Agilent Technologies MSD 5977B Series Manuals

Agilent Technologies MSD 5977B Series Manuals

Manuals and User Guides for Agilent Technologies MSD 5977B Series. We have 1 Agilent Technologies MSD 5977B Series manual available for free PDF download: Operating Manual

Agilent Technologies MSD 5977B Series Operating Manual

Agilent Technologies MSD 5977B Series Operating Manual (254 pages)

Brand: Agilent Technologies | Category: Water Pump | Size: 16.42 MB

Table of Contents

About this Manual
3
Hardware User Information
4
Table of Contents
5
1 Introduction

13
- 5977B Series MSD Version
  14
- Abbreviations Used
  15
- The 5977B Series MSD
  17
  - Physical Description
    17
  - Vacuum Gauge
    18
- MSD Hardware Description
  19
- Important Safety Warnings
  21
- Hydrogen Safety
  24
  - GC Precautions
    24
  - Dangers Unique to GC/MSD Operation
    25
  - Hydrogen Accumulation in an MSD
    25
  - Precautions
    26
- Safety and Regulatory Certifications
  28
  - Information
    29
  - Symbols
    29
  - Electromagnetic Compatibility
    30
  - Sound Emission Declaration
    30
- Intended Use
  31
- Cleaning/Recycling the Product
  31
- Accidental Liquid Spillage
  31
- Moving or Storing the MSD
  31
- To Replace the Primary Fuses
  32
2 Installing 8890 GC Columns

35
3 Installing Intuvo 9000 GC Columns

55
4 Installing 7890 GC Columns

77
5 Operating in EI Mode

101
6 Operating in CI Mode

144
- General Guidelines
  144
- CI Autotune
  145
- To Operate the CI MSD
  147
- To Pumpdown the MSD in CI Mode
  148
- To Set up the Software for CI Operation
  149
- To Operate the Reagent Gas Flow Control Module
  151
- To Set up Methane Reagent Gas Flow
  154
- To Use Other Reagent Gases
  156
- To Perform a PCI Autotune (Methane Only)
  159
- To Perform an NCI Autotune (Methane Reagent Gas)
  161
- To Verify PCI Performance
  163
- To Verify NCI Performance
  164
- To Monitor CI Mode High Vacuum Pressure
  165
7 General Maintenance

167
- Before Starting
  168
- Maintaining the Vacuum System
  173
- Maintaining the Analyzer
  174
- To Open the Analyzer Chamber
  176
- To Remove the EI HES
  178
- To Connect/Disconnect Wiring to the EI HES
  180
- To Disassemble the EI HES
  181
- To Clean the EI HES
  184
- To Assemble the EI HES
  187
- To Remove the EI HES Filaments
  192
- To Install the EI HES Filament
  194
- To Install the EI HES
  195
- To Remove the EI XTR, SS, or Inert Source
  196
- To Connect/Disconnect Wiring from the EI XTR, SS, and Inert Sources
  197
- To Disassemble the EI SS or EI Inert Source
  198
- To Disassemble the EI XTR Source
  201
- To Clean an EI XTR, SS, or Inert Source
  204
- To Assemble an EI SS or Inert Source
  209
- To Assemble the EI XTR Source
  212
- To Replace a Filament in an EI XTR, SS, or Inert Source
  215
- To Install the EI XTR, SS, or Inert Source
  217
- To Replace the Electron Multiplier Horn
  218
- To Close the Analyzer Chamber
  220
101 CI Maintenance

221

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