ABB Aztec 600 Operating	 Instruction

ABB Aztec 600 Operating Instruction

Ise ammonia and flouride, single-stream ion-selective analyzers
Hide thumbs Also See for Aztec 600:
Table of Contents

Advertisement

Quick Links

A B B M E A S U R E M E N T & A N A LY T I C S | O P E R AT I N G I N S T R U C T I O N
Aztec 600 ISE ammonia and flouride
Single-stream ion-selective analyzers
Introduction
This publication provides installation, operation and
maintenance procedures for the Aztec 600 ISE
ammonia and flouride anlayzers.
Measurement made easy
For more information
Further publications for the Aztec 600 ISE ammonia
and flouride anlayzers are available for free
download from www.abb.com (see links and
reference numbers below) or by scanning this code:
Search for or click on:
AAM631
DS/AAM631-EN
Aztec 600 ISE ammonia analyzer
Data sheet
AFM631
DS/AFM631-EN
Aztec 600 ISE fluoride analyzer
Data sheet

Advertisement

Table of Contents
loading

Summary of Contents for ABB Aztec 600

  • Page 1 Measurement made easy Introduction For more information This publication provides installation, operation and Further publications for the Aztec 600 ISE ammonia maintenance procedures for the Aztec 600 ISE and flouride anlayzers are available for free ammonia and flouride anlayzers. download from www.abb.com (see links and...
  • Page 2: Table Of Contents

    Configuration Level Chart View Menu – see Section 2.1, page 8 Indicator View Menu – see Section 2.1, page 8 See Section 6, page 26 See Section 7, page 44 See Section 8, page 51 See Section 11, page 57 See Section 12.2, page 62 See Section 4.2, page 23 See Section 9, page 53...
  • Page 3 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Contents Contents 1 Safety ................3 6 Configuration ..............26 Health & Safety ............3 Common ............... 28 Electrical Safety – CEI / IEC 61010-1:2001-2 ... 3 6.1.1 Setup ............28 Symbols –...
  • Page 4 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Contents 8 Chart Functions .............51 Appendix B – Troubleshooting ......... 77 Historical Review ............51 B.1 Analyzer Malfunction ..........77 Operator Messages ..........51 B.2 Reagent and Standard Solutions ......77 Chart Annotation ............51 B.3 Probe Malfunction ..........
  • Page 5: Safety

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 1 Safety 1 Safety Information in this manual is intended only to assist our customers in the efficient operation of our equipment. Use of this manual for any other purpose is specifically prohibited and its contents are not to be reproduced in full or part without prior approval of the Technical Publications Department.
  • Page 6: Symbols - Cei / Iec 61010-1:2001-2

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 1 Safety 1.3 Symbols – CEI / IEC 61010-1:2001-2 One or more of the following symbols may appear on the equipment labelling: This symbol indicates the presence of devices Protective earth (ground) terminal.
  • Page 7: Product Recycling Information

    Note. The following only applies to European customers. ABB is committed to ensuring that the risk of any environmental damage or pollution caused by any of its products is minimized as far as possible. The European Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/EC) that came into force on August 13 2005 aims to reduce the waste arising from electrical and electronic equipment;...
  • Page 8: Safety Conventions

    Other than the serviceable items listed in Appendix G, page 90, none of the instrument's components can be serviced by the user. Only personnel from ABB or its approved representative(s) is (are) authorized to attempt repairs to the system and only components formally approved by the manufacturer should be used.
  • Page 9: Introduction

    Analyzer main components are shown in Fig. 2.1. The hinged  Aztec 600 ISE Fluoride lower door provides environmental protection liquid-handling section to ensure stabilized measurement *For information about reagent solutions, contact the local ABB conditions. representative. Cable Entries (both sides of case) Display Electronics Liquid-Handling Section...
  • Page 10: Operator Display Overview

    39 Measured values and measurement units Alarm Event Log screen Chart trace Alarm icon, event, date and time – see Section 12.3.2, page 63 Status bar Table 2.1 Overview of Aztec 600 Operator and Log Screens OI/AXM630–EN Rev. I...
  • Page 11 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 2 Introduction Note. 1. Alarm Status – Flashing red alarm event icon – alarm active and unacknowledged – Continuous red alarm event icon – alarm active and acknowledged 2. Alarm Event and Operator Message Annotations If Alarm event annotation is enabled and an alarm becomes active, a red alarm event icon surrounded by a channel colored box is displayed at the point at which the alarm occurred, together with the alarm time and tag.
  • Page 12: Installation

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3 Installation 3.1 Optional Accessories 3.3 Location Optional accessories comprise: For general location requirements refer to Fig. 3.1. Install in a clean, dry, well ventilated and vibration-free location giving easy ...
  • Page 13: Mounting

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.4 Mounting 3.4.1 Mounting Dimensions Dimensions in mm (in.) 315 (12.4) 430 (16.9) 279 (11.0) 183 (7.2) 653 (25.7) (15.7) 300 (11.8) 600 (23.6) Fig. 3.2 Mounting Dimensions OI/AXM630–EN Rev. I...
  • Page 14: Mounting The Analyzer

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.4.2 Mounting the Analyzer 3.4.3 Mounting the Optional Reagent Tray Dimensions in mm (in.) Dimensions in mm (in.) 600 (23.6) (1.4) 565 (22.2) 300 (11.8) (1.4) 6 Holes Ø...
  • Page 15: Electrical Connections

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.5 Electrical Connections Warning.  The analyzer is not fitted with a switch therefore an isolation device such as a switch or circuit breaker conforming to local safety standards must be fitted to the final installation. It must be fitted in close proximity to the analyzer within easy reach of the operator and must be marked clearly as the isolation device for the analyzer.
  • Page 16: Connections Overview

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.5.1 Connections Overview AC Power Supply Earth (Ground) Stud (on AC models only) – see Warnings in Section 3.5, page 13 Sockets for Optional Digital Communications Stop Attention Relay...
  • Page 17: General Connections

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.5.2 General Connections Note.  Cable entry holes are located on both sides of the enclosure.  Application board connection terminal blocks TB1 to TB8 are identified in Fig. 3.5 on page 14.
  • Page 18: Ethernet Connection

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.5.3 Ethernet Connection 3.5.4 Alarm Relay Contact Protection and Interference Suppression NC C NO Relay Contacts External AC Supply Load A – AC Applications Relay Contacts NC C NO...
  • Page 19: Preparing The Analytical Section

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.6 Preparing the Analytical Section 3.6.1 Connecting Sample Inlet and Drain Lines The sample pot fills with sample and over-flows at the top to maintain a constant head from where sample is taken to be measured.
  • Page 20: Fitting Peristaltic Pump Pressure Plate

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.6.3 Fitting Peristaltic Pump Pressure Plate To prevent premature wear to the pump tubing, the analyzer is supplied from the factory with the pump tubing pressure plate not fitted. The pressure plate must be fitted and secured for the pump to function correctly –...
  • Page 21: Connecting Reagent And Calibration Solutions

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.6.4 Connecting Reagent and Calibration Solutions Warning.  Reagents and calibration solutions may contain hazardous chemicals. Ensure that safety information is read and understood before handling the solutions. ...
  • Page 22: Ammonia Probe Preparation

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.6.5 Ammonia Probe Preparation The ammonia probe is supplied in kit form and must be assembled before use. Referring to Fig. 3.12: 1. Unscrew end cap from probe body .
  • Page 23: Fluoride Probe Preparation

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 3 Installation 3.6.6 Fluoride Probe Preparation The fluoride probe is supplied with a protective end cap to prevent the Lanthanum Fluoride crystal (forming its tip) from drying out and from being scratched or chipped. To prepare for use, remove the end cap and carefully rinse the tip in distilled water.
  • Page 24: Getting Started

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 4 Getting Started 4 Getting Started 4.1 Overview The following procedure describes how to start up and 6. Press the key and use the keys to select configure the analyzer prior to operation.
  • Page 25: On-Line Help

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 4 Getting Started 10. Press the key and use the keys to select 4.2 On-line Help 'Operate' followed by 'Prime lines and Calibrate' and press the key. When the priming sequence is complete, a stabilizing period is initiated to allow the measurement cell temperature to stabilize.
  • Page 26: Operation

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 5 Operation 5 Operation 5.2 Navigation and Editing Warning. Depending on the type of field to be edited, the software provides a variety of methods for entering values. Protective eye wear and protective hand wear is recommended when contact with chemicals is possible.
  • Page 27: Numeric Editing

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 5 Operation 5.2.2 Numeric Editing If the field to be edited requires a numeric value, a number-pad Tabs is displayed: To select a tab, use the keys. Note. The tab indicates that there are more tabs available.
  • Page 28: Configuration

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6 Configuration Displayed only if 'Security system' parameter is set to Displayed only if 'Security 'Basic' – see on-line help system' parameter is set to system 'Advanced' – see on-line...
  • Page 29 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration Note.  If 'New Configuration' or 'Open Configuration' is selected and the modified configuration file is saved, new data files for all log files are created and any unarchived data is lost ...
  • Page 30: Common

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.1 Common There are nine tabs in the Common screen: 6.1.1 Setup Fields Description Lists the available languages. Language A new language selection does not take effect until the configuration is saved.
  • Page 31: Time

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.1.3 Time Fields Description Warning. Changing the time can result in the permanent loss of data. Once it is changed a Date and Time warning is displayed stating that recording is disabled until the configuration has been saved.
  • Page 32: Security

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.1.4 Security The analyzer is fitted with an internal security switch that, in combination with the 'Configuration security' parameter settings (see page 31), is used to prevent unauthorized access to the Configuration Level.
  • Page 33 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration Note. User 1 is the System Administrator and the only user with access to the 'Security type' parameter – see Table 6.1. User 1 User 1 (System Administrator) Security Rights Set initial password-protected access to Calibration &...
  • Page 34 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration Fields Description Sets access to the 'Calibration & Maintenance' and 'Logging' menus. If set to 'Off', no password is required. If set to 'On' and 'Security type' is set to 'Basic' an additional 'Operator level password' field is Operator level security displayed.
  • Page 35: User

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.1.5 User Fields Description If 'Security system' is set to 'Basic' this tab lists the four users, User 1 to User 4. Selecting a user opens a new page with two fields: ...
  • Page 36: Measurement

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.2 Measurement There are two tabs in the Measurement screen: 6.2.1 Setup Fields Description Chemical Units For certain parameters there is a choice of units to display the results.
  • Page 37: Calibration

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.3 Calibration There is one tab in the Calibration screen. 6.3.1 Setup Fields Description Calibration Time The time the analyzer calibrates. Calibration Date The next date when a calibration is due.
  • Page 38: Alarm Relays

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.4 Alarm Relays Concentration Hysteresis Trip Point Hysteresis Concentration Concentration Alarm On Alarm On Alarm Off Alarm Switches Alarm Switches Off Automatically Off Automatically High Alarm Action Low Alarm Action Fig.
  • Page 39 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration There are six tabs in the Alarm Relays screen, one for each alarm: Fields Description Each of the six alarms can be configured independently to one of the following sources: ...
  • Page 40: Current Outputs

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.5 Current Outputs There are seven tabs in the Outputs screen, one for each output and an output calibration tab: 6.5.1 Outputs 1 to 6 Fields Description The 'Output Source' field can be set to one of the following options: ...
  • Page 41: Logging

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.6 Logging There are four tabs in the 'Logging' screen: 6.6.1 Chart Fields Description The orientation and direction of the chart display. Options are:  Horizontal --> Chart view enable ...
  • Page 42: Archive

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.6.4 Archive Used to configure the data that is to be recorded on the SD card – see Section 7.1, page 45. When external archive media contains approximately 300 files, its read / write performance becomes too slow, archiving is stopped...
  • Page 43: Communications

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.7 Communications There are four tabs in the 'Communications' modules screen: 6.7.1 Ethernet Configures the way in which the analyzer can be accessed via an Ethernet network – see Appendix E on page 85.
  • Page 44: E-Mail 1 And E-Mail 2

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.7.2 E-mail 1 and E-mail 2 The analyzer can be configured to send e-mails to a maximum of 6 recipients in response to certain events. The addressees can all subscribe to the same SMTP server or the analyzer can be configured to send e-mails via 2 different SMTP servers to a maximum of 3 addressees per server.
  • Page 45: Commissioning

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 6 Configuration 6.8 Commissioning Note. Access to the Commissioning Level is protected by an Internal Security Switch. The switch is, by default, set to 'Disabled' and should be set to 'Enabled' only if the measurement parameter is to be changed. For further information on the function of the Internal Security Switch, refer to Section 6.1.4, page 30.
  • Page 46: Logging

    Additional files can also be archived: track of which data has been archived.  Alarm event log data Note. ABB’s DataManager Pro software can be used to  Audit log data store and view data archived from the analyzer. ...
  • Page 47: Sd Cards

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 7 Logging The measured value is logged at default intervals of 30 seconds. 7.1.1 SD Card Insertion / Removal Approximate durations for continuous recording of 1 stream is shown in Table 7.1 (internal storage), Table 7.2 (external text format files) and Table 7.3 (external binary format files).
  • Page 48: External Media Status Icons

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 7 Logging When an SD card is inserted and there is <1 day (Binary format) 7.1.2 External Media Status Icons The status of external media is indicated by icons displayed in or <1 hour (Text format) of data in internal memory, a dialog box...
  • Page 49: Text Format Data Files

    Alternatively, the data can be analyzed graphically in detail on a ® spreadsheet, for example, Microsoft Excel (as shown in Figs. PC using ABB's DataManager Pro data analysis software. 7.3 and 7.4. Fig. 7.3 Example of Text Format Channel Data File Fig. 7.4 Example Text Format Audit Log File...
  • Page 50: Text Format Stream Data Filenames

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 7 Logging 7.5.1 Text Format Stream Data Filenames Text format stream data files can be configured to contain data In addition to creating new stream data files according to the gathered over a predefined period of time (selected at the 'New 'New File Interval', they are also created in the following File Interval' parameter) –...
  • Page 51: Text Format Log Files (Audit And Alarm Log)

    <hour min> <day, mm, yy> Alarm Event The log data is stored in an encrypted text format. <process group tag>.e00 The files can be read on a PC using ABB's DataManager Pro <hour min> <day, mm, yy> Audit Log data analysis software package.
  • Page 52: Binary Format Stream Files

    Note. The analyzer's internal clock can be configured to saving period (summertime) are compatible with the adjust automatically at the start and end of 'Daylight Saving database feature of Version 5.8 (or later) only of ABB's Time' periods. DataManager Pro data analysis software package.
  • Page 53: Chart Functions

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 8 Chart Functions 8 Chart Functions Note. The 'Chart Functions' menu can be accessed only from the 'Chart View’ screen. see Section 8.1 see Section 8.2 see Section 8.3 see Section 8.4, page 52 Fig.
  • Page 54: Screen Interval

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 8 Chart Functions 8.4 Screen Interval Used to control the amount of data displayed on the screen. A longer screen interval displays more data, a shorter screen interval displays data over a shorter time period. In both cases, the full trace is preserved by plotting the maximum and minimum samples for each display.
  • Page 55: Operate

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 9 Operate 9 Operate Note. The 'Operate' menu can be accessed only from the 'Indicator View’ screen. see Section 9.1, page 53 see Section 9.2, page 53 see Section 9.3, page 53 see Section 9.4, page 53...
  • Page 56: Diagnostics

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 10 Diagnostics 10 Diagnostics Note. The 'Diagnostics' menu can be accessed only from the 'Indicator View’ screen. see Section 10.1, page 54 see Section 10.2, page 56 see Section 10.3, page 56 see Section 10.4, page 56...
  • Page 57: Cal

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 10 Diagnostics 10.1.2 Cal Fields Description Displays the standard currently being measured during the calibration cycle (for example, Calibration State Measuring Low, Measuring High, Sample, Recovery Period). Percentage Complete A 'real-time' indication of calibration progress.
  • Page 58: Cell Diagnostics

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 10 Diagnostics 10.2 Cell Diagnostics Cell Diagnostics enables the user to control the operation of the analyzer manually – bringing in reagents and sample etc. It also displays the detector output in real time giving an insight into how the analyzer is performing.
  • Page 59: Statistics

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 11 Statistics 11 Statistics Note. The 'Statistics' menu can be accessed only from the 'Chart View’ screen. Fig. 11.1 Statistics Selection Statistics displays the highest, lowest and mean values of the sample since the analyzer was either switched on or the value was reset.
  • Page 60: Diagnostic Information And Icons

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 12 Diagnostic Information and Icons 12 Diagnostic Information and Icons 12.1 Analyzer Diagnostic Information Diagnostic Icon NAMUR Status The analyzer is programmed to display diagnostic messages to provide information on servicing requirements and any other Failure conditions that develop during operation.
  • Page 61 A hardware error exists on the main board. Power the analyzer down, wait for 10 seconds and power-up again. If the error persists, contact the local ABB representative. Calibration Failed 'Calibration Fail Event' set to 'Fail' (see Section 6.3.1, page 35) 'Calibration Fail Event' set to 'Attention' (see Section 6.3.1, page 35) or...
  • Page 62 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 12 Diagnostic Information and Icons Stop Attention Calibration Failure Icon Diagnostic message Relay Relay Relay Relay Calibration Standard Empty The calibration standard bottle is empty. Replace the calibration solution. Critical Temperature Reached This alarm is initiated if the analyzer temperature rises above 60 °C...
  • Page 63  Power the analyzer down, wait for 10 seconds and power-up again. If the error persists, contact the local ABB representative. Probe Failure The probe is disconnected or the probe has failed. 1. Check the probe connections. 2. Replace the probe.
  • Page 64: Alarm Acknowledge

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 12 Diagnostic Information and Icons 12.2 Alarm Acknowledge 12.3 Audit Log and Alarm Event Log To acknowledge a particular alarm, use the keys to The 'Audit Log' and 'Alarm Event Log' are used to display a list highlight it in the menu and press the key.
  • Page 65: Alarm Event Log - Icons

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 12 Diagnostic Information and Icons 12.3.2 Alarm Event Log – Icons 12.3.3 Status Icons Note. Note. Status icons are displayed in the Status Bar – see Fig. 2.1, page 8. ...
  • Page 66: Maintenance

    – see Section 1, page 3.  Do not top-up solution bottles. Aztec 600 analyzers are designed to be as maintenance-free as  Dispose of the used bottles and contents safely, possible. The inherent product design and auto-calibrating according to national or local regulations.
  • Page 67: Regular Visual Checks

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 13 Maintenance 13.2 Regular Visual Checks 13.3.1 Replacing Pump Tubing and Capstans Inspect the analyzer on a regular basis to ensure the correct functioning of the system and to check the integrity of the Note.
  • Page 68 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 13 Maintenance 3. Referring to Fig. 13.2: Note. During step q, it is very important to ensure a. Press down on pump pressure plate , turn pressure that: plate locking pin turn counter-clockwise and withdraw the pin.
  • Page 69: Replacing Analyzer Tubing

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 13 Maintenance 13.3.2 Replacing Analyzer Tubing Note. Take note of the routing of all tubes removed in the following procedures to ensure the replacement tubing is routed correctly. Referring to Fig. 13.3: 1.
  • Page 70: Replacing Ammonia Probe Membrane

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 13 Maintenance 13.4 Replacing Ammonia Probe Membrane Referring to Fig. 13.4: Note. Mixer fitted to fluoride analyzers – 1. Unscrew end cap from probe body and allow filling optional fitting on ammonia analyzers.
  • Page 71: Replacing The Dc Fuse

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 13 Maintenance 13.5 Replacing the DC Fuse Caution. Use only replacement fuse: 12.5 A 125 V DC Type T, SCHURTER, Model SPT 5 x 20 Series Fig. 13.4 Replacing Ammonia Probe Membrane Fig.
  • Page 72: Specification - Aztec Ise Ammonia

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 14 Specification – Aztec ISE Ammonia 14 Specification – Aztec ISE Ammonia Measurement Environmental data Units Ambient operating temperature:  5 to 40 ºC (41 to 104 ºF)  Ambient operating humidity: Up to 95 % RH non-condensing ...
  • Page 73 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 14 Specification – Aztec ISE Ammonia Mechanical data Electrical Ingress protection Power supply ranges  IP31** 100 to 240 V max. AC 50 / 60 Hz ± 10 % (90 to 264 V AC, 45/65 Hz) ...
  • Page 74 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 14 Specification – Aztec ISE Ammonia Connectivity / communications Ethernet connection Web server with ftp for real-time monitoring, configuration, data file access and e-mail capability Communications PROFIBUS DP V1.0 (optional) Data handling, storage and display...
  • Page 75: Specification - Aztec Ise Fluoride

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 15 Specification – Aztec ISE Fluoride 15 Specification – Aztec ISE Fluoride Measurement Environmental data Range Ambient operating temperature:  0.100 to 100 ppm F 5 to 40 ºC (41 to 104 ºF)
  • Page 76 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 15 Specification – Aztec ISE Fluoride Mechanical data Electrical Ingress protection Power supply ranges  IP31** 100 to 240 V max. AC 50 / 60 Hz ± 10 % (90 to 264 V AC, 45/65 Hz) ...
  • Page 77 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers 15 Specification – Aztec ISE Fluoride Connectivity / communications Ethernet connection Web server with ftp for real-time monitoring, configuration, data file access and e-mail capability Communications PROFIBUS DP V1.0 (optional) Data handling, storage and display...
  • Page 78: Appendix A - Reagents And Standard Solutions

    Appendix A – Reagents and Standard Solutions A.2 Reagent and Standard Solutions – Fluoride-ISE Warning. A standard set of reagents for the Aztec 600 ISE fluoride analyzer comprises 1 reagent, a low calibration standard and a  Ensure personal protective equipment (PPE) such as high calibration standard.
  • Page 79: Appendix B - Troubleshooting

    To minimize malfunctions, ensure the system is functioning correctly. To check the integrity of the readings, ABB recommended that the analyzer and the sampling system is visually inspected on a regular basis as follows: ...
  • Page 80 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix B – Troubleshooting Fault Possible Cause Remedy Noisy electrode Air bubbles present on probe tip 1. Remove probe to clear air bubbles and refit output 2. Check sample supply and check for air leaks...
  • Page 81 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix B – Troubleshooting Fault Possible Cause Remedy Low readings Incorrect calibration Check calibration solutions for accuracy Ammonia probe response slow 1. Check probe and replace membrane if required 2. Check reference electrode for signs of stripping of chloridised...
  • Page 82 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix B – Troubleshooting Fault Possible Cause Remedy Calibration failure Probe sensing end fouled 1. Check end of probe is clean and clear of any possible fouling with slow probe 2. Check pump speed and tubing response 3.
  • Page 83: Appendix C - Principle Of Operation - Ammonia Analyzers

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix C – Principle of Operation – Ammonia Analyzers Appendix C – Principle of Operation – Ammonia Analyzers Solenoid valve and manifold assemblies Reagent pump Ammonia flowcell assembly (red) Standard Standard...
  • Page 84: Theory Of Operation

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix C – Principle of Operation – Ammonia Analyzers C.2 Theory of Operation Ion-selective electrodes are useful tools in analytical chemistry. The exact value of the slope can be used as indication of the Rapid measurements of a great variety of species over wide efficiency of the ion-selective electrode in use.
  • Page 85: Appendix D - Principle Of Operation - Fluoride Analyzers

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix D – Principle of Operation – Fluoride Analyzers Appendix D – Principle of Operation – Fluoride Analyzers Solenoid valve and manifold assemblies Reagent pump Conditioned sample Fluoride flowcell assembly (blue)
  • Page 86: Theory Of Operation

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix D – Principle of Operation – Fluoride Analyzers D.2 Theory of Operation Ion-selective electrodes are useful tools in analytical chemistry. The exact value of the slope can be used as indication of the Rapid measurements of a great variety of species over wide efficiency of the ion-selective electrode in use.
  • Page 87: Appendix E - Web Server

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix E – Web Server Appendix E – Web Server Fig. E.1 Web Server Screen d Language Selection – selects the language for the web The analyzer is fitted with an ethernet card as standard and, when the appropriate configuration settings have been made, pages.
  • Page 88: Stream Values

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix E – Web Server E.1 Stream Values E.5 Logging Status E.2 Operate Note. Menu options from the 'Operate' window start the routine described when the associated button is selected. E.6 Operator Message An 'Operator Message' is displayed on the chart view.
  • Page 89: Configuration

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix E – Web Server E.7 Configuration To access data stored on the analyzer via Internet Explorer: Note. A user must be logged-on for the configuration 1. Start Internet Explorer. button to be enabled.
  • Page 90: Ftp Access Via Datamanager

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix E – Web Server E.10 FTP Access via DataManager DataManager can be used with FTP to access data files that have been saved to the archive media (SD card) inserted in the analyzer.
  • Page 91: Appendix F - Updating The Software

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix F – Updating the Software Appendix F – Updating the Software 9. A 'Warning' screen appears next. This provides the option to upgrade the existing system software or exit without...
  • Page 92: Appendix G - Spare Parts

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix G – Spare Parts Appendix G – Spare Parts G.1 Maintenance Kits Part No. Description Part No. Description AW620 020 Annual consumable spares kit 8002 621 Ammonia probe inner electrode...
  • Page 93: Reagents

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix G – Spare Parts G.3 Reagents G.4 Valve Assemblies and Associated Parts Part No. Description Part No. Description AWRK620/0300 Set of Ammonia Reagents – 1 each of: AW620 030 Valve solenoid assembly ...
  • Page 94: Side Sample Pot Assembly And Associated Parts

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix G – Spare Parts G.5 Side Sample Pot Assembly and Associated Parts Part No. Description Part No. Description AW630 062 Side sample pot elbow fitting AW630 085 Sample pot bottom cap – complete with –...
  • Page 95: Pump Motor Assemblies And Associated Parts

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix G – Spare Parts G.6 Pump Motor Assemblies and Associated Parts G.7 Flowcell Assemblies and Associated Parts Part No. Description Part No. Description AW620 040 Pump motor assembly AW620 015...
  • Page 96 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix G – Spare Parts Part No. Description Part No. Description AW620 026 Heated block assembly AW622 051 Ammonia flowcell assembly (Red) AW621 051 Fluoride flowcell assembly (Blue) OI/AXM630–EN Rev. I...
  • Page 97: Plumbing And Tubing

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix G – Spare Parts G.8 Plumbing and Tubing Part No. Description Part No. Description AW620 060 Pump tube kit AW630 057 Level sensor assembly – 2.5 l / 5 l AW630 056 Level sensor assembly –...
  • Page 98: Electronic Boards

    Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Appendix G – Spare Parts G.9 Electronic Boards G.10 Transmitter Assembly Part No. Description Part No. Description AW600 051 Aztec / Navigator PSU kit – AC AW630 010 Transmitter assembly (fully tested) – AC AW600 056 Aztec / Navigator PSU kit –...
  • Page 99 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Index Index Access Editing ................24 User access .............. 33 e-mail ................42 Ethernet ................41 Alarm relays ..............36 Alarms ................9 Fail safe ..............37 New alarm ..............9 Fail safe ................
  • Page 100 Aztec 600 ISE ammonia and fluoride Single-stream ion-selective analyzers Acknowledgements Operate ................53 Sampling requirements ........... 10 Operator Screen capture ............... 28 Messages ..............51 Screen interval ..............52 Screen saver wait time ............ 28 Passwords ..............32 SD card ................45 Security ..............32 Secure digital media ............
  • Page 101 — Food & Beverage offices for details on your nearest Service and Repair Centre. — Manufacturing — Metals and Minerals — Oil, Gas & Petrochemical ABB Limited — Pulp and Paper Tel: +44 (0)1453 826661 Drives and Motors Fax: +44 (0)1453 829671 —...
  • Page 102 We reserve the right to make technical changes or modify the contents of this document without prior notice. With regard to purchase orders, the agreed particulars shall prevail. ABB AG does not accept any responsibility whatsoever for potential errors or possible lack of information in this document.

This manual is also suitable for:

Aam631Afm631Aztec 600 ise

Table of Contents