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Summary of Contents for EL-CELL ECC-Opto-Std-Aqu
- Page 1 User Manual Release 1.56 ECC-Opto-Std-Aqu Electrochemical test cell © 2020 EL-Cell GmbH...
- Page 2 The information in this manual has been carefully checked and believed to be accurate; however, no responsibility is assumed for inaccuracies. EL-Cell GmbH maintains the right to make changes without further notice to products described in this manual to improve reliability, function, or design. EL -Cell GmbH does not assume any liability arising from the use or application of this product.
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Page 3: Table Of Contents
2 Features ................................5 3 Safety precautions............................7 4 Assembly and connection ........................... 7 5 Disassembly and Cleaning .......................... 9 6 Windows for ECC-Opto-Std-Aqu ......................9 7 Cell holders ..............................11 8 Unpacking..............................13 9 Technical data .............................. 14 10 Spare parts ..............................15 ECC-Opto-Std-Aqu test cell .......................... -
Page 4: Product Description
ECC-Opto-Std-Aqu 1 Product description The ECC-Opto-Std-Aqu test cell is a version of the ECC-Opto-Std test cell specialized to highly corrosive aqueous and non-lithium aprotic electrolytes. For this purpose, current collectors are made of gold (optional nickel or platinum) replacing stainless steel. One restriction must be noted: Gold current collectors are not fully compatible with aprotic lithium based electrolytes, as lithium may alloy with gold at very low potentials. -
Page 5: Features
User Manual ECC-Opto-Std-Aqu 2 Features 2- and 3-electrode cell with optical window for highly corrosive aqueous and non-lithium aprotic electrochemistry. Materials in media contact are gold, PEEK and EPDM In the standard sandwich set-up, the backside of the disc-shaped working electrode ... - Page 6 User Manual ECC-Opto-Std-Aqu Working principle of the ECC-Opto-Std-Aqu (shown for the sandwich set-up): Inspection area (2 mm, optional up to 10 mm) Working electrode material (WE) placed on the holed current collector Optical window Holed current collector 16 mm Spring loaded...
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Page 7: Safety Precautions
User Manual ECC-Opto-Std-Aqu 3 Safety precautions Use proper safety precautions when using hazardous electrode materials and electrolytes. Wear protective glasses and gloves to protect you against electrolyte that may accidentally spill out during filling and disassembly. Upon cell disassembly, dispose al l materials properly. - Page 8 User Manual ECC-Opto-Std-Aqu 12. Fill the cell with electrolyte (e.g. 3 sulfuric acid) according to the following procedure: Connect the provided transfer line to port B. Charge a 5 ml syringe with ca. 0.2 ml of electrolyte. NOTE: We recommend single-use PP plastic syringes with low friction silicone pistons.
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Page 9: Disassembly And Cleaning
Wear appropriate protection equipment, goggles and gloves. Clean all cell parts right after disassembly. Leaving cell parts in contact with ambient atmosphere while still being wetted with electrolyte may result in severe corrosion. 6 Windows for ECC-Opto-Std-Aqu ECC-Opto Borosilicate glass window (standard) List of Components: Glass window (1 pc, 22 x 0.3 mm) - Page 10 User Manual ECC-Opto-Std-Aqu ECC-Opto Beryllium window kit II ECC1-00-0156-F List of Components: Beryllium window (1 pc, 22 x 0.2 mm) ECC1-00-0222-A Lid (1 pc) ECC1-00-0127-M ECC-Opto Polyimide window kit: ECC1-00-0156-F List of Components: 1. Polyimide (Cirlex) window (3 pcs, 22 x 0.23 mm) ECC1-00-0250-A 2.
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Page 11: Cell Holders
User Manual ECC-Opto-Std-Aqu ECC-Opto Sapphire window kit: ECC1-00-0156-C List of Components: Sapphire window (1 pc, 22 x 0.3 mm) ECC1-00-0149-A Lid (1 pc) ECC1-00-0127-B ECC-Opto Polyester window kit: ECC1-00-0156-G List of Components: Polyester (PET) window (3 pcs, 22 x 0.25 mm) - Page 12 User Manual ECC-Opto-Std-Aqu Cell holder II for ECC-Opto-Std ECC1-00-0335-A Measurements: Height: 41.8 mm Width: 78 mm Depth: 76 mm Designed for Bruker D8 Note: Only in combination with Lid ECC1-00-0127-M Cell holder III for ECC-Opto-Std ECC1-00-0419-A Measurements: Height: 20 mm Width: 75 mm Depth: 61.5 mm...
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Page 13: Unpacking
Contact EL -CELL, if anything is missing or damaged. NOTE: Damaged shipments must remain within the original packaging for freight company inspection. List of components: ECC-Opto-Std-Aqu test cell with stand, fully equipped for use in both 2-electrode and 3-electrode (reference) configuration in aqueous electrolytes ECC-Opto cell cable ECE1-00-0075-A Page 13 of 19 Release 1.56... -
Page 14: Technical Data
User Manual ECC-Opto-Std-Aqu Glass windows (5 pieces) LAB0018/V Glass fiber separators (5 pieces) ECC1-01-0012-J/V Feed wire (Au), assy ECC1-00-0010-O Transfer line syringe (5 ml) for vacuum filling ECC1-01-0001-A O-Ring 6.75 mm x 1.78 mm DIC9013 O-Ring 16 mm x 1.8 mm DIC9012 Hex wrench 0.9 mm... -
Page 15: Spare Parts
User Manual ECC-Opto-Std-Aqu 10 Spare parts ECC-Opto-Std-Aqu test cell Page 15 of 19 Release 1.56... - Page 16 User Manual ECC-Opto-Std-Aqu Central CE Piston ECC-OPTO-STD AQU ECC1-00-0180-B Page 16 of 19 Release 1.56...
- Page 17 User Manual ECC-Opto-Std-Aqu REF electrode OPTO, assy (Au) ECC1-00-0010-R Page 17 of 19 Release 1.56...
- Page 18 User Manual ECC-Opto-Std-Aqu Electrode Feed Wire, OPTO, assy (Au) ECC1-00-0010-O Page 18 of 19 Release 1.56...
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Page 19: Technical Support
12 Warranty For a period of one year from the date of shipment, EL-Cell GmbH (hereinafter Seller) warrants the goods to be free from defect in material and workmanship to the original purchaser. During the warranty period, Seller agrees to repair or replace defective and/or nonconforming goods or parts without charge for material or labor, or, at the Seller’s option, demand return...
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