Summary of Contents for Barnstead|Thermolyne D11911
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ARNSTEAD HERMOLYNE NANOpure DIamond ® ™ ultrapure water system Operation Manual Series 1191 Model No. Voltage D11911 100V - 240V LT1191X1 • 6/22/00...
Table of Contents Safety Information ......................................3 Alert Signals......................................3 Warnings ........................................3 Introduction ........................................5 General Usage......................................5 General Specifications ....................................6 Environmental Conditions ..................................7 Declaration of Conformity ..................................7 Unpacking ........................................8 Installation ........................................9 Choosing a Site ......................................9 Other Accessories ......................................10 UV Lamp Installation ....................................11 Bench Mounting ....................................12 Wall Mounting ......................................12 Installing the Control Panel in a Remote Location ..........................13 Water Connections ....................................14...
Care should be taken Note when installing, operating or servicing Barnstead Notes alert you to pertinent facts and products. The specific safety notes pertinent to this conditions.
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AFETY NFORMATION Avoid splashing disinfecting solutions on clothing or skin. Ensure all piping connections are tight to avoid chemical leakage. Ensure adequate ventilation. Carefully follow manufacturer’s safety instructions on labels of chemical containers and material safety data sheets. Depressurize system prior to removing the cartridge pack.
Introduction Congratulations on your purchase of a Barnstead| Thermolyne NANOpure DIamond UV ultrapure water sys- tem. This water purification system is designed to provide low TOC, high resistivity, reagent grade water that exceeds ASTM Type I, CAP and NCCLS Type I stan- dards.
Accuracy: ± 5% Repeatability: ± 3% Electrical Requirements The NANOpure DIamond UV is equipped with 2 power cords to be plugged into an electrical outlet of the appropriate voltage. Voltage and Frequency (Nominal) Model D11911 100-240 VAC, 47-63 Hz, 1 phase...
Altitude limit: 3,500 meters. Storage: -25°C to 65°C; 10% to 85% relative humidity. Declaration of Conformity Barnstead|Thermolyne hereby declares under its sole responsibility that this product conforms with the technical requirements of the following standards: EMC: EN 61000-3-2 Limits for Harmonic Current Emissions...
Unpacking Remove the unit from its shipping container. Remove all contents carefully. Ensure that the UV lamp, feed and drain tubing, sanitization cartridge, wall bracket, accessory parts bag and power cords (see list below) are re- moved from the packaging materials before discarding.
Installation Choosing a Site Caution The NANOpure DIamond UV features a removable con- Wall composition, condition and trol panel display which allows the system to be mounted construction as well as fastener type almost anywhere within the laboratory. Use the wall must be considered when mounting bracket for wall mounted systems as a template to drill this unit.
NSTALLATION Other Accessories Optional accessories for this unit include a float switch, low pressure switch, N.I.S.T. Traceable Calibration Module, remote dispenser, and printer. Installation proce- dures for these accessories are explained in later sec- tions of this manual.
NSTALLATION UV Lamp Installation Note Locate the UV chamber inside the left door of the The UV lamp contains mercury. If NANOpure DIamond UV. Install the UV Lamp as follows: broken or no longer needed, do not Disconnect the power cord from the unit. dispose of the UV lamp in the trash.
NSTALLATION Bench Mounting Caution Place the NANOpure DIamond UV on a bench Wall composition, condition and con- top that is accessible to pretreated water, elec- struction, as well as fastener type, tricity and an atmospherically vented drain. must be considered when mounting this unit.
NSTALLATION Installing the Control Panel in a Note The removable control panel was not Remote Location designed to be repeatedly removed For your convenience, the control panel can be removed from the unit, therefore, you may from the unit and mounted at a convenient location within experience difficulty when attempting 10 ft.
NSTALLATION Water Connections Feed Water Connection Caution Locate the length of 3/8” (.95 cm) O.D. tubing Do not connect feed water until direct- provided with the unit with a quick disconnect ed to do so during “Initial Sanitization.” insert on one end and a 3/8” (.95 cm) O.D. X 1/4”...
Please refer to “Installing the Control Panel in a Remote Location” in the “Installation” section of this manual for more information about how to remove the STANDBY control panel from the unit. START BACK ENTER STOP Barnstead DISPENSE NANOpure DIamond UV Control Panel...
ONTROLS Switches When the main power switch (on the lower back right side of the unit as you face the unit) is ON, the switches on the control panel function as follows: START/STOP allows you to alternate the unit between the normal (recirculation) mode;...
Initial Operation Cartridge packs will come bagged with four manifold connection caps. Part Application DIamond Kit Organic Free R/O & Distilled Feed D50280 Ultra-Low Organics, Type 1 Water, Reverse Osmosis or Distilled Water Feed Warning Allow cartridge pack to warm to room DIamond Kit Organic Free Deionized Feed temperature before installation.
NITIAL PERATION Initial Rinse Attach the feed water line to the unit by snapping the quick disconnect coupling into the quick disconnect body in the lower left back of the unit. Attach an atmospheric drain line [1/4” (.64 cm)] tubing by pushing it into the quick connect fitting on the lower left back of unit.
NITIAL PERATION System Sanitization Procedure Your NANOpure DIamond UV has been shipped with a Warning cleaning syringe (Cat. No. CMX25). When the system is Avoid splashing disinfecting solution new or whenever a new cartridge pack is installed, the on clothing or skin. system should be sanitized (cleaned).
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NITIAL PERATION and press ENTER. Display will now read, “Unit Sanitizing.” 14. Unit may now be left unattended until display reads, “Sanitization Complete: Press ENTER.” 15. After sanitization is complete the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculation mode.
Normal Operation Turn the system power ON by depressing the main power switch to the “I” position. The system greeting display indicates the type of unit you own. This greeting is “UV.” Note On initial start-up, the purity meter The system electronics will initialize and check may display “...MΩ-cm or uS/cm.”...
User Settings Adjusting Display Brightness From the (Idle) mode, when the display reads, “NANOpure Diamond (Idle) xx:xx:xx xx/xx/xx,” press the UP or DOWN arrow until display reads, “Advanced Menu?” Press ENTER. Press ENTER to proceed through the options until “Set Display Brightness” is displayed. Press the UP or DOWN arrow to choose “Yes.”...
ETTINGS Press ENTER. Press ENTER when the unit displays “Printer Attached?” When prompted with “Date Format” press the UP or DOWN arrow to show the date format desired. Press ENTER to select the desired for- mat and continue. When prompted with “Set Date,” press the UP or DOWN arrow to choose “Yes,”...
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ETTINGS Unlatch and open the right side door. Find and copy down the two cell constants attached to the gray cable, leaving the electron- ics board mounted on the inside of the right side door. Close and latch the right side door. Reconnect the power cord and turn unit ON.
ETTINGS Use of Standby Mode Note At the end of the work day, place the NANOpure When in Standby mode, press DIamond UV in Standby mode for the night. To place the START/STOP to continue normal unit in Standby mode: operation.
ETTINGS Press ENTER. Press BACK to return to the (Idle) mode. The second line of the display will show a “Below Set point” message once every 8 to 10 seconds when the measurement is below the set point. (The set point indica- tion is set at the factory at 10 MΩ-cm.) Resetting the Sanitization Timer From the (Idle) mode, when the display reads,...
ETTINGS Press the UP or DOWN arrow to select “Yes.” Press ENTER and the timer will be reset for approximately five months of operational time. Display will show, “Reset San Timer?” Press BACK twice to return to the (Idle) mode. Setting Volumetric Dispensing Note From the normal recirculating mode, when the...
ETTINGS Setting Timed Dispensing From the normal recirculating mode, when the dis- play is showing purity, press the UP or DOWN arrow until the display reads, “Auto Dispense Menu?” Press ENTER. Display will read, “Dispense Method.” Press the UP or DOWN arrow to select TIME. Press ENTER.
ETTINGS Press the UP or DOWN arrow to select “MΩ-cm” or “uS/cm” Press ENTER. Press BACK to return to the normal recirculating mode. Temperature Compensation Note (Factory set to “ON.”) Purity displayed will have an asterisk From the normal recirculating mode, when the (*) the the left of the reading (* xx.x display is showing purity, press the Up or MΩ-cm or * x.xx uS/cm) to inform the...
Installing Float or Pressure Switch Accessories D8964 (float switch) and D2706 (pressure switch) are designed to protect the NANOpure DIamond UV pump by alerting the system of an inadequate feed water condition so that the pump can be shut down. If an inadequate feed water condition exists and the pump is shut down due to this condition, the display will read “Check Inlet.”...
N.I.S.T Calibration Module Performing an Electronic Calibration Using the Optional N.I.S.T. Calibration Module If you purchased the optional N.I.S.T. calibration module (Catalog No. E896X5) you can perform a calibration of the NANOpure DIamond purity sensing electronics traceable to N.I.S.T. standards. Disconnect power cord from the unit.
N.I.S.T. C ALIBRATION ODULE 11. Press BACK to return to the (Idle) mode. 12. Turn the main power switch to the OFF “O” position. Unplug the unit. 13. Remove the calibration module and reconnect the cell. 14. Reattach the cover plate and close and latch the door.
Computer/Printer Setup Connecting NANOpure DIamond to Computer and Communicating Though the RS-232 Port Using Hyperterminal or Procomm Hyperterminal RS-232 Capture Instructions Connect the 9 pin serial cable (part no. WHX18) from the NANOpure DIamond RS-232 port to COM2: port or (COM1: port) on back of computer.
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OMPUTER RINTER ETUP capture text. Accepting default will put the file which you name in the c:/windows directory called capture.txt and the file will be an ASCII text file. 11. You should see the data on the computer screen. 12. When you are finished storing data from the NANOpure DIamond, save your file.
OMPUTER RINTER ETUP 12. Type in 21 <Enter>, sets to COM2: or (Type in 20 <Enter>, sets to COM1:), depending on your computer. 13. Type in 24 <Enter>, saves settings. 14. Type ESC to exit setup menu. 15. Procomm is now ready to accept input from the NANOpure DIamond.
OMPUTER RINTER ETUP From the “Printer Attached” display, press the Up or DOWN arrow for (YES). Press ENTER. Press BACK twice to return to the (Idle) mode. During normal Recirculation mode, a purity and temperature reading will be printed once every 12 minutes.
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OMPUTER RINTER ETUP down; or—the paper may be jammed in the printer. Turn the printer OFF before checking for jammed paper. Note Remove the paper jam and turn the printer back ON. If A colored stripe along the edge of the the printer still will not print, unplug it and refer servicing paper indicates that you are approach- to qualified personnel.
Maintenance and Servicing General Cleaning Instructions Warning Disconnect electrical service to the unit. Wipe exterior • Avoid splashing mild detergent surfaces with lightly dampened cloth containing mild soap or weak acid on clothing or solution. skin • Ensure all piping connections are tight to avoid chemical Cell Cleaning leakage...
AINTENANCE AND ERVICING System Sanitization Note After sanitization is complete (approximately 3.5 hours), The sanitization timer will display after place the unit into its normal (recirculation) mode to allow six months, reminding you to sanitize the system to recirculate overnight after cleaning. the unit.
AINTENANCE AND ERVICING 14. Unit may now be left unattended until the display reads, “Sanitization Complete: Press ENTER.” 15. After sanitization is complete and the user presses “ENTER” the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculating mode.
AINTENANCE AND ERVICING Cartridge Pack Replacement Warning The frequency with which you will need to clean your unit Depressurize system prior to removing and replace your cartridge pack is dependent on your cartridge pack. feed water’s characteristics, your purity requirements and your usage.
AINTENANCE AND ERVICING 0.2 Micron Filter Replacement Caution Replace the 0.2 micron final filter whenever any of the fol- Do not overtighten the 0.2 micron filter lowing conditions occur: every 30 days, the product water or use excessive force in seating it. flow rate is reduced or bacteria break through.
AINTENANCE AND ERVICING UV Lamp Replacement Warning The ultraviolet lamp requires changing every 5-6 months. This unit is equipped with an ultraviolet Lamp Life will vary according to the number of times the lamp. Ultraviolet radiation is harmful to NANOpure DIamond UV is turned on and off (the the eyes and skin.
AINTENANCE AND ERVICING Make sure the UV lamp cable is tucked behind the chamber before closing and relatching the door. Reconnect power cord and turn unit ON. Reset UV Timer according to “Resetting the UV Timer.” Operate normally. Warning Fuse Replacement Replace fuses with those of the same type and rating.
Troubleshooting Problem Possible Causes Solutions NANOpure DIamond completely No electrical power to NANOpure Ensure NANOpure DIamond power inactive (pump and display DIamond. cord is connected to a live power not operating.) source and completely plugged into electrical outlet as well as power entry module on the unit.
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Poor quality feed water. If a Barnstead ROpure is the feed water source, check that the membrane is functioning properly. If a Barnstead Still is the feed water source, ensure that the distillate temperature to the NANOpure DIamond does not exceed 40°C (104°F).
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ROUBLESHOOTING Display reads, “Meter PC board communication error. Turn the NANOpure DIamond OFF Board Problem.” (I/O Switch) and restart the unit. System electronics failure. Replace the resistivity meter board mounted on the inside of the right door. Water is leaking between the Wing head screws are not Tighten wing head screws on unit tight enough.
(filters, resin cartridges, etc.) and other items of limited life (indicator lights, fuses, etc.) that you can expect to replace on a more or less random basis. Where practical, Barnstead|Thermolyne recommends the frequency of replacement, or provides information on life expectancy from which you may calculate a replacement interval compatible with your usage pattern.
EPLACEMENT ARTS Safety Stock For critical applications where performance with minimum downtime is required, Barnstead|Thermolyne rec- ommends that you maintain a local stock of those parts listed in the General Maintenance Parts and Safety Stock sections. Description Catalog No. Recommended Quantity...
Flow Chart Operational Overview power switch turned on Barnstead /Thermolyne Vx.xx Style English Unit Initialization & Meter Calibration Check NANOpure DIamond (Idle) xx :xx :xx xx /xx /xx standby start_stop back key up or down enter key key pressed key pressed...
If the dealer cannot handle your request, then contact our Customer Service Department at 319-556-2241 or 800-553-0039. Prior to returning any materials to Barnstead|Thermolyne Corp., please contact our Customer Service Department for a “Return Goods Authorization” number (RGA).
(1) year, the parts necessary to remedy any such defect. The warranty period shall commence either six (6) months following the date the product is sold by Barnstead|Thermolyne or on the date it is purchased by the original retail consumer, whichever date occurs first.
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