Teledyne Tekmar 15-3200-074 Manuals

Manuals and User Guides for Teledyne Tekmar 15-3200-074. We have 1 Teledyne Tekmar 15-3200-074 manual available for free PDF download: User Manual

Teledyne Tekmar 15-3200-074 User Manual

Teledyne Tekmar 15-3200-074 User Manual (244 pages)

Brand: Teledyne Tekmar | Category: Laboratory Equipment | Size: 84 MB

Table of Contents

Table of Contents
3
Essential Instructions
13
Teledyne Tekmar Customer Support Center
13
Warranty
13
Notations and Hazard Severity Levels
14
Atomx XYZ Safety Symbols Defined
15
Atomx XYZ Safety Labels
17
Working Safely
20
CE Mark
21
Explanation of Regulatory Marks
21
Unit Disposal
21
Chapter 1: Introduction

23
- Atomx XYZ with Methanol Extractions Overview
  23
- Purge and Trap Background
  23
- Purge and Trap Fundamentals
  23
- Brief History
  24
- Purge and Trap Operation Overview
  24
- Headspace Equilibrium Diagram
  25
- Trapping, Adsorption and Desorption
  26
- Atomx XYZ Specifications
  27
- General Specifications
  27
- Performance Specifications
  28
- Sample Needle
  29
- Liquid Samples
  29
- Low-Level Solid Samples
  29
- High-Level Solid Samples
  29
- Internal Standard Injection
  30
- Sample Gas Handling and Requirements
  30
- Electrical Requirements
  31
- Atomx XYZ Component Overview
  33
- Sample Mount and Sparger
  35
- Vials
  35
- Internal Standard Pressure Regulator
  36
- Internal Standard Vessels
  36
- Syringe Drive with Sweepable 25 Ml Syringe
  37
- Sample Needle
  37
- XYZ Autosampler Pick and Place Assembly
  38
- Elevator
  38
- Elevator and Sample Vial Cup
  38
- Vial Mixer Assembly
  39
- Status Light
  39
- Vial Mixer
  39
- Unit Status Light
  39
- Sample Purge Gas Inlet
  40
- Mass Flow Controller (MFC)
  40
- Sample Pathway
  40
- Analytical Trap
  41
- Moisture Control System (MCS)
  41
- Carrier Gas Inlet Line/Heated Sample Transfer Line
  42
- Carrier Gas Inlet Line and Heated Sample Transfer Line
  42
- Valving
  43
- Heated 6-Port Valve
  44
- Soil Valve
  44
- Optional Accessories
  45
- Sparge Vessel Heater
  45
- 6-Port Syringe Valve
  45
- Vial Chiller Plate
  46
- Guardian Foam Sensor and Eliminator
  46
Chapter 2: Installation and Setup

47
Chapter 3: Atomx XYZ Teklink Software Overview

75
- About Atomx XYZ Teklink Software
  75
- The Atomx XYZ Teklink Software Environment
  75
- Touchscreen Capability
  75
- Pinnable" Screens
  76
- Title Bar
  76
- Schedules Screen Title Bar
  76
- Open, Save, Load, and Print Buttons
  77
- Instrument Control Buttons
  77
- Control Buttons
  77
- Delete at Next Archive Check-Box
  78
- Delete at Next Archive Check-Box - Schedule Screen
  78
- Open Schedule Dialog Source Drop-Down Menu
  78
- Primary Screens
  79
- The Home Screen
  79
- Home Screen
  79
- Instrument Status Panel
  80
- Methods Screen
  81
- Standby Tab
  81
- Purge Tab
  82
- Soil Methods Screen - Purge Tab
  84
- Methanol Extraction Methods Screen - Purge Tab
  85
- Desorb Tab
  86
- Bake Tab
  87
- Water Methods Screen - Bake Tab
  87
- Schedules Screen
  88
- Methanol Methods Screen - Bake Tab
  88
- Tools Screen
  90
- Prime Menu
  91
- Commands Menu
  91
- System Menu
  94
- Leak Check Dialog
  96
- System Properties Dialog
  97
- System Properties - Data Tab
  98
- About Dialog
  101
- Diagnostics
  102
- Arm/Elevator
  103
- Pumper Diagnostics
  104
- Upgrade Firmware Dialog
  104
- Benchmark Test
  105
- Upgrade Firmware Dialog
  105
- Add, Connect and Deactivate an Instrument Profile
  106
- Add an Instrument Profile and Connect
  106
- Options Tab
  107
- Deactivate an Instrument Profile
  108
- Leak Check Tab
  108
- Using the Methods Screen
  109
- Methods Types
  109
- Default Methods
  109
- Configuration Dialog Showing Current Instrument Profile
  109
- Open a Method
  110
- Creating a Custom Method
  110
- Choose Method Type
  110
- Load the Method
  113
- Print a Method
  113
- Using the Schedule Screen
  113
- Open Schedule
  113
- Create a Schedule
  113
- Schedules Screen - Blank Schedule
  113
- Schedules Screen Right-Click Options
  114
- Select Method Dialog
  115
- Sample ID Column
  115
- Save Schedule
  116
- Select Standard Drop-Down
  116
- Print Schedule
  117
- Load (Run) the Schedule
  117
- Step Schedule
  118
- Hold Schedule
  118
- Schedule Hold - Instrument Status Panel
  118
- Abort a Sample or Schedule
  119
- Completion of the Schedule
  119
- Data Storage Location and Archiving Data
  120
- System Properties - Data Tab
  120
Chapter 4: Instrument Operations

121
- Atomx XYZ Mode Descriptions
  121
- Atomx XYZ Valve Output/Mechanism Chart
  123
- Waters
  123
- Soils
  125
- Methanol Extraction
  126
- Optimization/Method Development
  128
- Purge Mode
  130
- Dry Purge Mode
  130
- Desorb Ready Mode
  130
- Desorb Pre-Heat Mode
  130
- Desorb Mode
  131
- Bake Mode
  131
- Method Parameters
  132
- Water
  132
- Soil
  133
- Methanol Extraction
  134
- Analytical Trap Recommended Operating Conditions
  135
Chapter 5: Maintenance and Troubleshooting

137
- Maintenance Safety
  137
- Replacing Parts
  137
- Preventative Maintenance Checks
  138
- Daily Maintenance Checks
  138
- Weekly Maintenance Checks
  138
- Monthly Maintenance Checks
  139
- Quarterly Maintenance Checks
  139
- Preventative Maintenance Chart
  140
- GC In/Out (I/O) Cable and GC Type Reference
  141
- Instrument Access Panels
  142
- Front of the Atomx XYZ
  142
- Right Side of Atomx XYZ
  143
- Analytical Trap Compartment and Sparger Panel Open
  143
- Plumbing Overview
  144
- Plumbing Components
  144
- Electrical Overview
  146
- Printed Circuit Boards
  146
- Printed Circuit Board Locations - Atomx XYZ Concentrator
  147
- Printed Circuit Board Locations - Autosampler
  147
- CPU Communication Board (Master Board)
  148
- Multi-Channel Temperature Control Board
  149
- DC Valve Control Board
  150
- Internal Standard Valve Control Board
  151
- Banner Board/Status Light
  152
- XYZ Interface Board (XYZ) (Sidekick Board)
  152
- XYZ Control Board (Incrediboard)
  153
- XYZ Input/Output Board (Generic Aux IO Board)
  153
- Elevator Drive Board (ASX 7200 W-Axis Driver Board)
  154
- Power Supplies
  154
- System Leak Check
  155
- System Leak Check Flow Diagram
  157
- Leak Check Failed - Check Sub-System a
  158
- Sub-System a Leak Check Flow Diagram
  159
- Leak Check Failed - Check Sub-System B
  160
- Sub-System B Leak Check Flow Diagram
  161
- Leak Check Failed - Check Sub-System C
  162
- Sub-System C Leak Check Flow Diagram
  163
- Leak Check Failed - All Sub-Systems Checked and Passed
  164
- Glassware Good Practices Cleaning Procedures
  164
- Sparger Cleaning
  164
- Verifying/Setting Internal Standard Vessel Pressure
  165
- Verify the Internal Standard Vessel Pressure
  165
- Setting the Internal Standard Vessel Pressure
  166
- Sample Needle Replacement
  167
- Tools and Supplies
  167
- Procedure
  167
- Sparger Replacement
  169
- Analytical Trap Replacement
  171
- Analytical Trap Conditioning
  173
- Analytical Trap Recommended Conditioning Settings
  173
- Procedure
  173
- Elevator Lubrication
  174
- Tools and Supplies
  174
- Procedure
  174
- XYZ Autosampler Cleaning Procedure
  175
- Monthly Autosampler External Cleaning
  176
- Quarterly Autosampler Cleaning
  176
- XYZ Autosampler Alignment
  176
- When Is Alignment Needed
  177
- Alignment Overview
  177
- Tools and Supplies
  178
- Procedure
  178
- Syringe Initialization
  190
- Syringe Replacement
  190
- Power Entry Module (PEM) Fuse Replacement
  190
- Multi-Channel Temperature Control Board Fuse Replacement
  193
- Main Fuse
  193
- Multi-Channel Temperature Control Board
  193
- Heater Output Fuses
  195
- Diagram - Heater Output Fuses
  196
- Upgrade Concentrator Firmware
  197
- Download Firmware
  197
- Upgrade Board Firmware
  198
- Upgrade Autosampler Firmware
  198
- File Selected
  200
- Upgrade Atomx XYZ Teklink Software
  201
- Troubleshooting
  202
- Benchmark Test
  202
- Benchmark Test
  203
- No Power Flow Chart
  204
- No Response Flow Chart
  205
- Low Response Flow Chart
  206
- Carryover Contamination Flow Chart
  207
- Returning the Atomx XYZ
  208
- Prepare for Shipment Function
  208
- Unit and Parts Disposal
  208
- Technical Assistance
  208
- Teledyne Tekmar Customer Support
  208
Appendix A: Diagrams

209

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