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Summary of Contents for Barnstead|Thermolyne NANOpure DIamond D11931
- Page 1 ARNSTEAD HERMOLYNE NANOpure DIamond ® ™ Life Science (UV/UF) ultrapure water system Operation Manual Series 1193 Model No. Voltage D11931 100V - 240V LT1193X1 • 6/22/00...
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Page 2: Table Of Contents
Table of Contents Safety Information ......................................3 Alert Signals......................................3 Warnings ........................................3 Introduction ........................................5 General Usage......................................5 General Specifications ....................................6 Environmental Conditions ..................................7 Declaration of Conformity ..................................7 Unpacking ........................................8 Installation ........................................9 Choosing a Site ......................................9 Ultrafilter Installation ....................................10 UV Lamp Installation ....................................11 Other Accessories ....................................11 Bench Mounting ....................................12 Wall Mounting ......................................12 Installing the Control Panel in a Remote Location ..........................13... -
Page 3: Safety Information
Care should be taken Note when installing, operating or servicing Barnstead Notes alert you to pertinent facts and products. The specific safety notes pertinent to this conditions. - Page 4 AFETY NFORMATION Avoid splashing disinfecting solutions on clothing or skin. Ensure all piping connections are tight to avoid chemical leakage. Ensure adequate ventilation. Carefully follow manufacturer’s safety instructions on labels of chemical containers and material safety data sheets. Depressurize system prior to removing the cartridge pack.
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Page 5: Introduction
Introduction Congratulations on your purchase of a Barnstead| Thermolyne NANOpure DIamond Life Science (UV/UF) ultrapure water system. This water purification system is designed to provide nuclease-free (RNase and DNase), DNA-free, pyrogen-free, low TOC, high resistivi- ty, reagent grade water that exceeds ASTM Type I, CAP and NCCLS Type I standards. -
Page 6: General Specifications
Repeatability: ± 3% Electrical Requirements The NANOpure DIamond Life Science (UV/UF) is equipped with 2 power cords to be plugged into an electri- cal outlet of the appropriate voltage. Voltage and Frequency (Nominal) Model D11931 100-240 VAC, 47-63 Hz, 1 phase... -
Page 7: Environmental Conditions
Altitude limit: 3,500 meters. Storage: -25°C to 65°C; 10% to 85% relative humidity. Declaration of Conformity Barnstead|Thermolyne hereby declares under its sole responsibility that this product conforms with the technical requirements of the following standards: EMC: EN 61000-3-2 Limits for Harmonic Current Emissions... -
Page 8: Unpacking
Unpacking Remove the unit from its shipping container. Remove all contents carefully. Ensure that the UV lamp, ultrafilter, feed and drain tubing, sanitization cartridge, wall bracket, accesso- ry parts bag and power cords (see list below) are removed from the packaging materials before discarding. -
Page 9: Installation
Installation Choosing a Site Caution The NANOpure DIamond Life Science (UV/UF) features a Wall composition, condition and removable control panel display which allows the system construction as well as fastener type to be mounted almost anywhere within the laboratory. must be considered when mounting Use the wall bracket for wall mounted systems as a tem- this unit. -
Page 10: Ultrafilter Installation
NSTALLATION Ultrafilter Installation Remove the ultrafilter from its protective bag. Install the ultrafilter as follows: Note Open the front (right side) door and right side Do not install the ultrafilter until the door. NANOpure DIamond Life Science (UV/UF) is ready for use. If the unit Remove restraints (twist tie) from the three sits for longer than 72 hours without tubes. -
Page 11: Uv Lamp Installation
NSTALLATION UV Lamp Installation Note Locate the UV chamber inside the left door of the The UV lamp contains mercury. If NANOpure DIamond Life Science (UV/UF). Install the UV broken or no longer needed, do not Lamp as follows: dispose of the UV lamp in the trash. Disconnect the power cord from the unit. -
Page 12: Bench Mounting
NSTALLATION Bench Mounting Place the NANOpure DIamond Life Science (UV/UF) on a bench top that is accessible to pretreated water, electricity and an atmospheri- cally vented drain. Caution Wall Mounting Wall composition, condition and con- Install the NANOpure DIamond Life Science (UV/UF) on a struction, as well as fastener type, wall in a convenient location that is accessible to water, must be considered when mounting... -
Page 13: Installing The Control Panel In A Remote Location
NSTALLATION Installing the Control Panel in a Note The removable control panel was not Remote Location designed to be repeatedly removed For your convenience, the control panel can be removed from the unit, therefore, you may from the unit and mounted at a convenient location within experience difficulty when attempting 10 ft. -
Page 14: Water Connections
NSTALLATION Water Connections Feed Water Connection Caution Locate the length of 3/8” O.D. tubing provided Do not connect feed water until direct- with the unit with a quick disconnect insert on ed to do so during “Initial Sanitization.” one end and a 3/8” (.95 cm) O.D. X 1/4” (.64 cm) NPT tubing adapter on the other. -
Page 15: Controls
Please refer to “Installing the Control Panel in a Remote Location” in the “Installation” section of this manual for more information about how to remove the STANDBY control panel from the unit. START BACK ENTER STOP Barnstead DISPENSE NANOpure DIamond Life Science (UV/UF) Control Panel... -
Page 16: Switches
ONTROLS Switches When the main power switch (on the lower back right side of the unit as you face the unit) is ON, the switches on the control panel function as follows: START/STOP allows you to alternate the unit between the normal (recirculation) mode;... -
Page 17: Initial Operation
Initial Operation Cartridge packs will come bagged with four manifold connection caps. Part Application DIamond Kit Organic Free R/O & Distilled Feed D50280 Ultra-Low Organics, Type 1 Water, Reverse Osmosis or Distilled Water Feed DIamond Kit Organic Free Deionized Feed D50281 Ultra-Low Organics, Type 1 Water, Deionized Water Feed Warning... -
Page 18: Initial Rinse
NITIAL PERATION Initial Rinse Attach the feed water line to the unit by snapping the quick disconnect coupling into the quick disconnect body in the lower left back of the unit. Attach an atmospheric drain line [1/4” (.64 cm) ] tubing by pushing into the quick connect fitting on the lower left back of unit. -
Page 19: System Sanitization Procedure
NITIAL PERATION System Sanitization Procedure Your NANOpure DIamond Life Science (UV/UF) has been Warning shipped with a cleaning syringe (Cat. No. CMX25). When Avoid splashing disinfecting solution the system is new or whenever a new cartridge pack is on clothing or skin. installed, the system should be sanitized (cleaned). - Page 20 NITIAL PERATION and press ENTER. Display will now read, “Unit Sanitizing.” 14. Unit may now be left unattended until display reads, “Sanitization Complete: Press ENTER.” 15. After sanitization is complete the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculation mode.
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Page 21: Normal Operation
Normal Operation Turn the system power ON by depressing the main power switch to the “I” position. The system greeting display indicates the type of unit you own. This greeting is “UV/UF.” Note On initial start-up, the purity meter The system electronics will initialize and check may display “...MΩ-cm or uS/cm.”... -
Page 22: User Settings
User Settings Adjusting Display Brightness From the (Idle) mode, when the display reads, “NANOpure Diamond (Idle) xx:xx:xx xx/xx/xx,” press the UP or DOWN arrow until display reads, “Advanced Menu?” Press ENTER. Press ENTER to proceed through the options until “Set Display Brightness” is displayed. Press the UP or DOWN arrow to choose “Yes.”... -
Page 23: Setting The Cell Constant
ETTINGS Press ENTER. Press ENTER when the unit displays “Printer Attached?” When prompted with “Date Format” press the UP or DOWN arrow to show the date format desired. Press ENTER to select the desired for- mat and continue. When prompted with “Set Date,” press the UP or DOWN arrow to choose “Yes,”... - Page 24 ETTINGS Unlatch and open the right side door. Find and copy down the two cell constants attached to the gray cable, leaving the electron- ics board mounted on the inside of the right side door. Close and latch the right side door. Reconnect the power cord and turn unit ON.
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Page 25: Use Of Standby Mode
ETTINGS Use of Standby Mode Note At the end of the work day, place the NANOpure When in Standby mode, press DIamond Life Science (UV/UF) in Standby mode for the START/STOP to continue normal night. To place the unit in Standby mode: operation. -
Page 26: Resetting The Sanitization Timer
ETTINGS Press ENTER. Press BACK to return to the (Idle) mode. The second line of the display will show a “Below Set point” message once every 8 to 10 seconds when the measurement is below the set point. (The set point indica- tion is set at the factory at 10 MΩ-cm.) Resetting the Sanitization Timer From the (Idle) mode, when the display reads,... -
Page 27: Setting Volumetric Dispensing
ETTINGS Press the UP or DOWN arrow to select “Yes.” Press ENTER and the timer will be reset for approximately five months of operational time. The display will now display “Rest San Timer.” Press BACK two times to return to the (Idle) mode. Note Volumetric dispensing is based upon Setting Volumetric Dispensing... -
Page 28: Setting Timed Dispensing
ETTINGS Setting Timed Dispensing From the normal recirculating mode, when the dis- play is showing purity, press the UP or DOWN arrow until the display reads, “Auto Dispense Menu?” Press ENTER. Display will read, “Dispense Method.” Press the UP or DOWN arrow to select TIME. Press ENTER. -
Page 29: Temperature Compensation
ETTINGS Press the UP or DOWN arrow to select “MΩ-cm” or “uS/cm” Press ENTER. Press BACK to return to the normal recirculating mode. Temperature Compensation Note (Factory set to “ON.”) Purity displayed will have an asterisk From the normal recirculating mode, when the (*) the the left of the reading (* xx.x display is showing purity, press the Up or MΩ-cm or * x.xx uS/cm) to inform the... -
Page 30: Installing Float Or Pressure Switch
Installing Float or Pressure Switch Accessories D8964 (float switch) and D2706 (pressure switch) are designed to protect the NANOpure DIamond Life Science (UV/UF) pump by alerting the system of an inadequate feed water condition so that the pump can be shut down. -
Page 31: N.i.s.t Calibration Module
N.I.S.T Calibration Module Performing an Electronic Calibration Using the Optional N.I.S.T. Calibration Module If you purchased the optional N.I.S.T. calibration module (Catalog No. E896X5) you can perform a calibration of the NANOpure DIamond purity sensing electronics traceable to N.I.S.T. standards. Disconnect power cord from the unit. -
Page 32: Remote Dispenser
N.I.S.T. C ALIBRATION ODULE 11. Press BACK to return to the (Idle) mode. 12. Turn the main power switch to the OFF “O” position. Unplug the unit. 13. Remove the calibration module and reconnect the cell. 14. Reattach the cover plate and close and latch the door. -
Page 33: Computer/Printer Setup
Computer/Printer Setup Connecting NANOpure DIamond to Computer and Communicating Though the RS-232 Port Using Hyperterminal or Procomm Hyperterminal RS-232 Capture Instructions Connect the 9 pin serial cable (part no. WHX18) from the NANOpure DIamond RS-232 port to COM2: port or (COM1: port) on back of computer. - Page 34 OMPUTER RINTER ETUP capture text. Accepting default will put the file which you name in the c:/windows directory called capture.txt and the file will be an ASCII text file. 11. You should see the data on the computer screen. 12. When you are finished storing data from the NANOpure DIamond, save your file.
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Page 35: Connecting And Starting The Printer
OMPUTER RINTER ETUP 12. Type in 21 <Enter>, sets to COM2: or (Type in 20 <Enter>, sets to COM1:), depending on your computer. 13. Type in 24 <Enter>, saves settings. 14. Type ESC to exit setup menu. 15. Procomm is now ready to accept input from the NANOpure DIamond. -
Page 36: Printer Setup
OMPUTER RINTER ETUP From the “Printer Attached” display, press the Up or DOWN arrow for (YES). Press ENTER. Press BACK twice to return to the (Idle) mode. 10. During normal Recirculation mode, a purity and temperature reading will be printed once every 12 minutes. - Page 37 OMPUTER RINTER ETUP Installing the Paper Roll Note When the red PAPER OUT light illuminates, it is time to A colored stripe along the edge of the replace the paper roll. Replace the paper roll (AY669X4) paper indicates that you are approach- as follows: ing the end of the tape.
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Page 38: Maintenance And Servicing
Maintenance and Servicing General Cleaning Instructions Warning Disconnect electrical service to the unit. Wipe exterior • Avoid splashing mild detergent surfaces with lightly dampened cloth containing mild soap or weak acid on clothing or solution. skin • Ensure all piping connections are tight to avoid chemical Cell Cleaning leakage... -
Page 39: System Sanitization
AINTENANCE AND ERVICING System Sanitization Note For UV/UF units, it is best to perform cleaning procedures The sanitization timer will display after early in the afternoon. After sanitization is complete six months, reminding you to sanitize (approximately 3.5 hours), place the unit into its normal the unit. -
Page 40: System Depressurization
AINTENANCE AND ERVICING 14. Unit may now be left unattended until the display reads, “Sanitization Complete: Press ENTER.” 15. After sanitization is complete and the user presses “ENTER” the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculating mode. -
Page 41: Micron Filter Replacement
0.2 micron filter clogs rapidly after installation even though the cartridge pack was thoroughly rinsed before the 0.2 micron filter was installed. The simple-to-use cleaning syringe is available from BarnsteadlThermolyne (Catalog Number CMX25). This is used to effect a com- plete sanitization. -
Page 42: Ultrafilter Replacement
AINTENANCE AND ERVICING Caution Do not overtighten the 0.2 micron filter or use excessive force in seating it. The filter can be damaged by over- tightening or excessive force. 0.2 Micron Filter Replacement Replace the 0.2 micron final filter whenever any of the fol- lowing conditions occur: every 30 days, the product water Note flow rate is reduced or bacteria break through. - Page 43 AINTENANCE AND ERVICING Pull the ultrafilter out of the unit and turn it to the left side. (This will make it easier to disconnect the bottom fitting.) Using the tool supplied with the ultrafilter, simul- taneously push and hold the collet on the ultrafil- ter in while pulling the bottom fitting out of the connector.
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Page 44: Uv Lamp Replacement
AINTENANCE AND ERVICING UV Lamp Replacement Warning The ultraviolet lamp requires changing every 5-6 months. This unit is equipped with an ultraviolet Lamp Life will vary according to the number of times the lamp. Ultraviolet radiation is harmful to NANOpure DIamond Life Science (UV/UF) is turned on the eyes and skin. -
Page 45: Fuse Replacement
AINTENANCE AND ERVICING reduce the effectiveness of the lamp. If the glass portion of the lamp is touched, clean it with a damp, lint-free cloth: use isopropyl alcohol as required. Insert the lamp halfway into the UV lamp cham- ber and plug UV cable in, then fully insert the lamp into the chamber. -
Page 46: Shutdown
AINTENANCE AND ERVICING Shutdown If the NANOpure DIamond Life Science (UV/UF) is to be shut down for an extended period of time, the unit should be completely drained and the cartridge pack removed to prevent the growth of bacteria. If the system has remained inactive and full of water for more than 96 hours, the unit should be drained, sanitized and new car- tridge pack installed prior to use. -
Page 47: Troubleshooting
Troubleshooting Problem Possible Causes Solutions NANOpure DIamond completely No electrical power to NANOpure Ensure NANOpure DIamond power inactive (pump and display DIamond. cord is connected to a live power not operating.) source and completely plugged into electrical outlet as well as power entry module on the unit. - Page 48 Poor quality feed water. If a Barnstead ROpure is the feed water source, check that the membrane is functioning properly. If a Barnstead Still is the feed water source, ensure that the distillate temperature to the NANOpure DIamond does not exceed 40°C (104°F).
- Page 49 ROUBLESHOOTING Display reads, “Meter PC board communication error. Turn the NANOpure DIamond OFF Board Problem.” (I/O Switch) and restart the unit. System electronics failure. Replace the resistivity meter board mounted on the inside of the right door. Water is leaking between the Wing head screws are not Tighten wing head screws on unit tight enough.
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Page 50: Replacement Parts
(filters, resin cartridges, etc.) and other items of limited life (indicator lights, fuses, etc.) that you can expect to replace on a more or less random basis. Where practical, Barnstead|Thermolyne recommends the frequency of replacement, or provides information on life expectancy from which you may calculate a replacement interval compatible with your usage pattern. -
Page 51: Safety Stock
EPLACEMENT ARTS Safety Stock For critical applications where performance with minimum downtime is required, Barnstead|Thermolyne rec- ommends that you maintain a local stock of those parts listed in the General Maintenance Parts and Safety Stock sections. Description Catalog No. Recommended Quantity... -
Page 52: Flow Chart Operational Overview)
Flow Chart power switch turned on Barnstead /Thermolyne Vx.xx Style English Unit Initialization & Meter Calibration Check NANOpure DIamond (Idle) xx :xx :xx xx /xx /xx standby start_stop back key up or down enter key key pressed pressed keys pressed... -
Page 53: Wiring Diagram
120V: (2) FSX47 230V: (2) FSX54 NEUTRAL CHASSIS GND CHASSIS LINE REMOTE DISPLAY CONNECTOR (SPG) MODEL #s D11911 & D11931 ONLY DIAGRAM COMPONENT LIST MODEL NO. AND OUR PART NO.(s) REF. DESCRIPTION D11901 D11901 D11911 D11921 D11931 POWER ENTRY MODULE... -
Page 54: Ordering Procedures
If the dealer cannot handle your request, then contact our Customer Service Department at 319-556-2241 or 800-553-0039. Prior to returning any materials to Barnstead|Thermolyne Corp., please contact our Customer Service Department for a “Return Goods Authorization” number (RGA). -
Page 55: One Year Limited Warranty
(1) year, the parts necessary to remedy any such defect. The warranty period shall commence either six (6) months following the date the product is sold by Barnstead|Thermolyne or on the date it is purchased by the original retail consumer, whichever date occurs first. - Page 56 Barnstead|Thermolyne 2555 Kerper Blvd. 9001 P.O. Box 797 Dubuque, IA 52004-2241 REGISTERED Phone: 319-556-2241 800-553-0039 Fax: 319-589-0516 E-Mail Address: mkt@barnstead.com...
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what direction should the arrows be pointing up or down ( flow ) on the ultra filter.