Zeiss Supra 35 VP FEG Operating Instructions Manual

Zeiss Supra 35 VP FEG Operating Instructions
Pre-Start:
1. Microscope is On and Operational (Green light on front panel)
2. Sign into log book.
Startup:
1. Login to Zeiss Computer
2 Start S SEM U
MART
3. Login to software [User: Basic User
4. V : and G : are on
AC UN
5. <CTRL + G>, goto G
6. Toggle DataZone if not visible <CTRL + D>
7. Goto Windows Desktop, start RemCon32
8. In RemCon32, left-click C
Loading/Changing Samples:
1. Scope to High Vac mode (not VP - See "VP Mode" section to change).
2. Verify that V : and G
AC
3. Switch Signal-A to TV mode; Left-Click Signal-A select TV
4. Check sample/stage is clear of pole piece and BSD, lower stage (Z-control)
5. Withdraw EBSD detector if inserted (See EBSD Instructions)
6. Left-click V : indicator and click V
AC
7. When vented roll out chamber door
8. Using gloves and/or forceps, Remove/Load Samples
9. Close chamber door, watch TV-Chamber scope to check samples will clear pole piece and
detectors
10. Left-click V : indicator and click P
AC
11. Wait until V :
AC
General Operating Parameters:
InLens Detector
SE2 Detector
VPSE
BSD
XEDS
EBSD
November, 2007 - V 1.75
I Software
SER NTERFACE
Password: Zeiss]
and operational, and EHT: IS OFF
tab, record Extractor Current in Log book.
UN
ö O
P
OMM PEN
: are on and operational, and EHT: IS OFF
UN
(Check Vent gas cylinder is open)
ENT
UMP
WD 3mm optimal
WD 6-8mm optimal, and longer
WD: Shorter the better
Min. WD 4mm, shorter the better
WD 8.5 and No Tilt
70E tilt, shorter WD
WD: 8.5, 10, 11, 14.5mm
; minimize window, return to S
ORT
(Listen)
Zeiss Supra 35VP - November 2007 - Ver1.75
SEM
MART