Endress+Hauser analytikjena multi N/C 2100 Manuals

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Endress+Hauser analytikjena multi N/C 2100 Operating Manual (102 pages)

TOC/TNb Analyzer

Brand: Endress+Hauser | Category: Laboratory Equipment | Size: 14 MB

Table of Contents
3
Index of Figures
6
Basic Information
7
User Manual Notes
7
Intended Use
7
General
7
Analyzer Area of Application
8
Warranty and Liability
9
Technical Data
10
Safety Instructions
12
Standards and Directives
12
Symbols and Signal Words Used
13
Safety Markings on the Analyzer
13
Technical Condition
14
Requirements for the Operating Personnel
14
Safety Instructions, Transport and Installation
15
Safety Instructions - Operation
16
General
16
Safety Instructions - Protection against Explosion and Fire
16
Safety Instructions - Electrical Equipment
16
Safety Instructions for Compressed Gas Containers and Systems
17
Handling of Auxiliary and Operating Materials
17
Safety Instructions - Service and Repair
18
Behavior in an Emergency
19
Technical Description
20
System Design
20
Fig. 1 Front View (Doors Open)
20
Components for Sample Preparation
21
TIC Lock
21
TC Lock
21
Microliter Syringes
21
Fig. 2 Lateral View Left (Side Wall Removed)
21
Fig. 3 TC Lock at the Top of the Device
21
Hose System
22
Fig.4 Hose Diagram
23
Components for Flow Adjustment
24
Fig.5 Needle Valve for Adjusting the Carrier Gas Flow
24
Fig.6 Needle Valve for Adjusting the NPOC Purging Flow (See Arrow)
24
Condensate Pump
25
4.1.2.3 Connection Method
25
Fig.7 Condensate Pump
25
Fig.8 Different Fast Connector Designs
25
Fig.9 Finger-Tight Screw Connection
25
Combustion System
26
Components for Gas Drying and Cleaning
26
Condensation Coil
26
Fig.10
26
Combustion Furnace (See Arrow)
26
TIC Condensate Container
27
Fig.11
27
Fig.12
27
Water Traps
28
Halogen Trap
28
Fig.13
28
Fig.14
28
Detectors
29
4.1.5.1 NDIR Detector
29
Electrochemical no Detector (Chd, Optional)
29
Indicator and Control Elements, Connections
30
Fig.15 LED to Indicate Readiness for Operation
30
Fig.16 LED Strip (Right Door Open)
30
Accessories
31
Fig.17 Connections on the Rear of the Device
31
Extension Options for the Analyzer
32
Sampler (Optional)
32
External Solids Module (Optional)
32
Double Furnace Solids Module (Optional)
32
TIC Solids Module (Optional)
32
Principle of Operation
33
Fig.18 Principle of Operation
33
Measuring Method
34
TC Analysis
34
TOC Analysis
34
TIC Analysis
35
NPOC Analysis
35
NPOC Analysis According to the NPOC Plus Method
35
TN B Analysis
36
Catalysts
36
Calibration
37
Calibration Strategies
37
4.5.1.1 Multiple Point Calibration with Constant Sample Volume
37
4.5.1.2 Single Point Calibration
37
Daily Factor
37
Calibration Method in Multiwin
37
4.5.3.1 Tc/Npoc
38
4.5.3.2 Tic
38
Fig
38
TOC (Diff)
39
4.5.3.4 NPOC Plus
39
4.5.3.5 Calibration TN
39
Method Characteristics
40
Other Calculations
41
Blank Values
41
Blank Water Values
41
Water for Preparing Standard Solutions Preparation Water Blind Value
41
Water for Diluting Solutions Diluting Blind Value
42
4.6.1.3 Eluate Blank Value
43
Boat Blank Value
43
First Commissioning
44
Site Requirements
44
Installation Conditions
44
Space Requirement
44
Power Supply
45
Gas Supply
45
Unpacking and Installing the Analyzer
45
Connecting Add-On Devices
46
Sampler APG 60
46
Fig.19
46
External Solids Module
48
Fig.20
48
Operation
49
General Information on Analysis Work
49
Switching on the Analyzer (Standard Commissioning)
50
Carrying out the Calibration
51
Preparing and Starting the Calibration
51
Fig.21
52
Fig.22
53
Displaying Calibration Results
54
Fig.23
54
Editing an Existing Calibration
55
Fig.24
56
Transferring Calibration Parameters to a Method
57
Fig.25
57
Managing Calibration Data
59
Fig.26
59
Performing Measurements
60
Measurement with Manual Sample Supply
60
Fig.27
60
Measurement with Sampler
61
Maintenance and Care
63
Maintenance Intervals
63
Adjustment and Setup Tasks
65
Adjust the Sampler
65
8.2.1.1 Adjust Position 1 / Furnace Position
65
8.2.1.2 Adjusting the Piston Position
66
Adjust the NPOC Purge Flow
67
Fig.28
67
Replacing the Water Traps
69
Replacing the Halogen Trap
71
Exchanging the Catalyst
72
Lifetime of the Catalyst
72
Removing the Combustion Tube
72
Filling the Combustion Tube
73
Inserting the Combustion Tube
75
Regenerating the TIC Reactor
77
Cleaning the TC Condensate Vessel
77
Maintaining the Condensation Coil
78
Condensation Coil
78
Installing the Condensation Coil
80
Removing and Installing the Combustion Furnace
81
Removing the Combustion Furnace
81
Installing the Combustion Furnace
82
Removing and Replacing the Pump Hose
83
Replacing the Hose Connections
84
Fig.30
85
Fig.31
85
Replacing the Septums
86
Troubleshooting
87
General Information
87
Error Messages in Multiwin
88
Status Errors - Indications in the System State Window
92
Equipment Faults and Analytical Problems
92
Transport and Storage
97
Transport
97
Preparing the Analyzer for Transport
97
Transport Notes
98
Moving the Analyzer in the Laboratory
98
Storage
99
Recommissioning after Transport or Storage
99
Assembling the Analyzer after Transport or Storage
99
Connecting the Analyzer
100
Disposal
102
Waste Water
102
Halogen Trap
102
Catalyst
102
Analyzer
102

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Endress+Hauser analytikjena multi N/C 2100 Operating Manual (102 pages)

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