Total Sulfur & Hydrogen Control ____________________________________________________________ 10 4.2.1 331S/330S TS Only ____________________________________________________________________ 10 4.2.2 330S/331S H2S & TS with Mode Switching __________________________________________________ 10 4.2.3 330SDS/331SDS H2S & TS with Hydrogen Saver _____________________________________________ 11 Calibration _____________________________________________________________________________ 11 Appendix A – Drawings & Diagrams _______________________________________________________ 12 330SDS with H2 Saver and H2 Pressure Switch Outline &...
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Contact Us ____________________________________________________________________________ 23...
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List of Figures Figure 1: Total Sulfur Oven Cutaway __________________________________________________________________ 5 Figure 2: High Temperature O-Rings and Ultra Torr Elbow/Fittings __________________________________________ 8 List of Tables Table 1: Estimated Hydrogen Bottle Life in Days ........................6 Table 2: Spare Parts ................................19 Table 3: Hydrogen Sulfide Properties ..........................
The Total Sulfur User’s Manual should be used in conjunction with the Hydrogen Sulfide Analyzer Model 330S & 331S User’s Manual. It provides a comprehensive overview of Envent Engineering’s total sulfur addition to the H2S analyzers, along with detailed installation and startup instructions.
Envent anticipates producing the current configuration(s) of the H2S analyzers for a minimum of 3 years. Envent aims to support any products for 10 years from the time of purchase. This timeline may be subject to change depending on component availability from our vendors. Envent reserves the...
Envent Engineering Ltd is not responsible for any injury or property damage caused by improper use of the equipment. Once in the field, the user is solely responsible for the safe operation of the equipment.
H2S. The total sulfur option involves the addition of a total sulfur reaction furnace (pyrolysis furnace) to a Model 330S or 331S. The furnace converts all sulfur compounds into H2S, allowing the H2S analyzer to read total sulfur as per the ASTM D 4468-85 “Standard Test Method for Total Sulfur in Gaseous Fuels by Hydrogenolysis and Rateometric Colorimetry”.
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 Total Sulfur Reaction Furnace The Total Sulfur option comes standard with furnace temperature control circuitry. It also consists of a reaction oven, flame arrestors, hydrogen and sample flow meters, and an optional 3-way solenoid valve to allow the user to measure both H2S and total sulfur on an alternating basis, or the use of an SDS to measure TS consistency.
Our calculations are based on a 200 cm /min (flow of 2 on a A- 157-1 flow meter). Assuming each analysis will run 3 times every six hours, Envent suggests the bottle should be checked at least 10 days prior to the estimated end of life.
Upon arrival, the packaging should be immediately inspected for any external damage that may have occurred during shipping. If any damage is present, please contact Envent Engineering Ltd and request that the carrier's agent be present when the analyzer is unpacked. If a disagreement arises, the incoterms agreed to by the seller and the customer will overrule any dispute.
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 Installation or Replacement of Combustion Tube Use TS furnace exploded view drawing in Appendix A to refer to appropriate parts coinciding with the following steps. Step 1 Turn off the total sulfur furnace and let it cool for a minimum of an hour.
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 Step 6 Perform leak check of the total sulfur furnace as per steps in 3.2.2. 3.2.1 Connecting Vacuum Fitting to Quartz Tube Step 1 With the quartz tube inside of the ceramic furnace, slide the Ultra Torr nut, ferrule, and high temperature O-ring over the end of quartz tube.
The Process Flow Diagrams in Appendix A illustrate the typical sample conditioning system used for the 330S & 331S Total Sulfur Analyzers. The Total Sulfur analyzer includes a reaction furnace and an additional flowmeter to control hydrogen flow, which are integrated into the standard H2S analyzer sample conditioning system.
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 330S/331S H2S & TS with Mode Switching and Hydrogen Saver A second solenoid may be added to shut off the hydrogen gas when in H2S mode. This configuration saves hydrogen usage by a large margin (see table 1). The analyzer is typically programmed to run every 6 hours or alternate between H2S mode and TS mode each analysis;...
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 330SDS with H2 Saver and H2 Pressure Switch Process Flow Diagram 331S Total Sulfur Process Flow Diagram...
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 APPENDIX B – RECOMMENDED SPARE PARTS LIST The spare parts table provided below offers a comprehensive list of all the Total Sulfur analyzer spare parts. To determine which spare parts are applicable to your specific requirements, please consult an Envent sales representative for further assistance.
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 APPENDIX C – RISKS & SAFETY INFORMATION Hydrogen Sulfide Properties Properties Description Physical State Gaseous above 60˚C Color Colorless - No visible sign of H2S to warn you of its presence ...
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 Hydrogen Sulfide Quantities and Health Effects Possible health Effects Exposure Less than You can smell it. 1ppm 10 ppm No known health effects for most people. For 10 ppm or less, the exposure limit is 8 hours - Check your local ...
Envent Engineering Ltd – Total Sulfur User’s Manual – Revision 4.0 APPENDIX D – FAQ & TROUBLESHOOTING Question Answer What is the oven internal temperature? ~1000 What is the oven external enclosure surface temperature? Can we read furnace temperature on the display?
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CONTACT US In the event that a situation arises that is not covered by this manual, we encourage you to contact us so that we can help you resolve any issues you may have. Please have this manual readily available when calling for assistance.
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Mexico Tel: +52 (833) 247 8260 Avenida Revolución No. 1267, Piso 19, Col. Los Alpes. Álvaro Obregón Email: international@enventengineering.com 01040 Ciudad de México, México International Sales Tel: +1 (877) 365 8408 Email: international@enventengineering.com...
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