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Bruker InsightMR manual available for free PDF download: User Manual
Bruker InsightMR User Manual (60 pages)
Brand:
Bruker
| Category:
Analytical Instruments
| Size: 15 MB
Table of Contents
Table of Contents
3
1 About this Manual
5
Policy Statement
5
Symbols and Conventions
5
2 Introduction
7
Concept
7
Intended Use
7
Limitation of Liability
8
Copyright
8
Warranty Terms
8
Customer Service
8
3 Safety
9
System Owner's Responsibility
9
Personnel Requirements
10
Unauthorized Persons
11
Instruction
11
Personal Protective Equipment
11
General Workplace Dangers
12
4 Design and Function
15
Description
15
Figure 4.1: Insightmr Flow Tube Assembly and the Transfer Line
15
Figure 4.2: Recommended Laboratory Setup
16
Software
17
Figure 4.3: Insightmr Flow Tube Assembly, Flow Tube Protector and Flow Interface
17
5 Transport, Packaging and Storage
19
Symbols on the Packaging
19
Inspection at Delivery
20
Packaging
20
Storage
21
6 Flow Unit Installation
23
Choose the Position of the Reactor
23
Figure 6.1: Typical Laboratory Setup for Monitoring Chemical Reaction
23
Connecting the Transfer Line Holder
24
Testing the Flow Unit Prior to Inserting It into the Magnet
24
Figure 6.2: the Transfer Line Holder
24
Figure 6.3: the Insightmr Flow Unit. from Left to Right: the Pump, the Reactor, the Flow Tube Assembly Secured with a Clamp Stand and the Thermostat
24
Figure 6.4: from Left to Right, Glass Flow Tube O-Rings, Vessel Connections ,And Flow Interface Valve
25
Temperature Control (Optional)
26
Figure 6.5: Temperature Control Connections
26
Software Installation
27
Figure 6.6: the Topspin Setup Tool
28
Figure 6.7: Selection of Components to Install
28
Figure 6.8: Topspin Release Letter Confirmation
28
Figure 6.9: Select an Installation Directory
29
Figure 6.10: Warning Message When the Installation Directory Does Not Exist
29
Figure 6.11: Select Setup Type
29
Figure 6.12: Select Products to Install
30
Figure 6.13: Select the NMR Super User
30
Figure 6.14: Select an NMR Administration Password
31
Figure 6.15: Installation Finished
31
Figure 6.16: Insightmr Release Letter
31
Software Configuration
32
Topspin Configuration
32
Insightmr Flow Mode Configuration
32
Figure 6.17: Configuration Check
32
Figure 6.18: Insightmr Icon
32
Figure 6.19: Starting the Icon Configuration
33
Figure 6.20: Iconnmr Configuration - Resource File Settings
33
Recommended Settings
34
Figure 6.21: Restoring the Default Settings
34
Figure 6.22: Configuring the Master Switches
34
Figure 6.23: Configuring the Automation Window
35
Figure 6.24: Selecting the Solvent and Probe Dependencies
35
Figure 6.25: Selecting the Tuning and Matching Options
36
Figure 6.26: Insightmr Acquisition Window Expansion Showing the New Protonated Solvents
36
Figure 6.27: Edsolv in Topspin
37
Figure 6.28: Solvents in the Iconnmr Configuration
37
Adding a New Protonated Solvent
38
7 Operation
39
Inserting and Using the Flow Unit
39
Figure 7.1: Inserting the Flow Unit Assembly into the Magnet
39
Acquiring NMR Data Using Insightmr Software
40
Figure 7.2: Mounting the Insulated Transfer Line
40
Removing the Flow Unit for Storage in the Transport Box
41
Returning the Spectrometer to Normal Operation
41
Figure 7.3: the Unhook Button
41
8 Flow Tube Assembly - Insertion Checklist
43
Prepare the NMR System
43
Figure 8.1: Insightmr Flow Unit Laboratory Setup
43
Prepare the Flow Tube Assembly
44
Connect the Temperature Control Equipment (Optional)
44
Connect the Sample Supply (Reactor or Equivalent)
44
Insert the Flow Tube Assembly
45
The System Is Ready to be Used
45
9 Flow Tube Assembly - Removal Checklist
47
Prepare the Flow Tube Assembly
47
Remove the Flow Tube Assembly
47
Figure 9.1: Insightmr Flow Unit Laboratory Setup
47
Storage
48
Prepare the NMR System
48
The System Is Ready for Normal Usage
48
10 Insightmr Glass Flow Tube Exchange Instructions
49
Removing the Glass Flow Tube
49
Mounting the Glass Flow Tube
50
11 Dismantling and Disposal
51
Dismantling
51
Disposal Europe
51
Disposal USA and Other Countries
52
12 Technical Data
53
13 Contact
55
List of Figures
57
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