monitor on 3200 and 4000 Series Systems
59
Connect the Monitor Cables
60
Bake the Interface
61
Clean the Ion Source
62
Clean the Nano Cell Heater Assembly
62
Required Materials
62
Tools and Supplies Available from the Manufacturer
63
Clean the Assembly
64
7 Troubleshooting
66
Mass Spectrometer Troubleshooting Tips
66
Syringe Troubleshooting Tips
67
External Pump Troubleshooting Tips
67
Nanospray ® III Head Troubleshooting Tips
68
Spray Plume Troubleshooting Tips
73
Monitor and Camera Troubleshooting Tips
73
Emitter Tip Troubleshooting Tips
74
Acquisition Troubleshooting Tips
75
A Principles of Operation
78
B Tips for Working with the Ion Source
80
Cleaving an Emitter Tip
80
Nanospray III Head
80
Sample Solvent Composition
80
Factors Affecting Optimization
80
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Sciex Categories
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