Table 5 Membrane specifications - Oxygen sensors (1) (continued) Specification 2956A-A 2958A-A 29552A-A 2952A-A Gaseous measurement range 0 Pa to 50 kPa 0 Pa to 100 kPa 0 Pa to 200 kPa 0 Pa to 200 kPa Accuracy The greater of The greater of The greater of The greater of...
Table 6 Membrane specifications - Oxygen sensors (2) (continued) Specification 2935A-A 29521A-A 2995A-A Integrated radiation dose limit [rads] Expected current in air @ 1 bar 25 °C [μA] Expected current in pure O [μA] consumption in O saturated water at 25 °C [μg/hour] Temp.
N O T I C E Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special emphasis. 2.1.2 Precautionary labels Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed.
Figure 3 Product components 1 Sensor 3 Sensor recharge kit 2 Protection caps 2.3.1 Electrochemical sensor The sensor may be delivered separately or as part of an ORBISPHERE system, depending on the individual order. The sensor will be delivered fitted with a plastic screw-on storage cap to protect the sensor head. This is held in place with a plastic collar.
being used once. Refer to the documentattion supplied with the recharge kit for instructions on how to use the anode cleaning tool for a GA2X00 sensor or for a A110X sensor. The cotton washers provide additional protection against the formation of deposits and residue on the center electrode and anode, which prolongs the time period required between sensor maintenance.
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1. Hold the main body of the sensor and unscrew the protection cap locking washer by turning counter-clockwise. Remove it from the sensor and put to one side. 2. Pull/twist off the protection cap and put to one side. 3. Hold the sensor with the membrane facing down to avoid spilling any electrolyte, then carefully unscrew the shipment cartridge.
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7. Hold the container steady between thumb and forefinger of one hand. Lower the sensor into the container until the top of the anode is covered with electrolyte. Leave for a few seconds to ensure the cotton washer has fully absorbed some of the electrolyte and that it is no longer dry. 8.
10. Rinse the sensor under a tap for about 5 seconds to remove any excess electrolyte, then gently wipe with a soft tissue to ensure all parts are completely dry. Drain the overflow electrolyte from the container into a sink and flush away. Discard the used container. ®...
Note: There may be situations where not all the above conditions can be met. If this is the case, or you have any concerns, please consult your Hach representative to appraise the situation and define the best applicable solution. 3.2.2 Sensor insertion Note: Check that the small O-ring at the bottom of the flow chamber is present during removal and installation of the sensor, as it may stick to the sensor head and fall.
3.3 Accessories installation 3.3.1 External pressure sensor The system can be fitted with an external pressure sensor. This enables a measurement of fraction of gas under variable pressure conditions during gas phase measurement. Note: Do NOT exceed the pressure range of the sensor. This would permanently deform the sensor membrane, thus delivering incorrect pressure values in the future.
Figure 6 Weld-on sensor socket 1 Pipe diameter 2 Setback allowed from internal pipe diameter Figure 7 Installation in-line 1 Shut off valve 4 Shut off valve 2 Sensor socket 5 Sampling valve 3 Sampling valve 3.3.3 The 32003 insertion/extraction valve The ORBISPHERE 32003 insertion/extraction valve allows for sensor removal and installation without having to drain the fluid in the line.
Figure 8 ORBISPHERE model 32003 insertion/extraction valve 1 Sensor 3 Sample flow 2 Valve 3.3.4 The 33095 sensor housing The ORBISPHERE 33095 sensor housing is also available for use with the GA2X00 sensor but requires that the sample flow be turned off prior to insertion or removal of the sensor. Sensor insertion is made by inserting the sensor into the housing and tightening the retaining collar until it stops.
3.3.6 ORBISPHERE flow chambers The ORBISPHERE 32001.xxx flow chambers are used to draw liquid and gaseous samples past the sensor. They are available in several materials, depending on the application. Refer to Table 7 Figure ™ They connect to 6-mm or ¼" stainless steel tubing by means of two Swagelok fittings.
Figure 11 Flow chamber connections 1 Measuring 7 Sample flow out 2 Calibration 8 Calibration gas in 3 Sensor 9 Calibration gas out 4 Calibration gas in shut off 10 Sample flow in shut off 5 Calibration gas out shut off 11 Sample flow out shut off 6 Sample flow in 3.3.7 Multi-parameter flow chamber...
Figure 12 Multi-parameter flow chamber Shown here with: • gas sensor (right), • pressure sensor (center), • optional second sensor (left) Section 4 Maintenance W A R N I N G Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the document.
4.1 Maintenance schedule The following table shows the recommended schedule for membrane replacement. The table should only be used as a guideline, as maintenance intervals will vary depending on a number of different parameters (e.g. water chemistry, CIP frequency, oxygen levels, sample temperature, etc.). Application Membrane type Membrane replacement...
4.3 Membrane replacement and sensor head cleaning C A U T I O N Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets (MSDS/SDS) for safety protocols.
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7. Rinse the sensor head under a tap for 15 seconds, aiming the jet of water directly onto the sensor head. Do not dry the center electrode area, as the gap between cathode and guard should be left filled with water. 8.
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11. Remove the polishing tool from the sensor. Remove any polish deposits by rinsing the sensor head under a tap for 30 seconds, aiming the jet of water directly onto the sensor head. Note: If the sensor is used in high level hydrogen sample, do not perform the following steps but continue at step 19.
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16. On the sensor cleaning and regeneration center, turn the knob to the Guard position and press the TIMER switch. Again, watch for the formation of bubbles and repeat the cleaning process if necessary. 17. On the sensor cleaning and regeneration center, turn the knob to the Cathode position and press the TIMER switch.
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20. Take a silicone disc from the recharge kit, hold it between thumb and forefinger and position it on top of the anode. Take a new cotton washer from the recharge kit. Hold it between thumb and forefinger and position it on top of the silicone disc. Note: During this step, it is very important to ensure your finger does not come into contact with the cathode (golden surface) as it could leave greasy deposits on the surface.
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25. Rinse the sensor under a tap for about 5 seconds to remove any excess electrolyte, then gently wipe with a soft tissue to ensure all parts are completely dry. Drain the overflow electrolyte from the container into a sink and flush away. Discard the used container. ®...
Section 5 Troubleshooting 5.1 Oxygen sensor Problem Probable cause Possible solution Sensor won't calibrate, even after Instrument internal Calibrate using a certified barometer. Do not cleaning and/or membrane barometric pressure correct for sea level ! change. sensor needs calibration. Wet membrane Wipe dry with a tissue and re-calibrate.
Problem Probable cause Possible solution Calibration is out of specification Sensor incorrectly setup. Check the sensor parameters on the instrument. or response time is too slow. Re-calibrate the sensor. Temperature Control the temperature with an external measurement incorrect. reference. Re-calibrate the sensor. Barometric pressure Calibrate the barometric pressure sensor using incorrect.
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Flow chambers and installation devices (continued) Description Item no. Flow chamber in Monel with 6 mm fittings. Supplied with EPDM O-rings. 32001.070 Flow chamber in Monel with ¼" fittings. Supplied with EPDM O-rings. 32001.071 Flow chamber in stainless steel (316) with 6 mm fittings. Supplied with Viton O-rings. 32001.110 Flow chamber in stainless steel (316) with ¼"...
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Sensor replacement parts (continued) Description Item no. GA2800 oxygen sensor, ATEX, hastelloy, kalrez o-rings, cap without grille GA280E-HKS Stainless steel sensor collar 28104 PPS sensor collar 28105 Delrin storage cap (sensor storage cap) 28129 Sensor support (base) for 31xxx, X110X and GA2X00 sensors 32205 Stainless steel 28mm cap for ORBISPHERE GA2X00 family EC sensors (without 33051-S0...
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Recharge kits (continued) Description Item no. For 6110 TPA. Recharge kit of 4 pre-filled cartridges with premounted 2956A membranes for A1xxx and GA2x00 oxygen sensors. Includes o-rings, cotton washers, 2956A-AT silicone discs and cleaning tools For 6110 TPA. Recharge kit of 4 pre-filled cartridges with premounted 2956A membranes for A1xxx and GA2x00 oxygen sensors.