Related Manuals for Organomation MULTIVAP 11809
Summary of Contents for Organomation MULTIVAP 11809
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Page 1: Installation
MULTIVAP Nitrogen Evaporation System Model 118 DIGITAL & TIME CONTROL SYSTEM INSTRUCTION MANUAL RGANOMATION SSOCIATES 266 RIVER ROAD WEST BERLIN, MA 01503 U. S. A. Tel: 888-838-7300 Fax: 978-838-2786... -
Page 3: Table Of Contents
Maintenance and Cleaning Trouble Shooting Technical Information Parts List Service and Returns Shipping - Claims for damage or shortage Specifications Wiring Diagrams Contacting Organomation and its Representatives Product designs are subject to change without notice Printed in U. S. A. V15.1... -
Page 4: Introduction
Retain all cartons and packaging materials until all components have been checked against the packing slip, the component list below, and the equipment has been assembled and tested. Contact Organomation immediately if any damage or discrepancies are found. - Page 5 MULTIVAP 118 INTRODUCTION Option Codes and additional items shipped The following list contains option codes and items which may have been shipped in conjunction with the standard parts shown on the previous page. Please check your packing list and order information carefully to determine if these items are included in your shipment. Your shipment may contain the following optional items: Option Description...
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Page 6: Instrument Description
MULTIVAP 118 INTRODUCTION Instrument Description The MULTIVAP Nitrogen Evaporation System is designed for general evaporation and / or concentration of analytical or biological samples in test tube based glassware under controlled and reproducible conditions. The complete instrument is shown below. Figure 1 V15.1 - 6 -... -
Page 7: Parts List
MULTIVAP 118 INTRODUCTION PARTS LIST Description Item Part Name Cat # Hoist Assembly P1224-M Assists lifting of instrument. Delivers gas to manifold. Toggle Gas Valve P1303 On/Off gas control for each manifold row. Lift Knob P0612-N Rotate to raise and lower manifold. Blunt Needle NA0603 Delivers gas to each sample. -
Page 8: Location
MULTIVAP 118 INSTALLATION Location The MULTIVAP Evaporator System should be located on a bench top or in a chemical fume hood if hazardous or flammable materials and solvents are to be used. The location should provide the necessary support services for the instrument. These include electrical power (required for dry block) and a clean inert gas source (Air or Nitrogen). - Page 9 MULTIVAP 118 INSTALLATION Dry Bath Setup (Continued) If you do not have this option, Type-Z Purge Intrinsically Safe Bath option - please proceed to the next section. Procedures for operating this system may be found in the Operation Section. Quick start instructions are posted on the front of the bath. Please refer to Figure 3 below for parts list and installation.
- Page 10 MULTIVAP 118 INSTALLATION Dry Bath Setup (Continued) Connect the black connector tube to the lower left connector on the rear of the unit labeled GAS INPUT. Connect the other end to a suitable gas source. Pressure Control is standard on all MULTIVAPs. This item is pre-installed onto the top of the bath box.
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Page 11: Instrument Setup
MULTIVAP 118 INSTALLATION Instrument Setup Install the two 5/8” DIA SS Tubes into the fittings located on either side of the bath chamber. Tighten the compression screws. Place the manifold over the tops of the two 5/8” SS tubes and slide the manifold downwards until 2 inches (50mm) of the tube extend above the manifold. - Page 12 MULTIVAP 118 INSTALLATION Instrument Setup (Continued) Needles and Pipets - SS Luer Lock Needles are supplied with the standard MULTIVAP system. Optional Pasteur Pipet Adapters allow the use of glass pipets. These fittings replace SS Needles on the MULTIVAP. Pasteur Pipet Adapters may be purchased separately with the standard MULTIVAP, allowing the use of both needles and pipets.
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Page 13: Safety Considerations - Read Before Operation
This equipment should not be modified or altered. Organomation assumes no liability for any misuse of or modification to this product and such misuse or modification will immediately void all warranties. -
Page 14: Operation
MULTIVAP 118 OPERATION Instrument Controls - Main Control Panel Digital Controller - Controls bath temperature Timer Controller - Controls timed functions when selected. Used for bath preheat or automated control of services. Time Switch - Starts or resets timed operation, momentary switch. Heat Switch - Selects manual or timed control of heat system. - Page 15 MULTIVAP 118 OPERATION Type Z-Purge Bath Operation - Optional What It Does The Type-Z Purged system prevents ignition of flammable materials caused by contact with electrical components inside the heating unit. How It Works The concept behind this purge system is to create a small positive pressure gradient inside the bath case.
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Page 16: Planning And Preparation
Under no circumstances should this equipment be used with materials capable of auto ignition below 150 Degrees Centigrade including materials containing peroxides. Please Contact Organomation Associates Technical Support if you have any questions concerning the use of TYPE-Z Purged equipment or questionable materials in OAI equipment. -
Page 17: Bath Operation
MULTIVAP 118 OPERATION Bath Operation Press the reset button on the GFCI (if present). Turn the bath rocker switch on. Digital Electronic Control - Adjust the digital controller to the desired temperature set point. The controller set point may be adjusted by depressing the “*” on the front panel and depressing the up or down arrow keys to the desired temperature. - Page 18 MULTIVAP 118 OPERATION Bath Operation Timed Gas and Heat Control The Time control system allows several operating modes which can be set for different operations. The timer may be used to preheat the bath in the morning prior to use, to shut down the system after a specific period of time (unattended operation), or for non- dryness endpoint operations.
- Page 19 MULTIVAP 118 OPERATION Bath Operation (continued) Timed Gas and Heat Control (Continued) Automatic shutdown of gas or heat services - unattended operation To shut down the bath services after a period of time during a sample evaporative run, ideal when each sample is to be taken to dryness and the operator will not be present at the completion of the run.
- Page 20 MULTIVAP 118 OPERATION Bath Operation (continued) Timed Gas and Heat Control (Continued) Non-dryness automated endpoint - unattended operation The MULTIVAP system may be used for timed non-dryness endpoint evaporation. In order for this operation to be successful the following parameters must be maintained. Test Tube Size - All tubes must be the same size Sample Volume -...
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Page 21: Instrument Operation
MULTIVAP 118 OPERATION Instrument Operation Turn on the heating and gas control system. Adjust the digital temperature control to the desired temperature. For samples which are not heat sensitive, adjust the controller to a temperature which is two degrees below the boiling point of the sample. -
Page 22: Optimization
When the evaporation is complete, turn off the heating unit and gas flow. Raise the manifold to its highest position The unit may now be recalibrated and loaded for another run. Additional inserts for different glassware sizes are available from Organomation. Gas Flow Chart 14 ga Needles... -
Page 23: Maintenance And Cleaning
MULTIVAP 118 MAINTENANCE Maintenance and Cleaning The MULTIVAP Evaporation system is manufactured from extremely durable materials and may last for years if operated and maintained properly. The following guidelines are recommended for use with MULTIVAP systems. Instrument & Bath - The anodized aluminum components may be cleaned with a non-abrasive scouring pad followed by damp cloth wipe with clean water. -
Page 24: Troubleshooting
MULTIVAP 118 TROUBLESHOOTING SYMPTOMS CAUSES SOLUTIONS No Power to bath. Electrical outlet not energized. Energize electrical outlet. Bath power cord not plugged in. Plug in bath power cord. GFCI not reset. Reset switch on GFCI. Internal electrical fault. Contact OAI for instructions. Improper control setting Check temperature setting Bath does not heat. -
Page 25: Wiring Diagrams
MULTIVAP 118 WIRING DIAGRAMS POWER CORD 120 VOLT TIMER OCTAL NEUT. PIN BASE ON / OFF SWITCH SOLENOID DIGITAL CONTROLLER 1 2 3 4 5 6 7 8 SOLID STATE RELAY HIGH TEMPERATURE RED ALERT LIGHT PROTECTION SWITCH GREEN TIME LIGHT AMBER GAS LIGHT AMBER HEAT LIGHT MOMENTARY TIME SWITCH... - Page 26 MULTIVAP 118 WIRING DIAGRAMS POWER CORD 240 VOLT TIMER OCTAL NEUT. PIN BASE ON / OFF SWITCH SOLENOID DIGITAL CONTROLLER 1 2 3 4 5 6 7 8 SOLID STATE RELAY HIGH TEMPERATURE RED ALERT LIGHT PROTECTION SWITCH GREEN TIME LIGHT AMBER GAS LIGHT AMBER HEAT LIGHT MOMENTARY TIME SWITCH...
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Page 27: Service And Returns
MULTIVAP 118 TECHNICAL INFORMATION Service and Returns In the event a product purchased from Organomation needs service or must be returned please follow the outlined procedures below. Contact Organomation Technical Support Department Before returning any product to Organomation Associates for any reason, please contact the Technical Support Department, toll free at 888-838-7300 or at sales@organomation.com. -
Page 28: Shipping - Claims For Damage Or Shortage
Contact Organomation immediately at 888-838-7300 or sales@organomation.com If a damaged item needs to be replaced, Organomation will send this item under warranty at no charge. The damaged item must be returned to Organomation. Please follow the instructions listed in the Service and Returns section. Important - items not returned or which are further damaged or destroyed in transit are the responsibility of the customer and will be billable. -
Page 29: Specifications
MULTIVAP 118 TECHNICAL INFORMATION Specifications Electrical Requirements: 120 or 240 VAC single phase, 50 - 60 Hz. 3 wire grounded outlet required. GFCI (Ground Fault Circuit Interrupter) optional. Heating system 600 W* * 240V units divide wattage by 2. Optional EC compliance EN55014. Electrical Compliance's: (as marked on bath) none... - Page 30 EC Declaration of Conformity Revised January 3, 2003 We, Organomation Associates Inc a corporation registered in Massachusetts, United States of America, declare under sole responsibility that the following equipment to which this declaration relates, meets the principal protection requirements and is in conformity with relevant sections of the applicable EC standards and other normative documents.