Lovibond PM 600 Instruction Manual
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Lovibond PM 600 Instruction Manual

Lovibond PM 600 Instruction Manual

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Summary of Contents for Lovibond PM 600

  • Page 1 Photometer-System P 600 Instruction manual...
  • Page 3 Important steps before using the photometer Please carry out the following steps as described in the Instruction manual. Become familiar with your new pho- tometer before starting with the first tests: • Unpacking and inspection of delivery contents, see page 100. •...
  • Page 5 Wichtige Information Um die Qualität unserer Umwelt zu erhalten, beschützen und zu verbessern Entsorgung von elektronischen Geräten in der Europäischen Union Aufgrund der Europäischen Verordnung 2012/19/EU darf Ihr elektronisches Gerät nicht mit dem normalen Hausmüll entsorgt werden! Tintometer GmbH entsorgt ihr elektrisches Gerät auf eine professionelle und für die Umwelt verantwortungsvolle Weise.
  • Page 6 Información Importante Para preservar, proteger y mejorar la calidad del medio ambiente Eliminación de equipos eléctricos en la Unión Europea Con motivo de la Directiva Europea 2012/19/UE, ¡ningún instrumento eléctrico deberá eliminarse junto con los residuos domésticos diarios! Tintometer GmbH se encargará de dichos instrumentos eléctricos de una manera profesional y sin dañar el medio ambiente.
  • Page 7 Wichtiger Entsorgungshinweis zu Batterien und Akkus Jeder Verbraucher ist aufgrund der Batterieverordnung (Richtlinie 2006/66/ EG) gesetzlich zur Rückgabe aller ge- und verbrauchten Batterien bzw. Akkus verpflichtet. Die Entsorgung über den Hausmüll ist verboten. Da auch bei Produkten aus unserem Sortiment Batterien und Akkus im Lieferumgang enthalten sind, weisen wir Sie auf folgendes hin: Verbrauchte Batterien und Akkus gehören nicht in den Hausmüll, sondern können unentgeltlich bei den öffentlichen Sammelstellen Ihrer Gemeinde und überall...
  • Page 8 Indicación importante acerca de la eliminación de pilas y acumuladores Basado en la norma relativa a pilas/ baterías (directiva 2006/66/CE), cada consumidor, está obligado por ley, a la devolución de todas las pilas/ baterías y acumuladores usados y consumidos. Está prohibida la eliminación en la basura doméstica. Ya que en productos de nuestra gama, también se incluyen en el suministro pilas y acumuladores, le sugerimos lo siguiente: Las pilas y acumuladores usados no pertenecen a la basura doméstica, sino que pueden...

  • Page 9: Safety Precautions

    Be aware of the risks of using the required reagents by reading the MSDS (Material Safety Data Sheets). Failure could result in serious injury to the operator or damage to the instrument. MSDS: www.lovibond.com CAUTION The accuracy of the instrument is only valid if the instrument is used in an environment with controlled electromagnetic disturbances according to DIN 61326.

  • Page 10: Table Of Contents

    Table of contents Part 1 Methods ....................5 1.1 Table of Methods ..................... 6 Alkalinity-total (Alkalinity-m, m-Value) ................8 Alkalinity-total HR (Alkalinity-m HR, m-Value HR) ............10 Bromine .......................... 12 Chlorine .......................... 14 Chlorine with tablet ......................16 free Chlorine ....................... 16 total Chlorine ......................
  • Page 11 Part 2 Instrument Manual ................. 49 Operation ..................... 50 2.1.1 Set up ......................50 2.1.2 Saving data – Important Notes ............... 50 2.1.3 Replacement of batteries ................50 2.1.4 Instrument (explosion drawing) ..............51 Overview of function keys ................. 53 2.2.1 Overview ......................
  • Page 12 User method list ..................... 84 User Concentration Methods ................86 User Polynomials .................... 88 Delete User Methods ..................91 Print Data of User Methods ................92 Initialise User Method System ................. 93 2.4.8 Special functions .................... 94 Langelier Saturation Index ................94 2.4.9 Instrument basic settings 2 ................

  • Page 13: Part 1 Methods

    Part 1 Methods PM600_3h 02/2021...

  • Page 14: Table Of Methods

    1.1 Table of Methods No. Analysis Reagent Range Displayed Method OTZ Page [nm] 30 Alkalinity, total T tablet 5-200 mg/l CaCO Acid/Indicator 1,2,5 31 Alkalinity HR, tablet 5-500 mg/l CaCO Acid/Indicator 1,2,5 total T 80 Bromine T tablet 0.05-13 mg/l Br 100 Chlorine T * tablet 0.01-6...
  • Page 15 1.1 Methods The precision of Lovibond® Reagent Systems (tablets, powder packs and tube tests) is identical to the precision specified in standards literature such as American Standards (AWWA), ISO etc. Most of the data referred to in these standard methods relates to Standard Solutions. Therefore they are not readily applicable to drinking-, boiler- or waste-water, since various interferences can have a major influence on the accuracy of the method.

  • Page 16: Alkalinity-Total (Alkalinity-M, M-Value)

    1.1 Methods Alkalinity, total = Alkalinity-m = m-Value with Tablet 5 – 200 mg/l CaCO 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 17 1.1 Methods Notes: 1. The terms total Alkalinity, Alkalinity-m, m-Value and Alkalinity to pH 4.3 are identical. 2. For accurate results exactly 10 ml of water sample must be taken for the test. 3. Conversion table: Acid demand to pH 4.3 German English French...

  • Page 18: Alkalinity-Total Hr (Alkalinity-M Hr, M-Value Hr)

    1.1 Methods Alkalinity HR, total = Alkalinity-m HR = m-Value HR with Tablet 5 – 500 mg/l CaCO 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 19 1.1 Methods Notes: 1. For verification of the result look carefully at the bottom of the vial. If a thin yellow layer forms, then mix the vial again. This ensures that reaction is complete. Reread the result. 2. Conversion table: Acid demand to pH 4.3 German English...

  • Page 20: Bromine

    1.1 Methods Bromine with Tablet 0.05 – 13 mg/l Br 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 21 1.1 Methods Notes: 1. Vial cleaning: As many household cleaners (e.g. dishwasher detergent) contain reducing substances,the subsequent determination of Bromine may show lower results. To avoid any measurement errors, only use glassware free of Chlorine demand. Preparation: Put all applicable glassware into Sodium hypochlorite solution (0.1 g/l) forone hour, then rinse all glassware thoroughly with deionised water.

  • Page 22: Chlorine

    1.1 Methods Chlorine with Tablet 0.01 – 6 mg/l Cl Chlorine HR with Tablet 0.1 – 10 mg/l Cl Chlorine The following selection is shown in the display: >> diff free total for the differentiated determination of free, combined and >>...
  • Page 23 1.1 Methods Notes: 1. Vial cleaning: As many household cleaners (e.g. dishwasher detergent) contain reducing substances, the subsequent determination of Chlorine may show lower results. To avoid any measurement errors, only use glassware free of Chlorine demand. Preparation: Put all applicable glassware into Sodium hypochlorite solution (0.1 g/l) for one hour, then rinse all glassware thoroughly with deionised water.

  • Page 24: Chlorine With Tablet

    1.1 Methods Chlorine, free with Tablet 0.01 – 6 mg/l Cl 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.

  • Page 25: Total Chlorine

    1.1 Methods Chlorine, total with Tablet 0.01 – 6 mg/l Cl 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.

  • Page 26: Differentiated Determination (Free, Combined, Total)

    1.1 Methods Chlorine, differentiated determination with Tablet 0.01 – 6 mg/l Cl 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 27 1.1 Methods 13. Place the vial in the sample chamber making sure that marks are aligned. T1 accepted 14. Press TEST key. prepare T2 Wait for a reaction period of 2 minutes. press TEST Countdown 2:00 After the reaction period is finished the measurement starts automatically.

  • Page 28: Chlorine Hr With Tablet

    1.1 Methods Chlorine HR, free with Tablet 0.1 – 10 mg/l Cl 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.

  • Page 29: Total Chlorine

    1.1 Methods Chlorine HR, total with Tablet 0.1 – 10 mg/l Cl 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.

  • Page 30: Differentiated Determination (Free, Combined, Total)

    1.1 Methods Chlorine HR, differentiated determination with Tablet 0.1 – 10 mg/l Cl 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 31 1.1 Methods 12. Close the vial tightly with the cap and swirl several times until the tablet is dissolved. 13. Place the vial in the sample chamber making sure that marks are aligned. T1 accepted prepare T2 14. Press TEST key. press TEST Wait for a reaction period of 2 minutes.

  • Page 32: Copper With Tablet

    1.1 Methods Copper with Tablet 0.05 – 5 mg/l Cu Copper The following selection is shown in the display: >> diff free total for the differentiated determination of free, combined and >> diff total Copper. >> free for the determination of free Copper. for the determination of total Copper.

  • Page 33: Differentiated Determination (Free, Combined, Total)

    1.1 Methods Copper, differentiated determination with Tablet 0.05 – 5 mg/l Cu 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.

  • Page 34: Free Copper

    1.1 Methods Copper, free with Tablet 0.05 – 5 mg/l Cu 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.

  • Page 35: Total Copper

    1.1 Methods Copper, total with Tablet 0.05 – 5 mg/l Cu 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.

  • Page 36: Cya-Test (Cyanuric Acid)

    1.1 Methods CyA-TEST (Cyanuric acid) with Tablet 0 – 160 mg/l CyA 1. Fill a clean vial (24 mm Ø) with 5 ml of the water sample and 5 ml deionised water (Note 1), close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 37 1.1 Methods Notes: 1. Use deionised water or tap water free of Cyanuric acid. 2. If Cyanuric acid is present a cloudy solution will occur. Small single particles are not necessarily caused by Cyanuric acid. 3. Dissolve the tablet completely (therefore swirl the vial approx. 1 minute). Un-dissolved particles of the tablet can cause results that are too high.

  • Page 38: Hardness, Calcium With Calcio Tablet

    1.1 Methods Hardness, Calcium 2T with Tablet 0 – 500 mg/l CaCO 1. Fill a clean vial (24 mm Ø) with 10 ml of water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 39 1.1 Methods Notes: 1. To optimise the readings an optional batch related calibration can be performed using Mode 40, see page 76. 2. Strong alkaline or acidic water samples must be adjusted to a pH-value between pH 4 and 10 before the tablets are added (use 1 mol/l Hydrochloride acid resp. 1 mol/l Sodium hydroxide).

  • Page 40: Iron With Tablet

    1.1 Methods Iron (Note 1) with Tablet 0.02 – 1 mg/l Fe Determination of total dissolved Iron Fe and Fe *This information refers to analysis of the water sample without digestion. 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap.
  • Page 41 1.1 Methods Notes: Iron Determination dissolved and dissolved Iron undissolved Iron Filtration Digestion + Fe + Fe IRON LR IRON (II) LR method tablet tablet result A minus result B = Fe Digestion procedure for the determination of total dissolved and undissolved iron. 1.

  • Page 42: Ozone

    1.1 Methods Ozone with Tablet 0.02 – 2 mg/l O Ozon >> with Cl The following selection is shown in the display: without Cl >> with Cl for the determination of Ozone in the presence of Chlorine. >> without Cl for the determination of Ozone in the absence of Chlorine.
  • Page 43 1.1 Methods Notes: 1. Vial cleaning: As many household cleaners (e.g. dishwasher detergent) contain reducing substances, the subsequent determination of Ozone may show lower results. To avoid any measurement errors, only use glassware free of Chlorine demand. Preparation: Put all applicable glassware into Sodium hypochlorite solution (0.1 g/l) for one hour, then rinse all glassware thoroughly with deionised water.

  • Page 44: In Presence Of Chlorine

    1.1 Methods Ozone, in the presence of Chlorine with Tablet 0.02 – 2 mg/l O 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 45 1.1 Methods 13. Close the vial tightly with the cap and swirl several times until the tablet is dissolved. 14. Add one DPD No. 1 tablet and one DPD No. 3 tablet straight from the foil into the first cleaned vial and crush the tablets using a clean stirring rod.

  • Page 46: In Absence Of Chlorine

    1.1 Methods Ozone, in absence of Chlorine with Tablet 0.02 – 2 mg/l O 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 47 PM600_3h 02/2021...

  • Page 48: Phosphate, Ortho Lr With Tablet

    1.1 Methods Phosphate, ortho LR with Tablet 0.05 – 4 mg/l PO 1. Fill a clean vial (24 mm ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that the marks aligned.
  • Page 49 1.1 Methods Notes 1. Only ortho-Phosphate ions PO react. 2. The tablets must be added in the correct sequence. 3. The test sample should have a pH-value between 6 and 7. 4. Interferences: Higher concentrations of Cu, Ni, Cr (III), V (V) and W (VI) interfere due to their colour. Silicates do not interfere (masked by Citric acid in the tablets).

  • Page 50: Ph Value With Tablet

    1.1 Methods pH value 6.5 – 8.4 with Tablet 1. Fill a clean vial (24 mm Ø) with 10 ml of the water sample, close tightly with the cap. 2. Place the vial in the sample chamber making sure that marks are aligned.
  • Page 51 1.1 Methods Notes: 1. For photometric determination of pH-values only use PHENOL RED tablets in black printed foil pack and marked with PHOTOMETER. 2. Water samples with low values of Alkalinity-m (below 35 mg/l CaCO ) may give wrong pH readings. 3.

  • Page 52: Sodium Hypochlorite

    1.1 Methods Sodium hypochlorite (Soda bleaching lye) with Tablet 0.2 – 16 % w/w NaOCl Preparation: 1. Fill a 5 ml plastic syringe with the test solution, ensuring that all air bubbles are expelled. Transfer the 5 ml test solution slowly into a 100 ml beaker and dilute to the 100 ml mark with chlorine-free water.
  • Page 53 1.1 Methods 8. Place the vial in the sample chamber making sure that marks are aligned. Zero accepted prepare Test 9. Press TEST key. press TEST The result is shown in the display in % w/w as availa- ble chlorine present in the original sample of Sodium hypochlorite.

  • Page 54: Important Notes

    1.2 Important notes 1.2.1 Correct use of reagents The reagents must be added in the correct sequence. Tablet reagents: The tablet reagents should be added to the water sample straight from the foil without touching them with the fingers. 1.2.2 Cleaning of vials and accessories for analysis Vials, caps and stirring rods should be cleaned thoroughly after each analysis to prevent interferences.
  • Page 55 Correct position of the vial (Ø 24 mm): Correct filling of the vial: PM600_3h 02/2021...

  • Page 56: Sample Dilution Techniques

    1.2.4 Sample dilution techniques Proceed as follows for accurate dilutions: Pipette the water sample (see table) into a 100 ml volumetric flask and fill up to 100 ml mark with deionised water. Swirl to mix the contents. Water sample Multiplication [ml] factor Pipette the required volume of the diluted sample into the vial and proceed as described in...

  • Page 57: Part 2 Instrument Manual

    Part 2 Instrument Manual PM600_3h 02/2021...

  • Page 58: Operation

    2.1 Operation 2.1.1 Set up Before working with the photometer insert the batteries (delivery contents). See chapter 2.1.2 Saving data – Important Notes, 2.1.3 Replacement of batteries. Before using the photometer perform the following settings in the Mode-Menu: • MODE 10: select language •...

  • Page 59: Instrument (Explosion Drawing)

    2.1.4 Instrument (explosion drawing): (A) screws (B) battery compartment cover (C) notch (D) batteries: 4 batteries (AA/LR6) (E) seal ring (F) instrument back (B) battery compartment cover (E) seal ring (F) instrument back (A) screws (C) notch (D) batteries CAUTION: To ensure that the instrument is water proof: seal ring (E) must be in position •...
  • Page 60 PM600_3h 02/2021...

  • Page 61: Overview Of Function Keys

    2.2 Overview of function keys 2.2.1 Overview Switching the photometer on or off Press shift key to achieve figures key 0-9. Keep the shift key depressed and press desired figures key. Shift e.g.: [Shift] + [1][1] Returning to selection of methods or previous menu Function key: description in the text if key available Function key: description in the text if key available Function key: description in the text if key available...

  • Page 62: Displaying Time And Date

    2.2.2 Displaying time and date: Press [“clock”] key. 19:30:22 2013-06-15 The display shows: After 15 seconds the photometer reverts to the previous display automatically or press [ ] key or [ESC]. 2.2.3 User countdown With this function the operator is able to define his own countdown. Press [“clock”] key.

  • Page 63: Operation Mode

    2.3 Operation mode Switch the photometer on by pressing the [ON/OFF] key. selftest ... The photometer performs an electronic self-test. 2.3.1 Automatic switch off The instrument switches off automatically after 20 minutes. This is indicated 30 seconds before by a beeper. Press any key to avoid the instrument switching off. As long as the instrument is working (for example countdown or printing) the automatic switch off is inactive.

  • Page 64: Chemical Species Information

    2.3.2.2 Chemical Species Information Pressing the [F2] key the display shows a list with available chemical species and corresponding ranges. Changing chemical species see chapter 2.3.7 page 58. 319 Phosphate LR T Line 1: Method number, Method name 0.05-4 mg/l PO Line 2: Range with chemical species 1 0.02-1.3 mg/l P Line 3: Range with chemical species 2...

  • Page 65: Performing Tests

    2.3.5 Performing Tests When zero calibration is complete, remove the vial from the sample chamber and perform the tests as described under “Method“. When the results have been displayed: - with some methods you can change between different chemical species - you can store and/or print out the results - perform further analysis with the same zero - select a new method...

  • Page 66: Changing Chemical Species

    2.3.7 Changing chemical species For some methods there is a possibility to change the chemical species of the test result. If the test result is displayed press arrow key [ ] or [ ]. Example: 319 Phosphate LR T -----[ ]----> 319 Phosphate LR T <---- [ ] ----- 319 Phosphate LR T 0.05-4 mg/l PO 0.02-1.3 mg/l P...

  • Page 67: Printing Results (Infra-Red Interface Module) (Optional)

    Note: The display shows the number of free data sets. Storage: 900 free records left If there are less than 30 data sets free the display shows: Storage: only 29 free records left Clear the memory as soon as possible (see “Deleting stored results”).

  • Page 68: Selecting A New Method

    2.3.11 Selecting a new method Press [ESC] key to return to method selection. Or enter the required method number directly, e.g. [Shift] + [1][6][0] for CyA-TEST (Cyanuric acid). Confirm with [ ] key. 2.3.12 Measure absorbance Range: –2600 mAbs to +2600 mAbs Method-No.

  • Page 69: Photometer Settings: Table Of Mode Functions

    2.4 Photometer settings: Table of Mode Functions MODE-Function No. Description Page Calibration Special method calibration Clear calibration Deleting user calibration Clock Setting date and time Countdown Switching the countdown on/off to ensure reaction times Delete data Deleting all stored results Key beep Switching the acoustic signal on/off to indicate key- pressing...

  • Page 70: Blank Because Of Technical Requirements

    MODE-Function No. Description Page Temperature Selection of °C or °F for Langelier Mode 70 User calibration Storage of user calibration User concentration Entering the data necessary to run a user concentration method User polynoms Entering the data necessary to run a user polynomial User methods clear Delete all data of a user polynomial or of a concentration method...

  • Page 71: Setting Date And Time

    Key beep Press [MODE], [Shift] + [1][1] keys. Mode Confirm with [ ] key. The display shows: <Key-Beep> ON: 1 OFF: 0 • Press [Shift] + [0] keys to switch the key beep off. • Press [Shift] + [1] keys to switch the key beep on. Confirm with [ ] key.
  • Page 72 Countdown (Ensuring reaction periods) Some methods require a reaction period. This reaction period is incorporated in the method as standard with the countdown function. It is possible to switch the countdown off for all methods: Press [MODE], [Shift] + [1][3] keys. Mode Confirm with [ ] key.
  • Page 73 Signal beep Performing a zero or a measurement takes 8 seconds. The photometer indicates the end of zeroing or measuring by a short beep. Press [MODE], [Shift] + [1][4] keys. Mode Confirm with [ ] key. <Signal-Beep> The display shows: ON: 1 OFF: 0 •...

  • Page 74: Printing Of Stored Results

    2.4.3 Printing of stored results Printing all results Press [MODE], [Shift] + [2][0] keys. Mode Confirm with [ ] key. <Print> The display shows: Print all Data Start: cancel: Press [ ] key for printing out all stored test results. Test No.: The display shows e.g.: After printing the photometer goes back to <Mode-Menu>...
  • Page 75 Printing results of a selected time period Press [MODE], [Shift] + [2][1] keys. Mode Confirm with [ ] key. The display shows: <Print> sorted: date from yy-mm-dd Enter year, month and day for the first day of the required __-__-__ period, e.g.: 14 May 2013 = [Shift] + [1][3][0][5][1][4] Confirm with [ ] key.
  • Page 76 Printing results of a selected Code No. range Press [MODE], [Shift] + [2][2] keys. Mode Confirm with [ ] key. <Print> The display shows: sorted: Code-No. Enter numeric code number (up to 6 places) for the first from _ _ _ _ _ _ required Code No., e.g.: [Shift] + [1].
  • Page 77 Printing results of one selected method Press [MODE], [Shift] + [2][3] keys. Mode Confirm with [ ] key. The display shows: <Print> >>20 Acid demand 30 Alkalinity-tot Select the required method from the displayed list or enter 40 Aluminium T the method-number directly.

  • Page 78: Printing Parameter

    Printing Parameter Press [MODE], [Shift] + [2][9] keys. Mode Confirm with [ ] key. <printing parameter> The display shows: 2: Baud rate cancel: Press [Shift] + [2] keys to select ”Baud rate”. The display shows: <Baud rate> is: 19200 select: [ ] [ ] save: cancel:...

  • Page 79: Recall / Delete Stored Results

    2.4.4 Recall / delete stored results Recall all stored results Press [MODE], [Shift] + [3][0] keys. Mode Confirm with [ ] key. The display shows: <Storage> display all data Start: cancel: The stored data sets are displayed in chronological order, print: starting with the latest stored test result.
  • Page 80 Recall results of a selected time period Press [MODE], [Shift] + [3][1] keys. Mode Confirm with [ ] key. The display shows: <Storage> sorted: date from yy-mm-dd Enter year, month and day for the first day of the required __-__-__ period, e.g.: 14 May 2013 = [Shift] + [1][3][0][5][1][4] Confirm with [ ] key.
  • Page 81 Recall results of a selected Code No. range Press [MODE], [Shift] + [3][2] keys. Mode Confirm with [ ] key. <Storage> The display shows: sorted: Code-No. from _ _ _ _ _ _ Enter numeric code number (up to 6 places) for the first required Code No., e.g.: [Shift] + [1].
  • Page 82 Recall results of one selected method Press [MODE], [Shift] + [3][3] keys. Mode Confirm with [ ] key. <Storage> The display shows: >>20 Acid demand 30 Alkalinity-tot Select the required method from the displayed list or enter 40 Aluminium T the method number directly.
  • Page 83 Delete stored results Press [MODE], [Shift] + [3][4] keys. Mode Confirm with [ ] key. <Delete data> The display shows: Delete all data? YES : 1 NO : 0 • Press [Shift] + [0] keys to retain the data sets in me- mory.

  • Page 84: Calibration

    2.4.5 Calibration Calcium Hardness Method 191 – Calibration of a method blank Press [MODE], [Shift] + [4] [0] keys. Mode Confirm with [ ] key. <Calibration> 1: M191 Ca-Hardness 2 The display shows: 2: M191 0 Jus. Reset 3: M170 Fluoride L Press [Shift] + [1] keys.
  • Page 85 After the reaction period is finished proceed as follows: 9. Rinse the vial (24 mm Ø) with the coloured sample from the beaker and fill with 10 ml of the sample. prepare TEST 10. Press TEST key. press TEST stored The batch related method blank is saved.

  • Page 86: User Calibration

    User Calibration If a test method is user calibrated the method name is displayed inverse. Procedure: • Prepare a standard of known concentration and use this standard instead of the sample according to the test procedure. • It is recommend to use well known standards which are formulated according to DIN EN, ASTM or other international norms or to use certified standards which are commercially available.
  • Page 87 Table Method Recommended range for user calibration Alkalinity-total 50 – 150 mg/l CaCO Alkalinity-total HR T 50 – 300 mg/l CaCO Bromine Calibration with basic test 100 Chlorine free Chlorine T 0.5 – 1.5 mg/l Cl Chlorine HR T 0.5–6 mg/l Cl Copper T 0.5 –...

  • Page 88: Store User Calibration

    Store user calibration Perform the required method as described in the manual 100 Chlorine T using a standard of known concentration instead of the 0.02-6 mg/l Cl2 water sample. 0.90 mg/l free Cl2 If the test result is displayed press [MODE], [Shift] + [4] [5] Mode keys and confirm with [ ] key.

  • Page 89: Delete User Calibration

    Delete user calibration This chapter only applies for methods which can be user calibrated. Select the required method. Chlorine T 0.02-6 mg/l Cl2 prepare ZERO Instead of zeroing the instrument press [MODE], [Shift] + press ZERO [4][6] keys and confirm with [ ] key. Mode <user calibration>...

  • Page 90: Lab Function

    2.4.6 Lab function Reduced operator guidance => “Profi-Mode“ This function may be used for routine analyses with many samples of one method. The following information is always stored in the methods: a) Method b) Range c) Date and time d) Differentiation of results e) Detailed operator instruction Compliance with reaction periods If the Profi-Mode is active, the photometer provides only a minimum of operator instructions.

  • Page 91: One Time Zero

    One Time Zero (OTZ) OneTimeZero is available for all methods where Zero is performed in a 24 mm Ø round vial with sample water (see chapter 1.1 Table of Methods). OneTimeZero can be used for different tests providing the tests are performed with the same sample water and under the same test conditions.

  • Page 92: User Operations

    2.4.7 User operations User method list After switching on the instrument a scroll list of all available methods is automatically shown in the display. To shorten this list according to the requirements of the user it is possible to create a user defined scroll list. The program structure requires that this list must have at least one active (switched on) method.
  • Page 93 User method list, switch all methods on This mode function activates all methods. After switching on the instrument a scroll list of all available methods is automatically shown in the display. Press [MODE], [Shift] + [6][1] keys. Mode Confirm with [ ] key. <Mlist all on>...

  • Page 94: User Concentration Methods

    User Concentration Methods It is possible to enter and store up to 10 User Concentration Methods. Therefor you need 2 to 14 standards of known concentration and one blank (deionised water or reagent blank value). The Standards should be measured with increasing concentrations and from the brightest to the darkest colouration.
  • Page 95 Press the appropriate numerical key to select the required choose resolution resolution, e.g.: [Shift] + [3] for 0.01. 1: 1 2: 0.1 Note: 3: 0.01 Please enter the required resolution according to the in- 4: 0.001 strument pre-sets: range max. resolutions 0.000 ...9.999 0.001 10.00 ...99.99...

  • Page 96: User Polynomials

    Prepare the second standard and press [Test] key. S2: 0.10 mg/l prepare The display shows the input value and the measured absorp- press TEST tion value. Confirm with [ ] key. S2: 0.10 mg/l Note: mAbs: • Perform as described above to measure further stan- dards.
  • Page 97 Confirm with [ ] key. Note: Overwrite polynom? if the entered number has already been used to save a YES: 1, NO: 0 polynomial the display shows the query: • Press [Shift] + [0] or [ESC] keys to go back to method no. query.
  • Page 98 Press [ ] or [ ] keys to select the required unit. choose unit: >> mg/l mmol/l mAbs µg/l Confirm with [ ] key. choose resolution Press the appropriate numerical key to select the required 1: 1 resolution, e.g.: [Shift] + [3] for 0.01. 2: 0.1 3: 0.01 Note:...

  • Page 99: Delete User Methods

    Delete User Methods (Polynomial or Concentration) In principle a valid user method can be overwritten. An existing user method (Polynomial or Concentration) can be totally deleted as well and is removed out of the method selection list: Press [MODE], [Shift] + [6][6] keys. Mode Confirm with [ ] key.

  • Page 100: Print Data Of User Methods

    Print Data of User Methods (Polynomials & Concentration) With this Mode function all data (e.g. wavelength, unit ...) of stored user polynomials and concentration methods can be printed out or transferred with HyperTerminal to a PC. Press [MODE], [Shift] + [6][7] keys. Mode Confirm with [ ] key.

  • Page 101: Initialise User Method System

    Initialise User Method System (Polynomials & Concentration) Power loss will cause incoherent data. The user method system must be initialised with this mode function to set it to a predefined state. ATTENTION: All stored user methods (polynomial & concentration) are deleted with initialisation. Press [MODE], [Shift] + [6][9] keys.

  • Page 102: Special Functions

    2.4.8 Special functions Langelier Saturation Index (Water Balance) For calculation the following tests are required: • pH-value • Temperature • Calcium hardness • Total Alkalinity • TDS (Total Dissolved Solids) Run each test separately and note the results. Calculate the Langelier Saturation Index as described: Calculation of Langelier Saturation Index With Mode 71 (see below) it is possible to select between degree Celsius or degree Fahrenheit.

  • Page 103: Selection Of Temperature Unit

    pH value The display shows: 0<=pH<=12 +_ _ _ _ Enter the pH-value in the range between 0 and 12 and confirm with [ ] key. <Langelier> Langelier The display shows the Langelier Saturation Index. saturation index 0.00 Press [ ] key to start new calculation. Return to mode menu by pressing [ESC] key.

  • Page 104: Instrument Basic Settings 2

    2.4.9 Instrument basic settings 2 Adjusting display contrast Press [MODE], [Shift] + [8][0] keys. Mode Confirm with [ ] key. <LCD contrast> The display shows: • Press arrow key [ ] to increase contrast of the LCD display about one unit. •...

  • Page 105: Instrument Special Functions /Service

    Press [Store] key to increase brightness of the display about Store ten units. Press [Test] key to decrease brightness of the display about Test ten units. 0...254 : 200 The display shows: The brightness can be selected between 0 and 254 units, e.g.: 200.

  • Page 106: Data Transfer

    2.5 Data transfer To print data or to transmit to a PC the optional IRiM (Infra-Red Interface Module) is required. 2.5.1 Data Printing Besides the IRiM module the following printer is required to print data directly using the USB Interface of the module: HP Deskjet 6940. 2.5.2 Data transfer to a personal computer Besides the IRiM a transfer program, is required to transmit test results.

  • Page 107: Part 3 Enclosure

    Part 3 Enclosure PM600_3h 02/2021...

  • Page 108: Unpacking

    3.1 Unpacking Carefully inspect all items to ensure that every part of the list below is present and no visible damage has occurred during shipment. If there is any damage or something is missing, please contact your local distributor immediately. 3.2 Delivery contents Standard contents for PM600: 1 Photometer in plastic case...

  • Page 109: Technical Data

    3.4 Technical data Display Graphic Display Serial Interface IR interface for data transfer RJ45 connector for internet updates (see chapter 2.5.3) Light source light-emitting diode – photosensor – pair arrangement in a transparent measurement chamber Wavelength ranges: 1 = 530 nm IF = 5 nm 2 = 560 nm IF = 5 nm...

  • Page 110: Abbreviations

    3.5 Abbreviations Abbreviation Definition °C degree Celsius (Centigrade) °F degree Fahrenheit °F = (°C x 1.8) + 32 °dH degree German Hardness °fH degree French hardness °eH degree English Hardness °aH degree American Hardness Absorption unit ( = Extinction E) 1000 mAbs = 1 Abs = 1 A = μg/l...

  • Page 111: Troubleshooting

    3.6 Troubleshooting 3.6.1 Operating messages in the display / error display Display Possible Causes Elimination Overrange reading is exceeding the range if possible dilute sample or use other measuring range water sample is too cloudy filtrate water sample too much light on the photo cell seal on the cap? Repeat measurement with seal on the cap of the vial.
  • Page 112 Display Possible Causes Elimination The calculation of a value Test procedure correct? (e.g. combined Chlorine) is If not – repeat test not possible Example 1: Example 1 The readings for free and total 0,60 mg/l free Cl Chlorine are different, but comb Cl considering the tolerances of 0,59 mg/l total Cl...

  • Page 113: General

    3.6.2 General Finding Possible Causes Elimination Test result deviates from Chemical species not as Press arrow keys to select the the expected. required. required chemical species. No differentiation: Profi-Mode is switched on. Switch Profi-Mode off with e.g. for the Chlorine test Mode 50.

  • Page 114: Declaration Of Ce-Conformity

    Für das nachfolgend bezeichnete Erzeugnis / For the following mentioned product Bezeichnung / Name, MD 600 AL 400 PM 600 PM620 , 214020, 4214020, 214060, 214065 Modellnummer / Model No. wird hiermit erklärt, dass es den grundlegenden Anforderungen entspricht, die in den nachfolgend bezeichneten Harmonisierungsrechtsvorschriften festgelegt sind: / it is hereby declared that it complies with the essential requirements which are determined in the following harmonisation rules: Richtlinie 2014/30/EU des Europäischen Parlaments und des Rates vom 26.
  • Page 115 PM600_3h 02/2021...
  • Page 116 Tintometer GmbH The Tintometer Limited Tintometer Inc. Tintometer Spain Lovibond Water Testing Lovibond House 6456 Parkland Drive Postbox: 24047 ® Schleefstraße 8-12 Sun Rise Way Sarasota, FL 34243 08080 Barcelona 44287 Dortmund Amesbury, SP4 7GR Tel: 941.756.6410 Tel.: +34 661 606 770 Tel.: +49 (0)231/94510-0...

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