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Atomx XYZ User Manual Part Number: 15-3200-074 Rev: B, June - 2018...
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The companies indicated own the following trademarks: Tekmar .......... Teledyne Instruments, Inc. All other brands or product names are trademarks or registered trademarks of their respective owners. Contact Information Teledyne Tekmar 4736 Socialville Foster Road Mason, OH 45040 U.S.A www.teledynetekmar.com...
You must adhere to and integrate the following instructions into your safety program when installing, using, and maintaining the Atomx XYZ. Failure to follow the proper instructions may invalidate the warranty.
When replacement parts are required, ensure that qualified individuals use replacement parts specified by Teledyne Tekmar. Unauthorized parts and products can affect the product’s performance and jeopardize safety. Using look-alike substitutions may result in fire, electrical hazards, or improper operation.
P.5 Atomx XYZ Safety Symbols Defined The Atomx XYZ instrument is labeled in compliance with the marking and nomenclature specified in the UL61010-1Ed. 3 (2012) safety standard. The following symbols and their associated signal words are used in the manual and on instrument labels.
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Risque de blessures aux yeux. Porter des lunettes de sécurité et autres équipements de protection personnel appropriés. Pinch Point Hazard! Keep hands and other appendages away. Danger d’écrasement! Garder les mains et autres membres éloignés. Lift Point! Point de Levage! Atomx XYZ Safety Symbols Defined P - 4 Atomx XYZ User Manual...
P.6 Atomx XYZ Safety Labels Electrical Ground Prise de terre WARNING: Electrical shock hazard. Do not operate without cover. DANGER: Risque d’électrocution. Ne pas utiliser sans capot. WARNING: To avoid electrical shock, disconnect supply before changing fuses. DANGER: Pour éviter le risque d’électrocution, débrancher l’alimentation avant de remplacer les fus- ibles.
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Do not plug the Atomx XYZ into an extension cord. An extension cord may overheat and cause a fire. Only replace the Atomx XYZ mains supply AC power cable with a UL listed cable of the same current and voltage rating.
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To avoid injury to yourself or damage to the Atomx XYZ, do not exceed the recommended pressure settings. Observe safety regulations when handling pressurized gas. For more information see Matheson™ Gases Data Book (available from the Matheson Company, East Rutherford, New Jersey).
GC and the 4-way tee, allow the components to cool to room temperature. 6-Port Valve Analytical Trap Sample Mount Sample Needle & Cup Sample Transfer Line Soil Valve 4-Way Tee Working Safely P - 8 Atomx XYZ User Manual...
European Waste Electrical and Electronic Equipment Directive (WEEE, 2002/96/EC). Please contact Teledyne Tekmar or your local distributor for instructions on returning the system for proper disassembly and disposal. Contact Teledyne Tekmar Customer Support.
The Atomx XYZ single needle design transfers liquid sample aliquots from the vial to the sparger. Low -level solid samples are purged directly in the vial, transferring to the trap.
After a certain period of time at a constant temperature, the concentration of the volatile compounds in each phase will be stabilized, the chemical system will have reached equilibrium (Figure 1-1). Chapter 1: Introduction 1 - 2 Atomx XYZ User Manual...
These limitations are determined by the compounds of interest in the sample and the sorbent material used in the trap. Chapter 1: Introduction 1 - 3 Atomx XYZ User Manual...
The desorption is carried out by back-flushing the trap, ensuring that the less volatile, or heavier, analytes never come in contact with the stronger sorbent. Chapter 1: Introduction 1 - 4 Atomx XYZ User Manual...
1-10. GC Interface Designed to interface with virtually all commercially available GC instruments. Column Compatibility Teledyne Tekmar recommends the use of 20 m x 0.18 mm ID Fast Volatiles columns. Chapter 1: Introduction 1 - 5 Atomx XYZ User Manual...
Environmental, Food and Beverage, Petrochemical, & Plastics & Polymers Certifications Certifications are listed on the Declaration of Conformity (DOC). The DOC is included with the instrument, in the shipping box. Chapter 1: Introduction 1 - 6 Atomx XYZ User Manual...
Programmable automatic dilutions of methanolic extract of 1:100 or 1:50, 5 mL sample volumes. a. Includes all types of soils and sediments. Sample procedure: Automated methanol extraction and subsequent dilution per USEPA 5035 high-level soil methodology. Chapter 1: Introduction 1 - 7 Atomx XYZ User Manual...
(US Patent 7,651,866). Electronic Pressure Monitor Automatic leak check and over-pressure sensing capability. Ability to record purge and bake pressures for each sample. Chapter 1: Introduction 1 - 8 Atomx XYZ User Manual...
220-240 VAC +/- 10%, 50/60Hz, 5.0A, 1150W External Circuits The circuit used to power the Atomx XYZ should be protected by a Certi- fied/Listed 15/20 Circuit Breaker for short circuit protection. The AC Power Cable supplied with the Atomx XYZ is compliant with applicable safety standards.
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4 °C (39.2 °F) until they are sampled. Guardian Foam Sensor and Eliminator Optional Guardian Foam Sensor and Foam Eliminator senses foam, stops (Optional) purge, and adds defoaming agent for samples prone to foaming. Chapter 1: Introduction 1 - 10 Atomx XYZ User Manual...
The analytical trap heating jacket heats the analytical trap to a consistent tempera- Resistance Temperature Detector ture defined in the Atomx XYZ TekLink software. The Resistance Temperature Detec- (RTD) tor (RTD) in the heating jacket verifies this temperature to the software.
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Communicates to the GC via GC I/O cable and the controlling PC via the USB Port. Board) DC Valve Control Board Actuates the Atomx XYZ solenoid valves, as well as the analytical trap and the Mois- ture Control System (MCS) cooling fans. Internal Standard Valve Control Controls all Internal Standard valve outputs.
The front panel contains a heated sample mount and glass sparge vessel. The sample mount is heated via the 6-port valve oven plate on one end and a cartridge heater inside the mount itself. A standard 5 mL frit sparger is included with the Atomx XYZ. The following options are also available: ...
(i.e. Presweep A&B). 1.5.4 Internal Standard Vessels Atomx XYZ is equipped with three 15 mL amber internal standard vessels. The amber color prevents transmission of UV radiation, preserving standard integrity. Vessels are sealed with a PEEK cap to prevent adsorption and contamination of the standard solution.
"6-Port Syringe Valve". Figure 1-5 Syringe 1.5.6 Sample Needle The Atomx XYZ uses a patented 3-stage sample needle to displace sample from the vial (versus aspirating per USEPA methodologies), purge in the vial and complete methanol extractions. Figure 1-6...
If the gripper is not functioning correctly, first ensure the sample gas supply is on, properly connected, and supplying 65 - 100 psi (4.48 bar - 6.89 bar) to the Atomx XYZ. 1.5.8 Elevator The elevator moves from the down position where the vial is loaded, to the up position where the vial is pierced by the 3-stage needle for sampling.
1.5.10 Status Light The Atomx XYZ logo changes color to indicate the instrument’s state. The status related to each color is shown in Table 1-17 "Status Light Indications". The Atomx XYZ logo is lit using an LED board behind the panel.
TekLink. 1.5.12 Mass Flow Controller (MFC) The Atomx XYZ incorporates a patented mass flow controller to monitor and control the gas flow rates throughout the entire purge and trap process. Once set, the parameters remain precisely controlled throughout all modes of operation and achieve highly repeatable analyses.
Resistance Temperature Detector (RTD) inside the trap heating jacket. The trap compartment door is equipped with a magnetic switch and must be closed for the system to operate. Figure 1-11 Atomx XYZ Analytical Trap Compartment Resistance Temperature Detector (RTD) Cooling Fan...
VOCs being transferred to the GC column stay in their gaseous state. Carrier gas makes a passive loop through the Atomx XYZ and returns, unchanged, to the GC through the transfer line. GC carrier gas is independently controlled through the GC or an External Pressure Control (EPC).
1.5.17 Valving The Atomx XYZ contains the valves shown in Table 1-18 "Valve Overview". The internal standard pressure regulator is also located on the valve manifold. Table 1-18 Valve Overview Solenoid Valves 9 (standard configuration) or 11 (optional Guardian Foam Eliminator configuration) 24 VDC...
Heated Soil Valve The soil valve is an On/Off heated 24VDC solenoid used for solid (soil) samples purged in the vial (with or without methanol extraction). Figure 1-16 Soil Valve Chapter 1: Introduction 1 - 22 Atomx XYZ User Manual...
Resistance Temperature Detector (RTD) that is slid over the sample glassware. The heater is capable of heating the sparger from 35 °C to 100 °C (95 °F to 212 °F). Figure 1-18 Sparge Vessel Heater Chapter 1: Introduction 1 - 23 Atomx XYZ User Manual...
Atomx XYZ from the adverse effects of liquid entering the gas pathway. The Atomx XYZ can be equipped with only the foam sensor to trigger an alert or the sensor and eliminator to trigger an alert, remove the foam from the sample, and rerun.
2.1.2 Operating Environment The Atomx XYZ operates at temperatures between 10 °C and 30 °C (50 °F and 86 °F) with humidity levels between 10% and 90%. These temperatures and humidity levels are consistent with a standard lab environment and should pose no difficulty.
2.1.3 Work Surface Requirements The Atomx XYZ is 49.5 cm (19.5”) high, 70.1 cm (27.6”) wide, 58.4 cm (23”) deep, and weighs 43.09 kg (95 lbs). Caution The Atomx XYZ weighs 43.2 kg (95 lbs). If this weight exceeds your lifting ability, lift and position the Atomx XYZ with two people.
3. The diameter of the tubing that supplies the gas depends on the maximum pressure drop allowable for the configuration. If the helium supply is close to the Atomx XYZ, use the pre-installed blue 1/8” (0.32 cm) tubing. ...
PTFE tape. Volatile materials in the dope and/or low-grade tape will contaminate the tubing. 2.1.6 Minimum Computer Requirements Connect the Atomx XYZ to a computer that meets or exceeds the specifications shown in Table 2-1 "Minimum Computer Requirements": Table 2-1 Minimum Computer Requirements...
2.3 Unpacking the Atomx XYZ Caution The Atomx XYZ weighs 95 lbs (43.1 kg). If this weight exceeds your lifting ability, lift and position the Atomx XYZ with two people. When lifting the Atomx XYZ, use the designated lift points.
2.5 Atomx XYZ System Overview Figure 2-2 Front of Atomx XYZ Sample Vial Cup Sample Analytical Trap Sample Mount Status Light and Elevator Needle Compartment Sparger XYZ Robotic Syringe Internal Sample Vessels Chapter 2: Installation and Setup 2 - 6...
Figure 2-3 Back of Atomx XYZ GC I/O Connection USB Connection Heated Sample Transfer Line and Carrier Gas Line Power Entry Module Blue Sample Gas Tubing Drain Tubing Methanol Tubing Clear DI Water Tubing Chapter 2: Installation and Setup 2 - 7...
2. Plug the AC power cord into the PEM and connect it to a properly rated and grounded AC receptacle. WARNING The circuit used to power the Atomx XYZ should be protected by a Certified/Listed 15/20 Circuit Breaker for short circuit protection. WARNING Ensure the power cable is routed away from, and is not capable of contacting, any hot surface.
1. Connect the GC I/O cable to the gas chromatograph according to the GC instructions. 2. Connect the GC I/O cable to the GC I/O port on the back of the Atomx XYZ. 3. Once connected, communication to the GC will be configured via the >C...
(found in the Installation Kit Box) to the laboratory helium or nitrogen supply line. 2. Route the blue 1/8” (0.32 cm) sample purge gas tubing from the Atomx XYZ to the tee and connect. Insert the tubing into the union, and then tighten with a 7/16”...
Transfer Line Connection to the Gas Chromatograph (GC) The Atomx XYZ connects to the regulated carrier gas of the GC at a location after the GC Electronic Pressure Control (EPC) and prior to the GC injection port. By connecting at this location, the GC regulated carrier gas is routed through the Atomx XYZ to carry desorbed VOCs from the analytical trap back to the GC sample inlet.
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5/16” wrench to hold the center of the union and another to tighten the nut. 4. Connect the Atomx XYZ carrier gas line (outside tubing) to the union on the tubing from the GC Electronic Pressure Control (EPC). Connect the union to the tubing in the same manner as previous procedures.
The Atomx XYZ requires a source of DI water for system rinsing, auto-blanks and dilutions. The Atomx XYZ is supplied with a 10 L reservoir for the DI water supply. To avoid contamination problems, use blank (organic-free) water. Follow the instructions below to supply the instrument with DI water: 1.
NOTE Do not locate the water reservoir more than 4 ft (1.22 m) below the Atomx XYZ unit. Height differentials larger than 4 ft (1.22 m) can cause damage to the syringe due to siphoning. Figure 2-10 DI Water Tubing (Weights Not Shown) 2.8.3 Optional Methanol Reservoir Connection...
For computer requirements refer to Section 2.1.6 "Minimum Computer Requirements". 1. Ensure the controlling computer is not connected to the Atomx XYZ via USB cable. 2. Power on the controlling computer. 3. Insert the Atomx XYZ TekLink Software Installation CD into the computer’s disc drive.
8. The wizard will request where to install the software. Use the default software installation location shown or browse to a custom location. Once chosen, select the N to continue. UTTON Chapter 2: Installation and Setup 2 - 17 Atomx XYZ User Manual...
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TART OLDER shortcut. Use the default location or browse to a custom location for the software shortcut. Once chosen, select the N to continue. UTTON Chapter 2: Installation and Setup 2 - 18 Atomx XYZ User Manual...
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Select if you would like the software icon to be installed on the desktop by placing a check mark beside the selection. Once chosen, select the N to continue. UTTON Figure 2-20 Select Additional Tasks Chapter 2: Installation and Setup 2 - 19 Atomx XYZ User Manual...
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12. The software is now ready to install. Select the I to install the NSTALL UTTON software. Figure 2-21 Ready to Install 13. The software installation progress will be shown. Figure 2-22 Installation in Progress Chapter 2: Installation and Setup 2 - 20 Atomx XYZ User Manual...
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15. Once the software is installed, the C will be shown. Select the OMPLETION CREEN to complete the installation and close the wizard. INISH UTTON Figure 2-24 Software Completion Chapter 2: Installation and Setup 2 - 21 Atomx XYZ User Manual...
2.9.1 Connect the USB Interface Cable 1. Connect the supplied USB cable to the USB port at the back of the Atomx XYZ, then to a USB port on the computer. 2. Power on the Atomx XYZ. Figure 2-25 Atomx XYZ USB Connection 2.10 Create an Instrument Profile...
NOTE If other Atomx XYZ instruments are on the same network, use the name and description to differentiate one instrument from another. This will assist when defining system properties and settings. Enter a D that easily identifies the instrument. ...
4. On the L HECK Customize L pressure settings, HECK RESSURIZE HECK and L (amount of change in pressurization that indicates a HECK ELTA leak). Figure 2-28 Leak Check Tab Chapter 2: Installation and Setup 2 - 24 Atomx XYZ User Manual...
XYZ’s gas pathway. When combined with the optional foam eliminator, a defoamer is added to the sample. If ordered with the Atomx XYZ, the Guardian Foam Sensor and/or Foam Eliminator will be installed. To retrofit a Atomx XYZ with the Guardian Foam Sensor and/or Foam Eliminator refer to the installation instruction sheet included with the Guardian Foam Sensor and Foam Eliminator.
2.11.2 Atomx XYZ with Guardian Foam Sensor and Foam Eliminator 1. When foam is sensed, the Atomx XYZ shuts off the purge gas. The purge clock is stopped and the Foam Transfer Valve is activated to add a defoaming agent.
Figure 2-30 Configuration Dialog- Guardian Foam Sensor 2.12 Preparing DI Water The Atomx XYZ requires a source of DI water for system rinsing, auto-blanks, dilutions and high temperature system rinse. To avoid contamination problems, use blank (organic-free) water. Teledyne Tekmar recommends using deionized (DI) water. Several methods for preparing blank water are listed below: ...
E = Stock standard concentration (ppm) Example A = 5 ppb B = 25 mL C = 2 µL D = 10 mL E - 2000 ppm Chapter 2: Installation and Setup 2 - 28 Atomx XYZ User Manual...
"Minimum Computer Requirements". For information on installing Atomx XYZ TekLink refer to Section 2.9 "Install Atomx XYZ TekLink Software". 3.1 About Atomx XYZ TekLink Software Atomx XYZ TekLink is a software user interface designed for the following functions: Define custom methods or operating sequences that meet analytical requirements by defining Standby, Purge, Desorb and Bake parameters.
(according to screen). Figure 3-3 Schedules Screen Title Bar Instrument Profile Schedule Name Method Type Instrument Profile Method Type Method Name Chapter 3: Atomx XYZ TekLink Software Overview 3 - 2 Atomx XYZ User Manual...
- Save the currently open method or schedule. UTTON NOTE Atomx XYZ TekLink includes default water, soil, and methanol extraction methods that cannot be over-written. To use a default method, open it from the Method Screen or select it from the Method Drop-down on the Schedules Screen.
CHEDULE IALOG OURCE DOWN NOTE Archive settings and the Archive Now command are located under Tools>System Properties>Data Tab. Figure 3-7 Open Schedule Dialog Source Drop-down Menu Chapter 3: Atomx XYZ TekLink Software Overview 3 - 4 Atomx XYZ User Manual...
OOLS CREEN configuration options and settings, and sample, instrument, and error logs. - Atomx XYZ TekLink Help is context sensitive and provides information on the software and instrument functionality. Figure 3-8 Home Screen Chapter 3: Atomx XYZ TekLink Software Overview...
Current/Set-Point Temperature by Zone NOTE Right-clicking on the Zones Panel of the Instrument Status Screen will show additional display options. Figure 3-10 Instrument Status Zone Display Options Chapter 3: Atomx XYZ TekLink Software Overview 3 - 6 Atomx XYZ User Manual...
TANDBY URGE ESORB method parameters. Because method parameters vary according to the type of analysis conducted on the Atomx XYZ, the user is first prompted to select a method type (W ATER ETHANOL Figure 3-11 Choose Method Type Dialog Once the method type is selected, the header of the screen and the parameters contained on each of the screen’s tabs will correspond to that type of analysis.
Parameters vary according to the method type chosen. Water Method Purge Tab Options NOTE Teledyne Tekmar recommends a sample gas flow of 40 mL/min ±5 mL for 11 minutes to achieve a 440 mL purge volume. Chapter 3: Atomx XYZ TekLink Software Overview...
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Purge to ensure that all samples are purged under the desired conditions. Figure 3-14 Waters Methods Screen - Purge Tab - Sparge Vessel Heater Enabled Sparge Vessel Heater Enabled Chapter 3: Atomx XYZ TekLink Software Overview 3 - 9 Atomx XYZ User Manual...
This parameter allows for the addition of water to soil samples. It will be necessary to add water if the user wishes to add internal standards to the sample via the automated standard addition feature of the Atomx XYZ. Figure 3-15 Soil Methods Screen - Purge Tab...
Ensure that adequate settling time is allowed to prevent particulate matter from being drawn into the needle and syringe. Figure 3-16 Methanol Extraction Methods Screen - Purge Tab Chapter 3: Atomx XYZ TekLink Software Overview 3 - 11 Atomx XYZ User Manual...
B beginning and end (the latter two are typically ESORB ESORB used in conjunction with a cryofocusing inlet). Figure 3-17 Waters Methods Screen - Desorb Tab Chapter 3: Atomx XYZ TekLink Software Overview 3 - 12 Atomx XYZ User Manual...
Volume of methanol to be used to rinse the sparger. A volume of one or two milliliters larger than the sample volume should be employed to ensure adequate rinsing of the glassware. Figure 3-18 Water Methods Screen - Bake Tab Chapter 3: Atomx XYZ TekLink Software Overview 3 - 13 Atomx XYZ User Manual...
- A drop-down menu that allows the selection of default water, soil ETHOD and methanol methods, as well as any custom methods saved in the Current or Archived Data folders. Chapter 3: Atomx XYZ TekLink Software Overview 3 - 14 Atomx XYZ User Manual...
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STD1, STD2 and STD3 - These columns permit the addition of check and/or internal standards to the sample when running water and soil methods. When the Atomx XYZ is running a methanol extraction sample, STD3 is reserved for a matrix spike to be added to the vial prior to extraction. NOTE...
OOLS CREEN diagnostics. It also contains software preferences and configuration options and settings as well as sample, instrument, and error logs. Figure 3-21 Tools Screen Chapter 3: Atomx XYZ TekLink Software Overview 3 - 16 Atomx XYZ User Manual...
3.6.2 Commands Menu Leak Check Activates the Atomx XYZ leak check function. The system performs a leak check by closing specific valves and shutting down the Mass Flow Controller (MFC) to isolate the pressurized system. Once isolated, the Atomx XYZ will take pressure readings to identify any pressure loss that would indicate a leak.
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Moisture Control System Bake Temperature Bake Flow DI Water and Methanol Bake Rinse The dialog contains selection boxes for the following sample pathway rinses to reduce carryover: Chapter 3: Atomx XYZ TekLink Software Overview 3 - 18 Atomx XYZ User Manual...
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The wizard is used to align the X, Y, and Z axis of the autosampler arms through a sequence of steps. Refer to the Section 5.18 "XYZ Autosampler Alignment". Chapter 3: Atomx XYZ TekLink Software Overview 3 - 19 Atomx XYZ User Manual...
Tools>Instrument Manager unless the “Show deactivated instrument profiles” Check-Box is selected in that dialog. Figure 3-24 Tools - Configuration - General Tab Chapter 3: Atomx XYZ TekLink Software Overview 3 - 20 Atomx XYZ User Manual...
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GC. If the model is not found from the drop-down list, refer to the GC manufacturer’s instructions and use the S :63 or U TANDARD ADIO UTTONS Figure 3-25 Tools - Configuration - Options Tab Chapter 3: Atomx XYZ TekLink Software Overview 3 - 21 Atomx XYZ User Manual...
YSTEM ROPERTIES IALO configuration and histories (sample, instrument, and error). The M contains a selection box to display an on-screen keyboard. Figure 3-28 System Properties Dialog Chapter 3: Atomx XYZ TekLink Software Overview 3 - 23 Atomx XYZ User Manual...
USING THE MOST RECENT SETTINGS information. NOTE Data cannot be archived when a schedule is running. Archives are full backups of all current data used by Atomx XYZ TekLink. If the is selected on the M or S ELETE AFTER THE NEXT ARCHIVE...
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RROR ISTORY to refine results. When troubleshooting, information from the V VENT ILER ISTORY may be requested by a Teledyne Tekmar Customer Support Representative. Use the or E RINT XPORT UTTONS Figure 3-31 History Log - Sample History Chapter 3: Atomx XYZ TekLink Software Overview...
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Event filters can be returned to their default settings by selecting “Click here to return to the default filter for this view”. Figure 3-33 History Log Event Filter Chapter 3: Atomx XYZ TekLink Software Overview 3 - 26 Atomx XYZ User Manual...
Atomx XYZ TekLink software and the BOUT IALOG firmware installed on the Atomx XYZ. When troubleshooting, information from the may be requested by a Teledyne Tekmar Customer Support B O U T I A L O G Representative.
3.6.4 Diagnostics Valves and Flows The V provides discrete control of the Atomx XYZ valves, fans, ALVES AND LOWS CREEN and Mass Flow Controller (MFC) for diagnostics and troubleshooting. The MFC flow rate can be manually set and the actual flow and pressure can be observed. The beeper and banner board (Instrument Status Light) can also be tested on this screen.
- Used to manually open and close the gripper. This RIPPER LOSE control is frequently used to insert the alignment probe into the gripper for the autosampler alignment procedure. Chapter 3: Atomx XYZ TekLink Software Overview 3 - 29 Atomx XYZ User Manual...
Printed Circuit Boards (PCB). The current firmware version can be viewed via >A (Figure 3-34). OOLS BOUT UTTON NOTE For information on upgrading the XYZ autosampler firmware, refer to Section 5.24 "Upgrade Autosampler Firmware". Chapter 3: Atomx XYZ TekLink Software Overview 3 - 30 Atomx XYZ User Manual...
To access benchmark test results select T >V OOLS ISTORY >I NSTRUMENT ISTORY NOTE For information on using the benchmark test function refer to Section 5.26.1 "Benchmark Test". Figure 3-39 Benchmark Test Chapter 3: Atomx XYZ TekLink Software Overview 3 - 31 Atomx XYZ User Manual...
On the G ENERAL Enter a name for the instrument profile. If there are other Atomx XYZ instruments on the network, use the name and description to differentiate one from another. Enter a description that easily identifies the instrument.
. If the specific model of the GC is not shown in the drop-down menu, use the S :63 or U :31 check-box according to the GC TANDARD manufacturer’s User Manual instructions. Figure 3-41 Options Tab Chapter 3: Atomx XYZ TekLink Software Overview 3 - 33 Atomx XYZ User Manual...
1. From the H select the T CREEN OOLS UTTON 2. On the T select the C to display the OOLS CREEN ONFIGURATION UTTON ONFIGURATION IALOG Chapter 3: Atomx XYZ TekLink Software Overview 3 - 34 Atomx XYZ User Manual...
Figure 3-44 Choose Method Type Chapter 3: Atomx XYZ TekLink Software Overview 3 - 36 Atomx XYZ User Manual...
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ALUE OLUMN NOTE For information on parameters of note refer to Section 3.4 "Methods Screen". Also refer to Section 4.4 "Method Parameters". Chapter 3: Atomx XYZ TekLink Software Overview 3 - 37 Atomx XYZ User Manual...
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Note that the title bar on the Methods Screen updates with the method name. Figure 3-47 Save Method As Dialog Name Method Figure 3-48 New Method Saved - Name in Title Bar New Method Name Chapter 3: Atomx XYZ TekLink Software Overview 3 - 38 Atomx XYZ User Manual...
3.8.5 Load the Method Select the L to prompt the Atomx XYZ to begin using method ETHOD UTTON parameters immediately. After temperature set-points are reached, the system will go into standby/purge ready. If the method is not loaded from the M...
<Enter>. The zero will turn to BLK indicating a blank in the schedule line selected (Line 1 in Figure 3-51). Alternatively right-click in the V OLUMN and select U SE BLANK INSTEAD OF VIAL Chapter 3: Atomx XYZ TekLink Software Overview 3 - 40 Atomx XYZ User Manual...
OLUMN on the I via T >C NSTRUMENT ONFIGURATION CREEN OOLS ONFIGURATION . Enter a sample ID in the field. UTTON Figure 3-53 Sample ID Column Chapter 3: Atomx XYZ TekLink Software Overview 3 - 41 Atomx XYZ User Manual...
UTTON CHEDULE IALOG name for the schedule can be entered. Select the O to save the schedule. UTTON Figure 3-55 Save Schedule Name Schedule Chapter 3: Atomx XYZ TekLink Software Overview 3 - 42 Atomx XYZ User Manual...
M was not previously loaded from the ETHOD DOWN IELD , it will be loaded when the schedule is loaded and the Atomx XYZ will ETHODS CREEN begin using those method parameters. Once the schedule is loaded, the schedule’s S...
H will change to an A . Select the A UTTON UTTON UTTON resume the schedule. Figure 3-58 Schedule Hold - Instrument Status Panel Chapter 3: Atomx XYZ TekLink Software Overview 3 - 44 Atomx XYZ User Manual...
3. The E NTIRE CHEDULE AFTER URRENT AMPLE Figure 3-59 Abort Dialog 3. Once the type of abort has been selected, Atomx XYZ TekLink will prompt to confirm the abort command using the C on the S ONFIRM UTTON CHEDULES...
3.10 Data Storage Location and Archiving Data Archives are full backups of all data used by Atomx XYZ TekLink including method, s c h e d u l e , c o n f i g u r a t i o n , h i s t o r y a n d a r c h i v e s . T h e d a t a i s s t o r e d i n C:\ProgramData\Teledyne Tekmar\VOC AtomxXYZ TekLink Data by default, and cannot be changed.
Preheat Purge When the Atomx XYZ is working in conjunction with the sparge vessel heater, this mode allows the sample to reach a uniform programmed temperature, prior to sample purging. Purge This is a VOC extraction mode in which the inert gas (such as helium) is dispersed through the sample matrix in the sparger (or in the sample vial if a soil) for a preset time and flow.
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This mode allows methanol to be introduced into the sparger for syringe, glassware and line rinsing, to clean the system between samples. Methanol Rinse Drain This mode drains the methanol, introduced to the sample glassware during the Methanol Rinse Mode, from the system. Chapter 4: Instrument Operations 4 - 2 Atomx XYZ User Manual...
The temperature range for the Atomx XYZ sample mount is 35 °C to 100 °C (95 °F to 212 °F). The typical sample mount temperature is 90 °C. In some cases the sample mount will be set to ambient temperature to allow for condensation of water prior to entering the sample pathway.
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Contact a Teledyne Tekmar Customer Support Representative using the information in Section P.2 "Teledyne Tekmar Customer Support Center" prior to attempting the high temperature cleaning process. Chapter 4: Instrument Operations...
Desorb Ready Mode indicates that the trap has been loaded with VOCs and the Atomx XYZ is ready to desorb. If the GC is not ready, the Atomx XYZ will wait for the GC during this mode. While the Atomx XYZ is in this mode, there is no flow or heat through the trap;...
A typical desorb preheat temperature is 5 °C (41 °F) below the desorb temperature. The Atomx XYZ will hold in this mode for 0.33 min to ensure full heat transfer to the center of the trap. 4.3.5 Desorb Mode In desorb, the 6-port valve rotates to backflush analytes from the analytical trap to the GC.
Chapter 5: Maintenance and Troubleshooting 5.1 Maintenance Safety NOTE Caution and Warning Symbols are defined in Section P.5 "Atomx XYZ Safety Symbols Defined" and Section P.6 "Atomx XYZ Safety Labels". Les symboles d’Alerte et de Danger sont définis dans la section P.5 “Symboles Sécurité...
5.3 Preventative Maintenance Checks A carefully designed and faithfully executed Preventative Maintenance Program is the best method for maintaining the Atomx XYZ. Adherence to scheduled maintenance in the areas of cleaning, checking of parts, and lubrication will help continue the performance standards of the unit and decrease the possibility of down time.
Clean the autosampler according to the quarterly cleaning proce- dure. Refer to Section 5.17.2 "Quarterly Autosampler Cleaning". NOTE The Installation Kit Box includes most of the items needed for routine maintenance of the Atomx XYZ. Chapter 5: Maintenance and Troubleshooting 5 - 3 Atomx XYZ User Manual...
NOTE If Table 5-6 "GC I/O Cable and GC System Reference" does not contain your GC System, contact Teledyne Tekmar Customer Support using the contact information in Section 5.29 "Technical Assistance". Table 5-6 GC I/O Cable and GC System Reference...
Remove the Phillips screws from the side panel that is being removed. WARNING The Atomx XYZ is designed to keep liquid spills from coming in contact with electronics inside the unit. The Atomx XYZ access panels must be installed prior to turning the instrument ON.
Figure 5-2 Right Side of Atomx XYZ Right Access Panel Figure 5-3 Analytical Trap Compartment and Sparger Panel Open Moisture Control System (MCS) Resistance Temperature Detector (RTD) Heated Sample Mount Analytical Trap in Trap Heater Jacket Analytical Trap Compartment Sparger...
5.7 Plumbing Overview NOTE Also refer to Section A.3 "Atomx XYZ Plumbing Diagram". Figure 5-4 Plumbing Components 4-Way Tee 6-Port Valve Valve Manifold Sample Mount and Sparger Analytical Trap Moisture Control System Soil Valve Water Heater/Reservoir IS Pressure Regulator Syringe...
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Figure 5-5 Plumbing Components 6-Port Valve, MCS, and 4-Way Tee Carrier Gas Inlet Line/Heated Sample Transfer Line Valve Manifold Hot Water Heater/Reservoir Chapter 5: Maintenance and Troubleshooting 5 - 9 Atomx XYZ User Manual...
5.8 Electrical Overview NOTE Also refer to Section A.1 "Atomx XYZ Concentrator Electrical Schematic" and Section A.2 "Atomx XYZ Autosampler Electrical Schematic". Figure 5-6 Electrical Components Temperature Control Board CPU Comm Board 24VDC Power Supply 5VDC Power Supply Power Entry Module...
Locations of the boards are shown in Figure 5-7 and Figure 5-8. Diagrams of the boards are affixed to the interior of the instrument, as well as shown in relevant maintenance procedures. Figure 5-7 Printed Circuit Board Locations - Atomx XYZ Concentrator Temperature Control Board CPU Comm Board Internal Standard Valve Control Board...
I/O cable and USB Port for external communication to the controlling PC. Figure 5-9 CPU Communication Board (Master Board) Figure 5-10 CPU Communication Board Location CPU Comm Board Chapter 5: Maintenance and Troubleshooting 5 - 12 Atomx XYZ User Manual...
Figure 5-11 Multi-Channel Temperature Control Board Figure 5-12 Multi-Channel Temperature Control Board Multi-Channel Temperature Control Board Chapter 5: Maintenance and Troubleshooting 5 - 13 Atomx XYZ User Manual...
5.8.4 DC Valve Control Board The DC valve control board is located in the right side of the Atomx XYZ. This board controls all DC valve outputs. Figure 5-13 DC Valve Control Board Figure 5-14 DC Valve Control Board Location...
5.8.5 Internal Standard Valve Control Board The internal standard valve control board is located in the right side of the Atomx XYZ. This board controls all internal standard valve outputs. Figure 5-15 Internal Standard Valve Control Board Figure 5-16 Internal Standard Valve Control Board Location...
5.8.6 Banner Board/Status Light The banner board is located in the marquee panel of the Atomx XYZ. This board controls the status light. Figure 5-17 Banner Board Location Banner Board/Status Light Figure 5-18 Banner Board 5.8.7 XYZ Interface Board (XYZ) (Sidekick Board) The XYZ Interface Board (Sidekick Board) is the large board located under the other circuit boards.
The XYZ Input/Output Board (Generic Aux IO Board) is located on top of the XYZ Interface Board (Sidekick Board) in the rear, left-side of the compartment. It controls communications to and from the autosampler. Figure 5-21 XYZ Input/Output Board Chapter 5: Maintenance and Troubleshooting 5 - 17 Atomx XYZ User Manual...
5.8.11 Power Supplies 24VDC Power Supply The 24VDC power supply is located on the back wall of the right side of the Atomx XYZ. The 24VDC power supply is identified by its brown/orange wiring. This power supply powers motors and valves within the Atomx XYZ including the 6-port valve and solenoid valves.
5VDC Power Supply The 5VDC power supply is located on the back wall of the right side of the Atomx XYZ. The 5VDC power supply is identified by its black/red wiring. This power supply powers the status light and other boards within the Atomx XYZ (multi-channel temperature board, CPU communication board (master board), and DC valve control board, and XYZ main and interface boards).
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Figure 5-25 Begin Leak Check and Leak Check Indicating Failures Chapter 5: Maintenance and Troubleshooting 5 - 20 Atomx XYZ User Manual...
If the leak is in sub-system A the most like sources of the leak are: MFC outlet fitting COM Port of Bake Valve (B) NC Port of Purge Valve (A) COM Ports of Purge Select Valve (E) Chapter 5: Maintenance and Troubleshooting 5 - 22 Atomx XYZ User Manual...
Fittings of the Sample Needle COM, NO, and NC port of Soil Valve (F) Sample Vial not leak tight. The internal standard injection valve ports on the Valve Manifold. Chapter 5: Maintenance and Troubleshooting 5 - 24 Atomx XYZ User Manual...
Sample Mount fittings (Plug, Drain Line, Transfer Line). Eliminator Line if installed. Sample Mount to 4-Way Tee fittings Sample Mount weldments 6-Port Valve (cross-port leak, loose fitting, loose rotor) Chapter 5: Maintenance and Troubleshooting 5 - 26 Atomx XYZ User Manual...
Consult your laboratory’s Standard Operating Procedures (SOPs) for keeping glassware clean. In addition to your standard glassware protocol Teledyne Tekmar recommends the following: Only clean glassware with DI water and do not use soaps or cleaning products ...
3. The standard pressure will then be displayed as the system pressure, under the in the I . Click S again to return to normal ONES IELD NSTRUMENT TATUS ANEL operations. Chapter 5: Maintenance and Troubleshooting 5 - 29 Atomx XYZ User Manual...
4. Click Step and allow the system to record the pressure in the I NSTRUMENT ISTORY >V >I ). Normal operation of the OOLS ISTORY NSTRUMENT ISTORY instrument can then be resumed. Chapter 5: Maintenance and Troubleshooting 5 - 30 Atomx XYZ User Manual...
1/4” Open-ended wrench 5.12.2 Procedure 1. Power off the Atomx XYZ and remove the AC power cable from the back of the instrument. 2. Remove the protective cover over the sample needle. 3. Disconnect the tan purge gas tubing at the top of the needle. Next, use a 1/4”...
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7. Reinstall the protective cover over the sample needle. 8. Connect the AC power cord and turn the unit ON. 9. Start the Atomx XYZ TekLink software, if necessary. 10. Perform a leak check according to Section 5.9 "System Leak Check".
7/8” Open-ended Wrench Procedure Warning! Hot surface! Turn OFF power to the Atomx XYZ and remove the AC power line from the back of the instrument. Allow the sample mount and surrounding area to cool to room tem- perature.
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1. Power off the Atomx XYZ and remove the AC power cable from the back of the unit. Allow the sample mount and surrounding areas to cool. 2. Open the sparger panel door on the front of the Atomx XYZ.
Warning! Hot surface! The trap and surrounding areas can be extremely hot. Allow adequate time to cool. Warning! To avoid electrical shock turn OFF and unplug the Atomx XYZ before servicing. Chapter 5: Maintenance and Troubleshooting 5 - 35 Atomx XYZ User Manual...
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1. Power off the Atomx XYZ and remove the AC power cable from the back of the unit. Allow the sample mount, analytical trap and surrounding areas to cool. 2. Open the analytical trap compartment door. 3. Disconnect the trap heater and RTD plugs at the left side of the trap compartment.
UTTON IALOG 2. In the B , enter the recommended trap conditioning settings from the IALOG trap manufacturer. 3. Select the O to begin conditioning the trap. UTTON Chapter 5: Maintenance and Troubleshooting 5 - 37 Atomx XYZ User Manual...
. Select D from the E IAGNOSTICS CREEN LEVATOR and then select the M . Allow the elevator to move to ESTINATION UTTON the down position and stop. Chapter 5: Maintenance and Troubleshooting 5 - 38 Atomx XYZ User Manual...
It is especially important to clean up spills and remove contaminants, such as abrasives, from the autosampler’s moving parts. NOTE If a spill occurs, follow the appropriate laboratory-defined Standard Operating Procedure (SOP) to remove it from the autosampler. Chapter 5: Maintenance and Troubleshooting 5 - 39 Atomx XYZ User Manual...
5.17.1 Monthly Autosampler External Cleaning 1. Power off the Atomx XYZ and remove the AC power cable from the back of the unit. 2. Remove the autosampler vial rack and clean using a towel dampened with a lab-grade cleaning agent, followed by a towel dampened with clear water.
The X and Y-axis of the single alignment landmark of Zone 3, the sample vial cup, is then aligned using the probe and target and tested. Chapter 5: Maintenance and Troubleshooting 5 - 41 Atomx XYZ User Manual...
XYZ autosampler arm. 1. Ensure the autosampler vial rack is fully seated in the rack locater slots, and all vial positions, including the sample vial cup, are empty. Chapter 5: Maintenance and Troubleshooting 5 - 42 Atomx XYZ User Manual...
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UTTON OOLS CREEN TO UTOSAMPLER LIGNMENT IZARD Figure 5-36 Atomx XYZ TekLink Tools Screen and Align Autosampler Button 3. The A will be displayed and prepare for the UTOSAMPLER LIGNMENT IZARD alignment by disabling all current alignment corrections. When the wizard is ready for the alignment procedure, the N will be enabled.
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Use the C to close the gripper around the probe as LOSE RIPPER UTTON shown in Figure 5-39. Figure 5-38 Align Zone 1 - Gripper Controls Chapter 5: Maintenance and Troubleshooting 5 - 44 Atomx XYZ User Manual...
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5-41). Once the target is in place, click the OK B on the dialog. The probe will UTTON descend to a position just above the target (Figure 5-41). Figure 5-41 Align Zone 1 - Place Target Chapter 5: Maintenance and Troubleshooting 5 - 45 Atomx XYZ User Manual...
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Right-click on the field to decrease the distance, left-click to increase the distance. Figure 5-42 Probe Alignment Buttons Current Probe Coordinates Probe Left/Right Probe Up/Down and Forward Backward Chapter 5: Maintenance and Troubleshooting 5 - 46 Atomx XYZ User Manual...
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LIGNMENT . The wizard will calculate the correction values for Zone 1 and then apply UTTON them to the landmarks. Figure 5-45 Align Zone 1 - Test Alignment Chapter 5: Maintenance and Troubleshooting 5 - 47 Atomx XYZ User Manual...
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If the calculated value for one of the landmarks falls outside the bounds of the autosampler, an error notification will be displayed. Use the P REVIOUS ANDMARK to repeat the landmark alignments. UTTON Figure 5-48 Alignment Error Chapter 5: Maintenance and Troubleshooting 5 - 48 Atomx XYZ User Manual...
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The minimum uncorrected x, y position is 0, 0 and the maximum is 254.0, 360.0. If any of the aligned points are at the minimum or maximum, contact Teledyne Tekmar Customer Support using the contact information in Section P.2 "Teledyne Tekmar Customer Support Center"...
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1 and slowly lower it onto the vial. Once it detects the vial, it will raise the gripper all the way up and then back down on the vial. Figure 5-52 Z-Height Alignment Chapter 5: Maintenance and Troubleshooting 5 - 50 Atomx XYZ User Manual...
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EIGHTS UTTON Allow the wizard time to write the new parameters to the autosampler. Figure 5-55 Z-Height Alignment Complete for All Zones - Program All Zone Heights Chapter 5: Maintenance and Troubleshooting 5 - 51 Atomx XYZ User Manual...
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. The test will pick and place the vial to and from the following positions: UTTON Sample Cup, Position 84, Position 1, Position 77, Position 20 and Position 49. To only test specific zones select the buttons above the R UTTON Chapter 5: Maintenance and Troubleshooting 5 - 52 Atomx XYZ User Manual...
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Previous Button to re-align that zone. Once the zone is realigned, perform the Z-Height Alignment. 18. Click on the F to exit the A INISH UTTON UTOSAMPLER LIGNMENT IZARD Figure 5-59 Alignment Complete Chapter 5: Maintenance and Troubleshooting 5 - 53 Atomx XYZ User Manual...
Assistance". The PEM requires two IEC 5 x 20 mm fuses. To replace the fuses, follow the steps below. Fuses according to electrical standard are shown Table 5-9 "Atomx XYZ Fuse Ratings (2 IEC 5 x 20 mm Fuses)". Chapter 5: Maintenance and Troubleshooting...
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Warning! To avoid electrical shock turn OFF and unplug the Atomx XYZ before servicing. 1. Power off the Atomx XYZ and remove the AC power cable from the back of the unit. 2. Open the hinged fuse module cover by inserting a small flat-head screwdriver at the top, and then pulling the cover down.
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PEM as well as in Table 5-9 "Atomx XYZ Fuse Ratings (2 IEC 5 x 20 mm Fuses)". Fuses should be installed toward the rear of the module (toward the electrical contacts).
Atomx XYZ before servicing. 5.22.1 Main Fuse 1. Power off the Atomx XYZ and remove the AC power cable from the back of the unit. Remove the right access panel, and locate the Temperature Control Board. Figure 5-64 Multi-Channel Temperature Control Board...
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Figure 5-65 Multi-Channel Temperature Control Board Diagram - Main Fuse Main Fuse Chapter 5: Maintenance and Troubleshooting 5 - 58 Atomx XYZ User Manual...
8. Start the Atomx XYZ TekLink software, if necessary. 5.22.2 Heater Output Fuses 1. Power off the Atomx XYZ and remove the AC power cable from the back of the unit. Remove the right access panel, and locate the Temperature Control Board.
Figure 5-67 Multi-Channel Temperature Control Board Diagram - Heater Output Fuses Fuses 3. Remove the appropriate fuse by grasping it with a needle-nose pliers and pulling straight out. Chapter 5: Maintenance and Troubleshooting 5 - 60 Atomx XYZ User Manual...
5. Reinstall the right access panel. 6. Connect the AC power cord and turn the unit ON. 7. Start the Atomx XYZ TekLink software, if necessary. 5.23 Upgrade Concentrator Firmware First download the firmware and then install it according to the directions below.
Install The Firmware Update Utility Software 1. Insert the Atomx XYZ TekLink Installation Disc into the computer controlling the Atomx XYZ. When the disc menu is displayed, select and install the CETAC Field Programming Utility Software. Chapter 5: Maintenance and Troubleshooting...
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Autosampler Update Procedure 1. Power off the Atomx XYZ using the switch at the back of the instrument. 2. Remove the factory installed plug in the autosampler USB port (Figure 5-69). Figure 5-69 Plug Removed from Autosampler USB Port Autosampler USB Port 3.
The update process will take approximately 3 minutes. Once each step is complete, the dialog will indicate success with a check mark (Figure 5-72). Do not turn off the Atomx XYZ while the update is being installed!
UTTON CETAC Field Programming Utility. 10. Power off the Atomx XYZ and disconnect the USB cable from the computer and autosampler USB port. 11. Replace the plug in the autosampler USB port to prevent future inadvertent USB connection.
EQUENCE INDOW NOTE Make sure to give the Atomx XYZ the necessary time to complete the task. The results of the benchmark test can be printed at the completion of the test and are automatically saved in the I using the name entered at the...
Figure 5-74 Benchmark Test Prompt 4. As the benchmark test is conducted, Atomx XYZ TekLink will prompt the user for responses. Read the prompt and respond accordingly using the buttons in the ENCHMARK INDOW 5. Prior to completion of the test, Atomx XYZ TekLink will prompt if the benchmark test report should be printed.
5.26.2 No Power Flow Chart NOTE Refer to Section 5.21 "Power Entry Module (PEM) Fuse Replacement" for information on accessing the PEM fuses. Figure 5-75 No Power Flow Chart Chapter 5: Maintenance and Troubleshooting 5 - 68 Atomx XYZ User Manual...
5.27 Returning the Atomx XYZ Do not return the Atomx XYZ unless a Teledyne Tekmar Representative authorizes you to do so. A Customer Support Representative may be able to help you solve the problem over the telephone. If the instrument must be returned, the representative can tell you how to prevent damage during shipment.
A.4.13 Atomx XYZ Soils Flow Diagram - DI Transfer to Vial Figure A-16 Atomx XYZ - Soils Flow Diagram - DI Transfer to Vial Appendix A: Diagrams A - 17 Atomx XYZ User Manual...
Atomx XYZ User Manual Index Numerics Gas Requirements GC Communication 24VDC Power Supply 5-18 General Specifications 5VDC Power Supply 5-19 Guardian Foam Sensor and Foam Eliminator 1-24 6-Port Syringe Valve 1-15 1-23 Configure 2-25 Status and Manual Control 3-30 Heated Sample Transfer Line...
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Upgrade Concentrator Firmware 5-61 Concentrator Electrical Upgrade Firmware 3-30 Flow Upgrade Software 5-65 Plumbing User Interface Overview Dimensions Using Default Methods 3-35 Disposal Valves and Flows 3-28 of Parts 5-72 Version 3-27 Index I - 2 Atomx XYZ User Manual...
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ASX 7200 W-Axis Driver Board 5-18 Purge Gas Settings 3-21 Manual Movement 3-29 Requirements Environmental Specifications Gas Chromatograph Ethanol Carrier Gas Connection to Atomx XYZ 2-11 Carrier Gas Inlet 1-20 Communication Configure Type 3-21 Fans GC I/O Cable and GC Type Reference Manual Control...
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4-10 Instrument Access Panels Purge Ready Internal Standard Vessel Pressure Optimization Verifying and Setting 5-29 Sample Pre-Heat Time Leak Check 5-19 Sample Temperature Monthly Maintenance Checks Screen Multi-Channel Temperature Control PCB Standby Index I - 4 Atomx XYZ User Manual...
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Temperature and Pre-Heat Time Trapping, Adsorption, Desorption Pre-Purge Purge Tab Optimization Purge 4-10 Purge Ready Replacement Parts Sample Temperature Replacing Parts Standby Returning the Atomx XYZ 5-72 Flow Run Schedule 3-43 Temperature Safety Parameters Atomx XYZ Methanol Extraction 4-14 Safety Labeling...
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