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Summary of Contents for Barnstead|Thermolyne NANOpure DIamond Analytical
- Page 1 ARNSTEAD HERMOLYNE NANOpure DIamond ® ™ Analytical ultrapure water system Operation Manual Series 1190 Model No. Voltage D11901 100V - 240V LT1190X1 • 6/22/00...
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Page 2: Table Of Contents
Table of Contents Safety Information ......................................3 Alert Signals......................................3 Warnings ........................................3 Introduction ........................................5 General Usage......................................5 General Specifications ....................................6 Environmental Conditions ..................................7 Declaration of Conformity ..................................7 Unpacking ........................................8 Installation ........................................9 Choosing a Site ......................................9 Other Accessories ....................................10 Bench Mounting ....................................10 Wall Mounting ......................................10 Installing the Control Panel in a Remote Location..........................11 Water Connections ....................................12 Controls ........................................13... -
Page 3: Safety Information
Care should be taken Note when installing, operating or servicing Barnstead Notes alert you to pertinent facts and products. The specific safety notes pertinent to this conditions. - Page 4 AFETY NFORMATION Avoid splashing disinfecting solutions on clothing or skin. Ensure all piping connections are tight to avoid chemical leakage. Ensure adequate ventilation. Carefully follow manufacturer’s safety instructions on labels of chemical containers and material safety data sheets. Depressurize system prior to removing the cartridge pack.
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Page 5: Introduction
Introduction Congratulations on your purchase of a Barnstead| Thermolyne NANOpure DIamond Analytical ultrapure water system. This water purification system is designed to provide high resistivity, reagent grade water that exceeds ASTM Type I, CAP and NCCLS Type I stan- dards. It uses a four-stage deionization process and a 0.2... -
Page 6: General Specifications
Volumetric Dispense Accuracy: ± 5% Repeatability: ± 3% Electrical Requirements The NANOpure DIamond Analytical is equipped with 2 power cords to be plugged into an electrical outlet of the appropriate voltage. Voltage and Frequency (Nominal) Model D11901 100-240 VAC, 47-63 Hz, 1 phase... -
Page 7: Environmental Conditions
Altitude limit: 3,500 meters. Storage: -25°C to 65°C; 10% to 85% relative humidity. Declaration of Conformity Barnstead|Thermolyne hereby declares under its sole responsibility that this product conforms with the technical requirements of the following standards: EMC: EN 61000-3-2 Limits for Harmonic Current Emissions... -
Page 8: Unpacking
(see list below) are removed from the packaging materials before discarding. Put the NANOpure DIamond Analytical on a bench. Sanitization Cartridge CMX25 Wall Bracket (Unit) Wall Bracket (Remote Display) -
Page 9: Installation
Installation Choosing a Site Caution The NANOpure DIamond Analytical features a removable Wall composition, condition and control panel display which allows the system to be construction as well as fastener type mounted almost anywhere within the laboratory. Use the must be considered when mounting wall bracket for wall mounted systems as a template to this unit. -
Page 10: Other Accessories
Wall Mounting surface and/or equipment. If you are Install the NANOpure DIamond Analytical on a wall in a unsure of mounting surface composi- convenient location that is accessible to water, an atmos- tion, condition and construction or cor- pherically vented drain and electricity. -
Page 11: Installing The Control Panel In A Remote Location
NSTALLATION Installing the Control Panel in a Note The removable control panel was not Remote Location designed to be repeatedly removed For your convenience, the control panel can be removed from the unit, therefore, you may from the unit and mounted at a convenient location within experience difficulty when attempting 10 ft. -
Page 12: Water Connections
Pump Interlock Atmospheric Drain Connection Remote 2 When the NANOpure DIamond Analytical flushes, the water used is sent to drain through this connection. To install: Remote 1 Locate the drain water tubing. This is the 1/4” (.64 cm) O.D. tubing that is approximately 6 ft.(1.9 m.) long. -
Page 13: Controls
Note Control Panel The removable control panel was The NANOpure DIamond Analytical is controlled through a not designed to be repeatedly panel which incorporates switches to control its functions: removed from the unit, therefore, START/STOP, STANDBY, DISPENSE, DOWN, UP, you may experience difficulty when ENTER and BACK. -
Page 14: Switches
ONTROLS Switches When the main power switch (on the lower back right side of the unit as you face the unit) is ON, the switches on the control panel function as follows: START/STOP allows you to alternate the unit between the normal (recirculation) mode;... -
Page 15: Initial Operation
Initial Operation Cartridge packs will come bagged with four manifold connection caps. Part Application DIamond Kit Organic Free R/O & Distilled Feed D50280 Ultra-Low Organics, Type 1 Water, Reverse Osmosis or Distilled Water Feed Warning Allow cartridge pack to warm to room DIamond Kit Organic Free Deionized Feed temperature before installation. -
Page 16: Initial Rinse
NITIAL PERATION Initial Rinse Attach the feed water line to the unit by snapping the quick disconnect coupling into the quick disconnect body in the lower left back of the unit. Attach an atmospheric drain line [1/4” ((.64 cm)] tubing by pushing into the quick connect fitting on the lower left back of unit. -
Page 17: System Sanitization Procedure
NITIAL PERATION System Sanitization Procedure Warning Your NANOpure DIamond Analytical has been shipped Avoid splashing disinfecting solution with a cleaning syringe (Cat. No. CMX25). When the sys- on clothing or skin. tem is new or whenever a new cartridge pack is installed, the system should be sanitized (cleaned). - Page 18 NITIAL PERATION 13. Press the UP or DOWN arrow to select (YES) and press ENTER. Display will now read, “Unit Sanitizing.” 14. Unit may now be left unattended until display reads, “Sanitization Complete: Press ENTER.” 15. After sanitization is complete the unit will return to the (Idle) mode.
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Page 19: Normal Operation
Normal Operation Turn the system power ON by depressing the main power switch to the “I” position. The system greeting display indicates the type of unit you own. This greeting is “Base.” Note On initial start-up, the purity meter The system electronics will initialize and check may display “...MΩ-cm or uS/cm.”... -
Page 20: User Settings
User Settings Adjusting Display Brightness From the (Idle) mode, when the display reads, “NANOpure Diamond (Idle) xx:xx:xx xx/xx/xx,” press the UP or DOWN arrow until display reads, “Advanced Menu?” Press ENTER. Press ENTER to proceed through the options until “Set Display Brightness” is displayed. Press the UP or DOWN arrow to choose “Yes.”... -
Page 21: Setting The Cell Constant
ETTINGS Press ENTER. Press ENTER when the unit displays “Printer Attached?” When prompted with “Date Format” press the UP or DOWN arrow to show the date format desired. Press ENTER to select the desired for- mat and continue. When prompted with “Set Date,” press the UP or DOWN arrow to choose “Yes,”... - Page 22 ETTINGS Unlatch and open the right side door. Find and copy down the two cell constants attached to the gray cable,leaving the electron- ics board mounted on the inside of the right side door. Close and latch the right side door. Reconnect the power cable and turn unit ON.
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Page 23: Use Of Standby Mode
“Standby (Recirculating) xx minutes.” Press START/STOP to return to the recirculating mode. Selecting the Set Point The NANOpure DIamond Analytical electronics include a user programmable set point which alerts you when water quality falls below the programmed set point. The set point is user selectable from 1-18 MΩ-cm (factory set at... -
Page 24: Resetting The Sanitization Timer
ETTINGS Press ENTER. Press BACK to return to the (Idle) mode. The second line of the display will show a “Below Set point” message once every 8 to 10 seconds when the measurement is below the set point. (The set point indica- tion is set at the factory at 10 MΩ-cm.) Resetting the Sanitization Timer From the (Idle) mode, when the display reads,... -
Page 25: Setting Volumetric Dispensing
Volumetric dispensing is based upon display is showing purity, press the UP or total fluid volume entering the DOWN arrow until the display reads, “Auto NANOpure DIamond Analytical. Point Dispense Menu?” of drawoff accuracy will be compro- mised if you are dispensing water vol- Press ENTER. -
Page 26: Setting Timed Dispensing
ETTINGS Setting Timed Dispensing From the normal recirculating mode, when the dis- play is showing purity, press the UP or DOWN arrow until the display reads, “Auto Dispense Menu?” Press ENTER. Display will read, “Dispense Method.” Press the UP or DOWN arrow to select TIME. Press ENTER. -
Page 27: Temperature Compensation
ETTINGS Press the UP or DOWN arrow to select “MΩ-cm” or “uS/cm” Press ENTER. Press BACK to return to the normal recirculating mode. Temperature Compensation Note (Factory set to “ON.”) Purity displayed will have an asterisk From the normal recirculating mode, when the (*) the the left of the reading (* xx.x display is showing purity, press the Up or MΩ-cm or * x.xx uS/cm) to inform the... -
Page 28: Installing Float Or Pressure Switch
Screw the switch into the top of the tee, then connect the inlet tubing of the NANOpure DIamond Analytical into the re- maining opening of the PVC tee. Route the cable from the float or low pressure switch to the top left of the NANOpure DIamond Analytical. -
Page 29: N.i.s.t Calibration Module
N.I.S.T Calibration Module Performing an Electronic Calibration Using the Optional N.I.S.T. Calibration Module If you purchased the optional N.I.S.T. calibration module (Catalog No. E896X5) you can perform a calibration of the NANOpure DIamond purity sensing electronics traceable to N.I.S.T. standards. Disconnect power cord from the unit. -
Page 30: Remote Dispenser
N.I.S.T. C ALIBRATION ODULE 11. Press BACK to return to the (Idle) mode. 12. Turn the main power switch to the OFF “O” position. Unplug the unit. 13. Remove the calibration module and reconnect the cell. 14. Reattach the cover plate and close and latch the door. -
Page 31: Computer/Printer Setup
Computer/Printer Setup Connecting NANOpure DIamond to Computer and Communicating Though the RS-232 Port Using Hyperterminal or Procomm Hyperterminal RS-232 Capture Instructions Connect the 9 pin serial cable (part no. WHX18) from the NANOpure DIamond RS-232 port to COM2: port or (COM1: port) on back of computer. - Page 32 OMPUTER RINTER ETUP capture text. Accepting default will put the file which you name in the c:/windows directory called capture.txt and the file will be an ASCII text file. 11. You should see the data on the computer screen. 12. When you are finished storing data from the NANOpure DIamond, save your file.
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Page 33: Connecting And Starting The Printer
OMPUTER RINTER ETUP 12. Type in 21 <Enter>, sets to COM2: or (Type in 20 <Enter>, sets to COM1:), depending on your computer. 13. Type in 24 <Enter>, saves settings. 14. Type ESC to exit setup menu. 15. Procomm is now ready to accept input from the NANOpure DIamond. -
Page 34: Printer Setup
OMPUTER RINTER ETUP From the “Printer Attached” display, press the Up or DOWN arrow for (YES). Press ENTER. Press BACK twice to return to the (Idle) mode. During normal Recirculation mode, a purity and temperature reading will be printed once every 12 minutes. - Page 35 OMPUTER RINTER ETUP down; or—the paper may be jammed in the printer. Turn the printer OFF before checking for jammed paper. Note Remove the paper jam and turn the printer back ON. If A colored stripe along the edge of the the printer still will not print, unplug it and refer servicing paper indicates that you are approach- to qualified personnel.
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Page 36: Maintenance And Servicing
Maintenance and Servicing General Cleaning Instructions Warning Disconnect electrical service to the unit. Wipe exterior • Avoid splashing mild detergent surfaces with lightly dampened cloth containing mild soap or weak acid on clothing or solution. skin • Ensure all piping connections are tight to avoid chemical Cell Cleaning leakage... -
Page 37: System Sanitization
AINTENANCE AND ERVICING System Sanitization Note After sanitization is complete (approximately 3.5 hours), The sanitization timer will display after place the unit into its normal (recirculation) mode to allow six months, reminding you to sanitize the system to recirculate overnight after cleaning. the unit. -
Page 38: System Depressurization
AINTENANCE AND ERVICING 14. Unit may now be left unattended until the display reads, “Sanitization Complete: Press ENTER.” 15. After sanitization is complete and the user presses “ENTER” the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculating mode. -
Page 39: Cartridge Pack Replacement
Sanitize your NANOpure DIamond Analytical Warning and replace the cartridge pack when the product water A full cartridge pack may weigh about purity drops below acceptable levels of resistivity, when 20 lbs. -
Page 40: 0.2 Micron Filter Replacement
Remove the new 0.2 micron filter assembly from clogs rapidly after installation, the the bag and insert it into the dispense arm mani- NANOpure DIamond Analytical may fold. Gently turn it clockwise until it is fully seat- need to be sanitized to remove bacter- ed. -
Page 41: Fuse Replacement
Reattach the power cord. Operate normally. Shutdown If the NANOpure DIamond Analytical is to be shut down for an extended period of time, the unit should be com- pletely drained and the cartridge pack removed to prevent the growth of bacteria. If the system has remained inac-... -
Page 42: Troubleshooting
Troubleshooting Problem Possible Causes Solutions NANOpure DIamond completely No electrical power to NANOpure Ensure NANOpure DIamond power inactive (pump and display DIamond. cord is connected to a live power not operating.) source and completely plugged into electrical outlet as well as power entry module on the unit. - Page 43 Poor quality feed water. If a Barnstead ROpure is the feed water source, check that the membrane is functioning properly. If a Barnstead Still is the feed water source, ensure that the distillate temperature to the NANOpure DIamond does not exceed 40°C (104°F).
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Page 44: Replacement Parts
(filters, resin cartridges, etc.) and other items of limited life (indicator lights, fuses, etc.) that you can expect to replace on a more or less random basis. Where practical, Barnstead|Thermolyne recommends the frequency of replacement, or provides information on life expectancy from which you may calculate a replacement interval compatible with your usage pattern. -
Page 45: Safety Stock
EPLACEMENT ARTS Safety Stock For critical applications where performance with minimum downtime is required, Barnstead|Thermolyne rec- ommends that you maintain a local stock of those parts listed in the General Maintenance Parts and Safety Stock sections. Description Catalog No. Recommended Quantity... -
Page 46: Flow Chart Operational Overview)
Flow Chart power switch turned on Barnstead /Thermolyne Vx.xx Style English Unit Initialization & Meter Calibration Check NANOpure DIamond (Idle) xx :xx :xx xx /xx /xx standby start_stop back key up or down enter key key pressed pressed keys pressed... -
Page 47: Wiring Diagram
Wiring Diagram POWER ENTRY MODULE SWITCH & FUSES: 120V: (2) FSX47 230V: (2) FSX54 NEUTRAL CHASSIS GND CHASSIS LINE REMOTE DISPLAY CONNECTOR (SPG) MODEL #s D11911 & D11931 ONLY DIAGRAM COMPONENT LIST MODEL NO. AND OUR PART NO.(s) REF. DESCRIPTION D11901 D11901 D11911... -
Page 48: Ordering Procedures
If the dealer cannot handle your request, then contact our Customer Service Department at 319-556-2241 or 800-553-0039. Prior to returning any materials to Barnstead|Thermolyne Corp., please contact our Customer Service Department for a “Return Goods Authorization” number (RGA). -
Page 49: One Year Limited Warranty
(1) year, the parts necessary to remedy any such defect. The warranty period shall commence either six (6) months following the date the product is sold by Barnstead|Thermolyne or on the date it is purchased by the original retail consumer, whichever date occurs first. - Page 52 Barnstead|Thermolyne 2555 Kerper Blvd. 9001 P.O. Box 797 Dubuque, IA 52004-2241 REGISTERED Phone: 319-556-2241 800-553-0039 Fax: 319-589-0516 E-Mail Address: mkt@barnstead.com...
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