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7400040
Labconco 7400040 Manuals
Manuals and User Guides for Labconco 7400040. We have
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Labconco 7400040 manual available for free PDF download: User Manual
Labconco 7400040 User Manual (58 pages)
Freeze Dry System
Brand:
Labconco
| Category:
Laboratory Equipment
| Size: 1 MB
Table of Contents
Table of Contents
3
Chapter 1: Introduction
5
Freeze Dry Process
5
Freeze Dry Rates
6
Freeze Dry Capacity
7
Samples Containing Volatile Substances
7
Chapter 2: Prerequisites
9
Electrical Requirements
9
Location Requirements
9
Vacuum Pump Requirements
10
Unpacking Your Triad Freeze Dry
11
Chapter 3: Getting Started
12
Triad Freeze Dry Components
12
Setting up Your Triad Freeze Dry System
12
Component Orientation and Hose Connection
12
Venting the Vacuum Pump
13
Electrical Connection
13
Chemical Resistance of Freeze Dryer Components
13
Solvent Safety Precautions
15
Chapter 4: Operating Instruction
17
Triad Freeze Dry Controls
17
Operation Checklist
18
Vacuum Pump Ballast Setting
18
Operating the Triad Freeze Dry System
19
Set-Up
19
Setting the Operating Vacuum Level
21
Manual Control Operation
22
Automatic Control Operation
23
Programming
24
Starting the Freeze Dry Cycle
25
Changing the Program Parameters in the Middle of a Run
26
Stopping the Freeze Dry Cycle
26
Monitoring the System Operation
27
Sample Freezing
27
Shelf Loading
27
Freeze Drying Inside the Chamber
27
Manual Mode with Pre Frozen Samples
27
Manual Mode with Unfrozen Samples
28
Auto Mode with Pre Frozen Samples
28
Auto Mode with Unfrozen Samples
28
Stoppering Vials
29
Vacuum Break/Backfilling
29
Freeze Drying Using Manifold Valves
30
Defrosting
31
Alarms
32
Shelf Temperature Variations
32
Collector Temperature Variations
32
Vacuum
32
Vacuum Pump Service
32
Shelf Temperature Set Point
32
Power Failure
32
Platen Tilt
33
Chapter 5: Maintaining Your Freeze Dry System
35
Chapter 6: Using the Rs232 Receptacle
36
Computer Connection for Computer Interface
36
Chapter 7: Troubleshooting
39
Vacuum System
39
Vacuum Pump
39
Gaskets, Tubing, Connections, Sample Valves
40
Diagnostic Mode
41
Refrigeration Module Operation
43
Filling the Fluid System
43
Heat Transfer Fluid Precautions
45
Heat Transfer Fluid First Aid Procedures
45
Chapter 8: Modifying Your Freeze Dry System Display
46
Modifying the Display
46
Appendix A: Freeze Dry System Components
48
Appendix B: Freeze Dry System Dimensions
50
Appendix C: Freeze Dry System Specifications
51
Electrical Specifications
51
Environmental Conditions
51
Performance Specifications
52
Appendix D: Freeze Dry System Accessories
53
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