Table of Contents
Related Manuals for Organomation S-EVAP 12060
Summary of Contents for Organomation S-EVAP 12060
- Page 1 S-EVAP-RB Solvent Evaporation System Model 12060, 12090 & 12008 Digital Time and Control System INSTRUCTION MANUAL RGANOMATION SSOCIATES 266 RIVER ROAD WEST BERLIN, MA 01503 U. S. A. Tel: 888-838-7300 Fax: 978-838-2786...
-
Page 3: Table Of Contents
Optimization Maintenance and Cleaning Trouble Shooting Technical Information Service and Returns Shipping - Claims for damage or shortage Specifications Wiring Diagrams Contacting Organomation and its Representatives Product designs are subject to change without notice Printed in U. S. A. V15.1... -
Page 4: Introduction
Retain all cartons and packaging materials until all components have been checked against the packing slip, the component list below, and the equipment has been assembled and tested. Contact Organomation Associates Inc. immediately if any damage or discrepancies are found. -
Page 5: Glassware Sets
INTRODUCTION S-EVAP-RB Cat # Glassware Sets - Each Set includes the following: GS2161 125 ML Glassware Set, includes: GP3215 (Quantity 2): Standard flat bottom flask 125 ml, for 24/40 joint GP2212: Hopkins condenser 375mm with side arm for individual collection flask, for 24/40 joint ... - Page 6 S-EVAP-RB INTRODUCTION Option Codes and additional items shipped The following list contains option codes and items which may have been shipped in conjunction with the standard parts shown on the previous pages. Please check your packing list and order information carefully to determine if these items are included in your shipment. Your shipment may contain the following optional items: Option Description...
-
Page 7: Instrument Description
S-EVAP-RB INTRODUCTION Instrument Description The S-EVAP-RB Solvent Evaporation System is designed for general evaporation and / concentration of analytical or environmental samples in a variety of glassware configurations to meet the needs of specific methods under controlled and reproducible conditions. The S-EVAP-RB system features rapid solvent evaporation with solvent vapor recovery. -
Page 8: Installation
S-EVAP-RB INSTALLATION Location The S-EVAP-RB evaporator system should be located on a bench top or in a chemical fume hood if hazardous or flammable materials and solvents are to be used. The location should provide the necessary support services for the instrument. These include electrical power (required for water bath), cold water, and drain. -
Page 9: Type Z Purge Intrinsically Safe Bath Option
S-EVAP-RB INSTALLATION Bath Setup (Continued) Type-Z Purge Intrinsically Safe Bath option - If you do not have this option, please proceed to the next section. Procedur es for operating this system may be found in the Operation Section. Quick start instructions are posted on the front of the bath. Please refer to Figure 2 below for parts list and installation. - Page 10 Connect the clear 1/4” ID x 3/8” OD tube to a cold water source (tap or chiller). Source should be capable of producing 3.5 LPM (1 GPM) and being regulated to 30 psig maximum. If the source is in excess of 30 psig, then Organomation part # XA0631 Pressure Reducing Regulator will be required. Figure 3 V15.1...
- Page 11 S-EVAP-RB INSTALLATION Bath Setup (Continued) Pressure Reducing Regulator Option - If you do not have this option, proceed to the next section. When purchased with an S-EVAP System, this item is pre-installed onto the flow meter, between the flow meter and the Connector Tube. Refer to Figure 4. Remove the flow meter from the bracket.
- Page 12 S-EVAP-RB INSTALLATION WATER SERVICES TUBE ASSEMBLY ROTATING MANIFOLD CONDENSER HOLDER / WATER EXTENDABLE MANIFOLD ASSEMBLY AND CONDENSATION CENTER TUBE NOT SHOWN TUBE 3/8” SS INLET TUBE 1/2” PVC DRAIN TUBE S-EVAP BATH FLOWMETER CONTROL BOX Figure 5 V15.1 - 12 -...
-
Page 13: Instrument Setup
S-EVAP-RB INSTALLATION Instrument Setup Place the instrument and stand into the water bath or on a flat level surface. The stand is loose relative to the instrument and must be held in place while placing the assembly into position. Place the cover disk assembly onto the instrument. Slide the disk upwards 5” and secure in place with the set screws in the disk collar. - Page 14 Connect the drain tube at the bottom of the services tube to a suitable drain or chiller system. Chiller systems purchased from Organomation have the proper connection fittings provided, please reference the water chiller instructions for proper chiller connections.
- Page 15 S-EVAP system. Care and caution should be exercised relative to these instructions and in operation of non Organomation glassware in the S-EVAP system. Condenser Glassware Setup Procedures – The following procedures cover setup and installation of Organomation glassware in the S-EVAP instrument.
- Page 16 Position the round flask into each position on the S-EVAP cover disk. Turn on the condenser water and fill the condensers. Condensers should fill from the bottom. Rotate the unit and check all connections for leaks. If you encounter difficulties, contact the Organomation technical department. V15.1 - 16 -...
-
Page 17: Instrument Control Identification
S-EVAP-RB INSTALLATION Instrument Controls – Analog Water Bath System Toggle Switch - Located on the front right bath label. Turns power to the bath on and off. Thermostat Knob - Located on the front center bath label. Adjusts the bath temperature. -
Page 18: Safety Considerations - Read Before Operation
This equipment should not be modified or altered. Organomation assumes no liability for any misuse of or modification to this product and such misuse or modification will immediately void all warranties. -
Page 19: Operation
Under no circumstances should this equipment be used with materials capable of auto ignition below 150 Degrees Centigrade including materials containing peroxides. Please Contact Organomation Associates Technical Support if you have any questions concerning the use of TYPE-Z Purged equipment or questionable materials in OAI equipment. -
Page 20: Bath Operation
S-EVAP-RB OPERATION Bath Operation Press the reset button on the GFCI (if present). Check bath water level, fill if necessary. Analog Water Bath Systems Turn the bath toggle switch on. Thermostat Control - Adjust the bath thermostat to the desired temperature. S-EVAP water bath maximum temperature is 100 ºC. - Page 21 OPERATION S-EVAP-RB Bath Operation (Digital Control Box Systems – Continued) Timed Heat Control The time control system allows several operating modes which can be set for different operations. The timer may be used to preheat the bath in the morning prior to use, to shut down the system after a specific period of time (unattended operation), or for non-dryness end point operations.
- Page 22 S-EVAP-RB OPERATION Bath Operation (Digital Control Box Systems – Continued) Automatic shutdown of heat services - unattended operation To shut down the bath services after a period of time during a sample evaporative run, ideal when each sample is to be taken to dryness and the operator will not be present at the completion of the run.
-
Page 23: Optimization
S-EVAP-RB OPERATION Bath Operation (Digital Control Box Systems – Continued) Non-dryness automated endpoint - unattended operation The S-EVAP system my be used for timed non-dryness endpoint evaporation. In order for this operation to be successful the following parameters must be maintained. Flask Size - All flasks must be the same size Sample Volume -... - Page 24 S-EVAP-RB OPERATION Type Z-Purge Bath Operation - Optional What It Does The Type-Z Purged system prevents ignition of flammable materials caused by contact with electrical components inside the heating unit. How It Works The concept behind this purge system is to create a small positive pressure gradient inside the bath case.
-
Page 25: Instrument Operation
S-EVAP-RB OPERATION Instrument Operation Turn on the condenser water system. Adjust the condenser water flow to a minimum of 2500 CCM for eight positions. When operating with less than eight condensers in place and connected, the flow may be adjusted downwards. Minimum flow for one condenser installed is 1000 CCM. -
Page 26: Maintenance And Cleaning
S-EVAP-RB MAINTENANCE Maintenance and Cleaning The S-EVAP Evaporation system is manufactured from extremely durable materials and may last for years if operated and maintained properly. The following guidelines are recommended for use with all S-EVAP systems. Heating Media - Tap water, distilled water, de-ionized water, and bath heating oils may be used. - Page 27 Reference your Material Safety Data Sheets (MSDS) for instructions on proper cleanup and handling procedures. Contact Organomation Technical Department at (978) 838-7300 concerning any issue regarding decontamination and / or for alternative cleaning procedures. V15.1...
-
Page 28: Troubleshooting
S-EVAP-RB TROUBLESHOOTING SYMPTOMS CAUSES SOLUTIONS No Power to bath. Electrical outlet not energized. Energize electrical outlet. Bath power cord not plugged in. Plug in bath power cord. Internal electrical fault. Contact factory for instructions. Bath does not heat. Bad wire connection. Bath will require service, contact (heat light is on) Defective high temperature... -
Page 29: Technical Information
S-EVAP-RB TECHNICAL INFORMATION Service and Returns In the event a product purchased from Organomation needs service or must be returned please follow the outlined procedures below. Contact Organomation Technical Support Department Before returning any product to Organomation Associates for any reason, please contact the Technical Support Department, toll free at 888-838-7300 or email sales@organomation.com. -
Page 30: Shipping - Claims For Damage Or Shortage
TECHNICAL INFORMATION Shipping - Claims for damage and shortage Organomation makes a sincere effort to ensure your purchase is properly packed and all items listed on the packing slip are in fact enclosed with the shipment. In the event that your purchase is damaged or if any items are missing, please follow the procedures below. -
Page 31: Specifications
S-EVAP-RB TECHNICAL INFORMATION Specifications (includes available options) Environmental: Humidity 0-90%, Temperature 5-40°C, Indoor use only. Elevation up to 3000 Meters. Electrical Requirements: 120 or 240 VAC single phase, non-switchable, 50 - 60 Hz., 3 wire grounded outlet required. Model 12060 Bath 1100W Models 12090 &... -
Page 32: Wiring Diagrams
WIRING DIAGRAMS 120V S-EVAP-RB NEUT. TIMER - OCTAL PIN BASE POWER CORD GROUND WIRE BATH CASE TO CONTROL CASE SOLENOID DIGITAL CONTROLLER 1 2 3 4 5 6 7 8 SOLID STATE RELAY HIGH TEMPERATURE RED ALERT LIGHT PROTECTION SWITCH GREEN TIME LIGHT AMBER HEAT LIGHT BATH HEATER... - Page 33 WIRING DIAGRAMS 240V S-EVAP-RB NEUT. TIMER - OCTAL PIN BASE POWER CORD GROUND WIRE BATH CASE TO CONTROL CASE SOLENOID DIGITAL CONTROLLER 1 2 3 4 5 6 7 8 SOLID STATE RELAY HIGH TEMPERATURE RED ALERT LIGHT PROTECTION SWITCH GREEN TIME LIGHT AMBER HEAT LIGHT AMBER GAS LIGHT...
- Page 34 EC Declaration of Conformity Revised January 3, 2003 We, Organomation Associates Inc a corporation registered in Massachusetts, United States of America, declare under sole responsibility that the following equipment to which this declaration relates, meets the principal protection requirements and is in conformity with relevant sections of the applicable EC standards and other normative documents.