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Endress+Hauser Analytik Jena ScanDrop2 Operating Manual
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Endress+Hauser Analytik Jena ScanDrop2 Operating Manual

Endress+Hauser Analytik Jena ScanDrop2 Operating Manual

Uv/vis spectrophotometer
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Operating Manual
ScanDrop
2
UV/Vis Spectrophotometer

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Summary of Contents for Endress+Hauser Analytik Jena ScanDrop2

  • Page 1 Operating Manual ScanDrop UV/Vis Spectrophotometer...
  • Page 2 Analytik Jena GmbH+Co. KG Manufacturer Konrad-Zuse-Str.1 07745 Jena  Germany Phone + 49 3641 77 70 + 49 3641 77 9279 Email info@analytik-jena.com Analytik Jena GmbH+Co. KG Service Konrad-Zuse-Str. 1 07745 Jena  Germany Phone + 49 3641 77 7407 Email service@analytik-jena.com For a proper and safe use of this product follow the instructions.
  • Page 3 ScanDrop Contents Contents Basic information ....................... 5 User manual notes ......................5 Intended use ........................6 Warranty and liability......................6 Safety instructions ...................... 7 General notes ........................7 Safety labeling on the ScanDrop ..................7 Requirements for the operating personnel ..............8 Safety instructions, transport and installation ..............
  • Page 4 Figures ScanDrop Figures Fig. 1 Front view of the ScanDrop ................11 Fig. 2 ScanDrop with opened cell compartment ............12 Fig. 3 ScanDrop with integrated control unit ............12 Fig. 4 CHIPCUVETTE ..................... 13 Fig. 5 CHIPCUVETTE, inserted into the adapter ............14 Fig.
  • Page 5 ScanDrop Basic information Basic information User manual notes The user manual informs about the design and function of the ScanDrop and provides Contents the necessary know-how for the safe handling of the device and its components. Fur- thermore, the user manual includes information on the maintenance and servicing of the device as well as hints on potential causes for malfunctions and their correction.
  • Page 6 Basic information ScanDrop Intended use The ScanDrop is a UV/Vis spectrophotometer that was specially designed for the analy- sis of microliter samples with a minimum sample volume of 0.3 µL and a maximum of 2 mL. The ScanDrop is a combined device that is capable of accepting different cell adapt- ers for measuring of up to 16 samples.
  • Page 7 ScanDrop Safety instructions Safety instructions General notes For your own safety and for a trouble-free operation carefully read this chapter before commissioning the ScanDrop Comply with all safety instructions in the manual and pay careful attention to all mes- sages and notes which are displayed on the screen by the control software. Also, observe the safety instructions for system components by other manufacturers supplied with this device (e.g.
  • Page 8 Safety instructions ScanDrop Warning symbol Meaning Remark Warning of Do not look directly or indirectly via a mirror UV radiation into the beams of the UV lamp. The lamp ra- diation can cause conjunctivitis! The device is designed in such a way as to prevent the customer from looking into the lamp radiation during measurements.
  • Page 9 ScanDrop Safety instructions  Caution when handling glass components (e.g. cells). Risk of broken glass and there- fore risk of injury!  The ventilation equipment on the device must be in good working condition. Covered ventilation grilles or slits etc. may cause the device to break down or may cause dam- age to it.
  • Page 10 Safety instructions ScanDrop  The operator is responsible for carrying out suitable decontamination should the de- vice be contaminated externally or internally with dangerous substances. For suitable disinfection agents and procedures see the chapter entitled "Maintenance and care". Other disinfection agents that are not included in the list may only be used after con- sultation with Analytik Jena.
  • Page 11 ScanDrop Function and setup Function and setup The ScanDrop The ScanDrop is a robust UV/Vis spectrophotometer that was specially designed for the The spectrophotometer analysis of microliter samples with a minimum sample volume of 0.3 µL and a maxi- mum of 2 mL. The ScanDrop can be used to measure absorption, transmission and en- ergy in the wavelength range from 190 nm to 1,000 nm.
  • Page 12 Function and setup ScanDrop center heights ranging from 8.5 to 15 mm. Thus the ScanDrop is ideally suited for the use of different cells. Magnetic carriage Dowel pin Fig. 2 ScanDrop with opened cell compartment The ScanDrop can optionally be supplied as a standalone system with an integrated The control unit control unit.
  • Page 13 ScanDrop Function and setup The software enables:  Quantitative analyses with three calibration models  Biochemical analyses  Analyses with freely programmable formulas  Cyclical or kinetic sample measurements  User administration with 3 authorization levels  Import and export of data via USB stick and bar code reader Cells and adapters The ScanDrop can accommodate different cells (with adapters) for multiple sample...
  • Page 14 Function and setup ScanDrop Fig. 5 CHIPCUVETTE, inserted into the adapter Analytik Jena offers a special measuring adapter for measuring with CHIPCUVETTE. Butterfly Cuvette 9 Measuring spaces Foldings wings Magnetic bar Distance piece (0.5 mm) Quartz glass Fig. 6 Butterfly Cuvette The Butterfly Cuvette was developed for measuring 6 samples with a volume of 2.0-4.0 µL and 3 references (in column 1).
  • Page 15 ScanDrop Function and setup Fig. 7 Beam path through the Butterfly Cuvette The cell is made of a composite of quartz glass and metal. It can be cleaned and reused, rendering the measurement free of expendable materials. An 8-cell changer capable of accepting up to 8 cells (10 mm) is also available for the 8-cell changer ScanDrop .
  • Page 16 Function and setup ScanDrop Connections and control elements The connections and control elements of the ScanDrop are easily accessible at the front face and on the rear of the device. Measuring position for one cell (10 mm rectangular or 16 mm round) Status LED Cell compartment for different measuring adapt-...
  • Page 17 ScanDrop Function and setup Fig. 10 Rear of the device with tablet Tablet Mains switch, Support bracket Fuse holder, USB port for PC Mains connection Type plate The tablet has its own on/off key. The two USB ports can be used for data transfer via The tablet USB stick or bar code reader.
  • Page 18 Function and setup ScanDrop Overview 1 Information on the type plate Manufacturer (with address) Analytik Jena GmbH+Co. KG, Konrad Zuse Str. 1, 07745 Jena, Germany, Made in Germany Device type and model ScanDrop Order number e.g. REF 844-00503-2 Serial number e.g.
  • Page 19 ScanDrop Installation and commissioning Installation and commissioning Site requirements The following requirements are placed on the climatic conditions in the operating room Installation conditions of the ScanDrop  Temperature range: +5 °C to +35 °C  Max. humidity: 80 % at 30 °C The operating room should have the characteristics of a biological-chemical laboratory.
  • Page 20 Installation and commissioning ScanDrop Installing ScanDrop ATTENTION Before connecting the ScanDrop and the PC to the mains verify that the operating volt- age specified on the type plates of the devices matches the mains voltage. Operation with a voltage other than the specified operating voltage can destroy the devices. 1.
  • Page 21 ScanDrop Installation and commissioning Switching off the ScanDrop CAUTION There is a slight risk of crushing when manually or automatically closing either of the two cell compartments! The sensor system of the ScanDrop notices if fingers or other objects are in the infeed area of the large cell compartment on the front.
  • Page 22 Installation and commissioning ScanDrop In the FlashSoftPro software, make preparations for an individual measurement or a Preparing for the measurement series. measurement 1. Via M  M , open the M EASUREMENT EASUREMENT PARAMETERS EASUREMENT PARAMETERS window. 2. On the T tab, define the name and storage location for the results file.
  • Page 23 ScanDrop Installation and commissioning remains open during the measurement. After the measurement, manually close the cover.  The cover of the measuring compartment for standard cells cannot be opened until after the ScanDrop has been initialized. The cover is locked, if a different cell or a different cell adapter was selected in the measuring parameters.
  • Page 24 Installation and commissioning ScanDrop Magnetic carriage Dowel pin Fig. 13 ScanDrop with opened cell compartment The magnet carriage transports the cell adapters into the interior of the device for measuring. Using the CHIPCUVETTE Fig. 14 Inserting the CHIPCUVETTE with the adapter 1.
  • Page 25 ScanDrop Installation and commissioning Using the Butterfly Cuvette Fig. 15 Inserting the Butterfly Cuvette ATTENTION Only use the Butterfly Cuvette supplied with the device. The device and the Butterfly Cu- vette are paired with each other for optimal measuring performance. Measuring spaces Reference Sample...
  • Page 26 Installation and commissioning ScanDrop When the magnet carriage is moved into the interior of the device, the wings of the But- terfly Cuvette are folded upwards by the two ramps in the cell compartment (see the ar- rows). Owing to the high surface tension of the solvent (water) there is no risk of the drop-shaped samples running into one another.
  • Page 27 ScanDrop Maintenance and care Maintenance and care WARNING Risk of electric shock! Do not touch! Before performing any cleaning work, switch off the ScanDrop (and the tablet) and dis- connect the mains plug. Do not recommission the ScanDrop again until it is completely dry.
  • Page 28 Maintenance and care ScanDrop We recommend the following disinfection agents for the device interior: Decosept AF by Dr Schuhmacher GmbH Meliseptol HBV cloths by B. Braun  These disinfection agents are only to be used for wiping disinfection, since liquid might enter through the ventilation slots into the sensitive electronics.
  • Page 29 ScanDrop Maintenance and care  After use and cleaning, put the cell back into the storage box (supplied) and close the box. Mounting and dismounting the tablet The ScanDrop can easily be converted from control via PC or laptop to standalone oper- ation via tablet, and vice versa.
  • Page 30 Maintenance and care ScanDrop Dismounting the tablet At the ScanDrop : Port for the tablet Fig. 19 Dismounting the tablet 1. Switch off both the ScanDrop and the tablet. 2. Remove the tablet with support bracket from the ScanDrop To do so, undo the four hexagon socket screws.
  • Page 31 ScanDrop Fault removal Fault removal The following chapter describes a number of possible problems that the user can par- tially remedy independently. Once the ScanDrop and the control unit have been switched on, system monitoring takes place. In the event of operator error or device fault, the software displays both an error code and the corresponding error message.
  • Page 32 Fault removal ScanDrop Software error Error code Error Lid open Cause Remedy Lid of the measuring compartment for Remove cell, close the lid. standard cells open Measurements in the large cell compartment on the front side cannot be started until the lid is closed.
  • Page 33 ScanDrop Fault removal Error code Error Invalid sample adapter Cause Remedy Cell and adapter do not match the software  Insert suitable cell and adapter in Scan- settings. Drop  Check software settings and change if re- quired Error code Error Door open during running operation Cause...
  • Page 34 Transport and storage ScanDrop Transport and storage Packaging the device for transport WARNING Risk of damage to health due to improper decontamination! Perform a professional and documented decontamination of the device before returning it to Analytik Jena (see documents in the project folder). Analytik Jena must refuse ac- ceptance of contaminated devices.
  • Page 35 ScanDrop Transport and storage 6. Place the ScanDrop inside a plastic bag to protect it against humidity and scratches. 7. Place the ScanDrop onto the mold insert in the cardboard box. 8. Insert the side mold inserts in the cardboard box. Insert the front and rear pins into the recesses on the bottom mold insert (see arrow).
  • Page 36 Transport and storage ScanDrop Storage ATTENTION Risk of device damage due to environmental conditions and condensation water. The device must only be stored in air-conditioned rooms. The atmosphere must be low in dust and free from aggressive vapors. If the device is not installed immediately after delivery or not required for prolonged pe- riods, it should be stored in its original packaging.
  • Page 37 ScanDrop Disposal Disposal The operator of the ScanDrop must dispose of the waste materials produced during measurements (sample materials) in accordance with the statutory and local regula- tions. At the end of its service life, the ScanDrop and all its electronic components must be disposed of as electronic waste in accordance with the applicable regulations.
  • Page 38 Specification ScanDrop Specification Technical data Optical system Spectrometer system Polychromator system with symmetrical Czerny-Turner Detector Linear CCD detector optimized for the UV/Vis range Sample position 2D scanning range for different center heights from 8.5 to 15 mm Light source Xenon flash lamp Technical specificationen Measurement modes Absorbance, transmittance, en-...
  • Page 39 ScanDrop Specification Electrical connection Elektrical requirements 80 V to 264 V/AC, 50 to 60 Hz Mains fuses 2 x T3,15 A / 250 V Power consumption Max. 30 W Noise emission/ Noise emission Max. 69 dB Environmental conditions Operating conditions 15 °C to 35 °C, relative humidity max.
  • Page 40 Specification ScanDrop Standards and directives The ScanDrop is classified as protection class I. Protection class and The casing is protection type IP 20. type of protection The ScanDrop complies with the safety standards Device safety  DIN EN 61010-1 (VDE 0411-1; IEC 61010-1) ...