EYELA FDS-1000 Instruction Manual
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EYELA FDS-1000 Instruction Manual

Freeze dryer 230v
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R00
Freeze dryer
取扱説明書
Instruction Manual
Model FDS-1000
（230V）
This instruction manual is designed to use the product safely with keeping its best
performance.
Be sure to read "Safety precautions" before use.
IMPORTANT
Please keep this manual in a place easily accessible to every users.
Tokyo Rikakikai Co., Ltd.

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  • Page 1 Freeze dryer 取扱説明書 Instruction Manual Model FDS-1000 （230V） This instruction manual is designed to use the product safely with keeping its best performance. Be sure to read “Safety precautions” before use. IMPORTANT Please keep this manual in a place easily accessible to every users.
  • Page 3 IMPORTANT SAFETY INFORMATION 1. Warning signal word To ensure the safety, this manual defines the Attempting to carelessly operate the product or to touch the portion not-specified may result in information on such matters as requiring particular unexpected injury. care in the safety as follows in terms of the importance and risk and attaches the alert mark and Most of such accidents can be prevented if such signal word.

  • Page 4: Table Of Contents

    Thank you for purchasing our product. Introduction This instruction manual explains installation, operation, troubleshooting, maintenance and inspection, and discarding procedures for the Freeze dryer FDS-1000. Always read this manual before use to ensure familiarization of the product. Contents 5. Operation 1 For safe operations 5 - 1 Preparation 2.

  • Page 5: For Safe Operations

    1 For safe operations This product is not explosion-proof. Be sure to take extreme care for safety during operation. Take utmost care when drying the sample containing flammable substances, such as organic solvent, etc Be very careful when drying flammable substances, such organic Warning solvent, etc.

  • Page 6: Product Outline

    An electric shock or a malfunction may result if the product is modified or used for any purposes other than that specified. 2-2 Specification Product name Freeze dryer Model FDS-1000 Cooling method Can body cooling Trap cooling temperature ※1 -80℃ Dehumidification rate 150mL/one batch...

  • Page 7: Sublimation Rate Data（Reference

    2-3 Sublimation rate data（reference） ・AC230V,50Hz Conditions ■ Model FDS-1000 ・Ambient temperature 20℃ ・ After prior freezing of four 100 mL sample (egg-plant shaped) flasks, each filled with 38g of water (a total of 152g), they were installed to the trap. The sublimation rate was calculated back from the residue of flasks after the time had passed.

  • Page 8: Optional Parts

    2-4 Optional parts ■ Cock Ｃ,test tube, ampoule, etc. ① ④ ② ⑦ ⑨ ⑩ ⑮ ⑤ ⑧ ⑭ ⑲ ⑯ ⑫ ⑪ ③ ⑥ ⑱ ⑬ ⑰ ⑳ ※① The cock C belongs to the manifold. Prepare other adapters separately according to the intended use. - 4 -...
  • Page 9 Name Standard Quantity Code No. Cock C FD-1000,PMS-4S/4A（manifold for FDS-1000） 191140 Adapter for ampoule For φ8 120520 For 6 120530 Ampoule Egg-plant shaped（1ml） 120210 Pencil shaped with round bottom（1ml） 120220 Pencil shaped with flat bottom（1ml） 120221 Flat bottom（2ml） 120230 Flat bottom（5ml）...
  • Page 10 Name Standard Quantity Code No. Cap （for freeze-drying bottle） φ70、（for 120ml, 150ml, 300ml） 120030 Micro-tube holder 1.5ml×12 micro-tubes installed 191110 Freeze-drying bottle 150ml、φ70 120130 Freeze-drying bottle set Bottle：150ml、φ70 / cap：φ70 119970 Micro-tube holder 1.5ml×24 micro-tubes installed 191150 Freeze-drying bottle 300ml、φ70 120140 Freeze-drying bottle set Bottle：300ml、φ70 / cap：φ70...

  • Page 11: Name Of Parts

    2-5 Name of parts 180°turn Trap barrier Control panel Trap bath Option fixing plate Trap packing Drain plug Hose holder Set screw (x 8) Drain hose Rubber leg (x 4) Ventilation cover ※Details of filter installation Install a tube to the one-touch coupling for leak filter and insert the filter onto the tube.

  • Page 12: Name And Functions Of Parts

    3 Name and Functions of Parts 3-1 Control panel ⑪ Vacuum indicator ⑩ Trap temperature display ⑫ Timer indicator ⑳ Set lamp ⑬ Freeze-drying ready ⑱ Timer mode display lamp selector key Timer ⑲ Set key ⑭ Refrigerator operation Trap Disp Temp.
  • Page 13 Name Functions ① Power switch Switch to turn ON/OFF system power ② AUTO/MANUAL selector Switch to select the automatic operation or manual operation switch ③ AUTO lamp ON when the automatic operation is selected ④ Refrigerator key With this key ON in the automatic or manual operation, the refrigerator operates.
  • Page 14 Name Functions ⑰ Time mode display lamp The lamp goes on to display the timer measuring time mode: Mode1：ON for display of the vacuum pump operation time Mode2：On to display the time of stopwatch function ⑱ Timer mode selector key Key to select the timer display time (Mode1・2) To set the power failure time, press the key.

  • Page 15: Safety Functions

    3-2 Safety Functions This product has the safety functions and alarm display functions as shown in the table below. Safety functions Safety device Description Cause ・Either the leak or overcurrent has occurred. Leak/overcurrent OFF to turn OFF power supply breaker ・The operating ambient temperature exceeds Refrigerator self- The refrigerator is stopped when its...
  • Page 16 Alarm functions Name of alarm Alarm display and operation Cause and canceling Cause Vacuum sensor Alarm lamp goes ON, the vacuum display ・The vacuum sensor broken break alarm shows “PrEr”, and the buzzer sounds (10 sec). Alarm canceling The control continues in the manual ・Turn OFF power supply, replace the sensor, operation.

  • Page 17: Installation

    15cm 20cm wall/ceiling surfaces so as to maintain the product performance. Exhaust Caution 20cm Take sufficient care when Air intake transporting the product since it is a heavy object. FDS-1000(Approx.18kg) - 13 -...

  • Page 18: Connecting The Utilities

    Product type Voltage Capacity connected. Power supply to be connected to the product FDS-1000 AC230V is as shown in the right. (2) Check the receptacle of installation place. ( * Do not connect the power supply yet. ） The power plug with an earth pole can be connected to an earthed outlet directly.
  • Page 19 (1) Prepare the vacuum pump. GCD-051X 50/60 190850 GCD-136XN 135/162 189160 ※ The consumption current for two receptacles of FDS-1000 main body is a total of 【Max GCD-051XF 50/60 191080 5A】. GCD-136XNF 135/162 191090 When only one receptacle is used, the vacuum pump of 【max 5A】can be...
  • Page 20 Disassembling connector for vacuum pump (3)Wiring connector for vacuum pump 1) Disassemble connector for vacuum pump Remove and solder lead wires of external device Screw for the Turn the shell clamp for fixing on the terminal of connector. Main unit left to remove lead wire ※Insulate soldered...
  • Page 21 ※ The holding plate of Model PMS-4A secures the flange Place the holding plate on the manifold while of manifold. Secure the manifold to the FDS-1000 main aligning the central concave of the plate to body and turn the upper port to adjust the direction.
  • Page 22 ※ For securing of the manifold, refer to “5-1.3.1 FDS-1000 Installing the manifold” of the operation manual of Model FDS-1000. ※ Depending on the position at which the drip Holding plate box for flask is screwed, the holding plate may Turn the holding not be assembled in the direction of the figure.
  • Page 23 ※ When the cover is removed and placed by the side of the main body, take care not to damage the Trap cover opening (vacuum sealed). （packing） FDS-1000 Option fixing plate Main body Set screw (at four Option points) used as...

  • Page 24: Operation Method

    5-2 Operation method When using such options as the dry chamber, spare This operation is for freeze-drying in the flask while freezing bath, pre-freezer, etc., refer to the manual using the optional manifold. attached to these options. The operation is basically the same for other options and containers.
  • Page 25 1. Before operation Remove the drain plug and confirm that water is drained from the trap and drain hose. After confirmation, insert the drain plug firmly. ※ If the operation is started while water is remaining Disconnect from the hose holder in the trap and drain hose, the vacuum pump and Pirani vacuum gauge sensor may fail.
  • Page 26 3）Use of the timer The timer display changes between Mode1/Mode2 each time the “[Disp(▲)]” key of Timer on the control panel is pressed. Timer Mode1 hour Mode1：The vacuum pump operation time is Mode2 hour.min automatically measured and displayed. This ※ The display range of mode1 is 0～9999 hours. mode proves convenient when used for （the lowest digit;...
  • Page 27 【 Automatic operation 】 4.Automatic Operation Caution ● This section describes the operation while referring Take utmost care for the amount of to the case of using the manifold. dry sample 1) With the “Auto” lamp of control panel ON, press The dehumidification capacity of the product the “Run/Stop”...
  • Page 28 【 Automatic operation 】 After installation of the sample container, 5) Freeze drying the degree of vacuum rises gradually, with After installation of the sample container, the frosting occurs on the cooling section in the trap. degree of vacuum rises gradually, with frosting White frosting on the surface of sample container occurs on the inner wall (cooling section) in the trap.
  • Page 29 【 Automatic operation 】 8) Defrosting Caution Keep pressing the [Def] key for three seconds or more. The “Defrosting” lamp goes ON, and defrosting begins. In this event, the refrigerator and Do not collect 300 mL or more water vacuum pump stop operation automatically. in the trap bath.
  • Page 30 【 Manual operation 】 5.Manual Operation Caution The refrigerator and vacuum pump can be operated independently (with the control panel “Auto” lamp Take utmost care for the amount of OFF). dry sample In the manual operation, the freeze-drying ready lamp “Freeze Drying”...
  • Page 31 【 Manual operation 】 After installation of the sample container, 5) Freeze drying the degree of vacuum rises gradually, with After installation of the sample container, the frosting occurs on the cooling section in the trap. degree of vacuum rises gradually, with frosting White frosting on the surface of sample container occurs on the inner wall (cooling section) in the trap.
  • Page 32 【 Manual operation 】 8) Defrosting Caution Keep pressing the [Def] key for three seconds or more. The “Defrosting” lamp goes ON, and defrosting begins. In this event, the refrigerator and Do not collect 300 mL or more water vacuum pump stop operation automatically. in the trap bath.

  • Page 33: Troubleshooting Guide

    Contact your dealer or the nearest 6 Troubleshooting Guide service center for troubles not listed here. Symptom Cause Countermeasure The leak breaker is turned Electric leak Stop operation immediately and contact the OFF immediately even when shop from which you have purchased the Overcurrent flowing it is turned ON.
  • Page 34 Symptom Cause Countermeasure No light exhaust sound in Vacuum cock not fully closed Check the direction of vacuum cock and about 30 seconds after start close it fully. of the vacuum pump Faulty installation of the trap Retry installation of the trap. （Pressure not lowering) Dust adhering to the contact surface Remove dust。...
  • Page 35 Symptom Cause Countermeasure Vacuum sensor break Break in the vacuum sensor circuit Contact the shop from which you have alarm issued purchased the product or our nearest service center. Vacuum display Vacuum Guage Alarm lamp Alarm Ref.Alarm Power failure alarm Power has failed during control or Press the [Set] key.

  • Page 36: Maintenance And Inspection

    7 Maintenance and Inspection 7-1.Replacing the consumables Leak filter The trap packing (material: chloroprene rubber), (Air filter) vacuum hose (material; natural rubber), leak filter, and Vacuum tube vacuum sensor are consumables. Since deterioration and aging differ depending on the dry sample and use conditions, carry out regular inspection.

  • Page 37: Operation Test Of The Leak Breaker

    7-2 Operation test of the leak breaker Caution Leak breaker Control panel in the front of main body Never fail to perform an operation test （Power switch） for ELB. Operating the product with a defective ELB might cause an electric leakage and an electrical Test button shock.

  • Page 38: Cleaning And Care Of The Product

    7-4. Cleaning and care of the product WARNING CAUTION Never attempt to disassembly Do not touch the cooling fin with the product. bare hand. The unit contains parts with high voltage Do not touch the cooling fin with bare hand applied become hot,...

  • Page 39: Disposal Of Product

    Standard/ Total External dimensions Components How to discard （mm） specifications weight Approx. Request the disposal FDS-1000 445W×220D×497H Main body 19kg operator for disposal. Material of principal parts Principal components Principal component parts Principal materials Galvanized plyboard （SECC,SEHC） Casing, fin cover...

  • Page 40: After-Sale Services

    After-sale Services 1. In case the product does not function satisfactorily, check first referring page troubleshooting to see if this is actually a trouble. 2. If the product remains unsatisfactory even after checking, please contact the distributor from which the user has purchased the product.

  • Page 41: Optional Products

    Optional Products No. Code No. Model/STD Q'ty No. Code No. Model/STD Q'ty No. Code No. Model/STD Q'ty No. Code No. Model/STD Q'ty 261990 PMS-4S 1 set 262100 PMS-4A 1 set 262008 DRS-1 1 set 262018 DRS-2 1 set No. Code No. Model/STD Q'ty No.

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