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Agilent Technologies 1200 Series User Manual

Thermostatted column compartment
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G1316A /G1316B
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  • Page 1 Agilent 1200 Series Thermostatted Column Compartment G1316A /G1316B User Manual...
  • Page 2 Customers of Software. Agilent the Agilent 1200 Series Thermostatted Col- tions are fully understood and provides this customary commercial license umn Compartment. It is available as Adobe met.
  • Page 3 In This Guide… This manual covers the Agilent 1200 Series Thermostatted Column Compartments (TCC) G1316A Agilent 1200 Series TCC G1316B Agilent 1200 Series TCC-SL Introduction to the Column Compartment This chapter gives an introduction to the TCC, instrument overview and internal connectors.
  • Page 4 Parts and Materials for Maintenance This chapter provides information on parts for maintenance. Appendix This chapter provides addition information on safety, legal and web. 1200 Series TCC User Manual...

  • Page 5: Table Of Contents

    Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications Installing the Column Compartment Unpacking the Column Compartment Optimizing the Stack Configuration Installing the Column Compartment Flow Connections of the Column Compartment Installation of Heater and Cooling Devices 1200 Series TCC User Manual...
  • Page 6 Installing the Temperature Sensor Maintenance and Repairing Introduction to Maintenance and Repair Warnings and Cautions Cleaning the Column Compartment Using the ESD Strap Maintenance Overview of Maintenance Changing Column Identification Tags Replacing Head Parts of Column Switching Valve 1200 Series TCC User Manual...
  • Page 7 G1316B SL Capillary System Kit G1316B SL Micro Valve Kit 2 Position/10 Port Column Regeneration Kit Plastic Parts Leak Parts Appendix General Safety Information Lithium Batteries Information Radio Interference Sound Emission Solvent Information Agilent Technologies on Internet 1200 Series TCC User Manual...
  • Page 8 Contents Index 1200 Series TCC User Manual...

  • Page 9: Introduction To The Column Compartment

    Agilent 1200 Series Thermostatted Column Compartment User Manual Introduction to the Column Compartment Introduction to the Column Compartment Extendended Specifications on G1316B SL System Overview Column-Identification System Column Switching Valve (Optional) Electrical Connections Instrument Layout This chapter gives an introduction to the TCC, instrument overview and internal connectors.

  • Page 10: Introduction To The Column Compartment

    The Agilent 1200 Series thermostatted column compartment is a stackable temperature-controlled column compartment for LC. It is available as standalone module or as a component of a Agilent 1200 Series system. It is used for heating and cooling to meet extreme requirements of retention time reproducibility.

  • Page 11: Extendended Specifications On G1316B Sl

    Introduction to the Column Compartment Extendended Specifications on G1316B SL The 1200 series G1316B SL thermostatted column compartment is usable from 10°C below ambient up to 80° for flow ranges up to 5 ml/min and up to 100°C for flow ranges up to 2.5 ml/min. To reduce the risk of additional dispersion...
  • Page 12 The use and optimization of the new small heat-exchangers and cooling devices is N O T E described in detail in a Technical Note. 1200 Series TCC User Manual...

  • Page 13: System Overview

    This depends on several factors: flow rate, setpoint temperature, ambient temperature and column dimensions. The higher the flow rate, the faster the column equilibrates (due to thermostatted mobile phase). 1200 Series TCC User Manual...
  • Page 14 Heat exchanger temperature Column temperature Example for a flow rate of 5 ml/min of water Time (min) Figure 2 Equilibration of Heat Exchanger and Column Temperature The temperature calibration and verification is described in the Service Manual. 1200 Series TCC User Manual...

  • Page 15: Column-Identification System

    Introduction to the Column Compartment Column-Identification System The Agilent 1200 Series thermostatted column compartment is equipped with a column-identification system. This allows to write and to read column-specific information to and from the column-identification tag. Antennas Column-identification tag, see page 17...
  • Page 16 For example, if the left column is selected, the right column is not updated, and vice versa. If no column switching valve is installed both sides are updated at the same time. 1200 Series TCC User Manual...

  • Page 17: Column-Identification Tag

    Figure 5 on page 17. The Agilent logo should be always at the front side. Column-identification tag Figure 4 Column-Identification Tag for Left Heat Exchanger Column-identification tag Figure 5 Column-Identification Tag for Right Heat Exchanger 1200 Series TCC User Manual...

  • Page 18: Column Clip

    Introduction to the Column Compartment Column Clip For better positioning of the column on the heat exchanger a column clip is available (see “Accessory Kits” on page 85). Figure 6 Column Clip (part number 5063-6526, pack of 6) 1200 Series TCC User Manual...

  • Page 19: Column Switching Valve (Optional)

    Switching should be done when the flow is off and the pressure is zero. From autosampler Heater assembly 1 Heater assembly 2 Column 1 Column 2 To detector Figure 8 Column 1 Active 1200 Series TCC User Manual...
  • Page 20 After the valve has switched, the analytical column flow continues in normal direction. Only the precolumn is back-flushed, eluting highly retained peaks directly to the detector. From autosampler Heater assembly 1 Heater assembly 2 Precolumn Analytical Column To detector Figure 10 Precolumn Back-flushing 1200 Series TCC User Manual...

  • Page 21: Electrical Connections

    Electrical Connections • The CAN bus is a serial bus with high-speed data transfer. The two connectors for the CAN bus are used for internal Agilent 1200 Series module data transfer and synchronization. • The REMOTE connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features such as common shut down, prepare, and so on.
  • Page 22 Configuration switch serial number: manufactured in Germany 2006 week of last major change 00130 number of unit product number serial number safety standards configuration switch settings voltage range power consumption / frequency Figure 11 Electrical Connections 1200 Series TCC User Manual...

  • Page 23: Instrument Layout

    • the plastic layers help cushion the electronic and mechanical parts from physical shock, and • the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the column compartment. 1200 Series TCC User Manual...
  • Page 24 Introduction to the Column Compartment 1200 Series TCC User Manual...

  • Page 25: Site Requirements And Specifications

    Agilent 1200 Series Thermostatted Column Compartment User Manual Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications This chapter gives information on environmental requirements, physical and performance specifications. Agilent Technologies...

  • Page 26: Site Requirements

    Make sure to have easy access to the power cable of the instrument, in order to C A U T I O N disconnect the instrument from line. 1200 Series TCC User Manual...
  • Page 27 Never use a power cord other than the power cord designed for your region. Never use cables other than the ones supplied by Agilent Technologies to ensure WA R N I N G proper functionality and compliance with safety or EMC regulations.

  • Page 28: Physical Specifications

    Operating altitude Up to 2000 m (6500 ft.) Non-operating altitude Up to 4600 m (14950 ft.) For storing the instrument Safety standards: IEC, CSA, UL, EN Installation Category II, Pollution Degree 2 For indoor use only. 1200 Series TCC User Manual...

  • Page 29: Performance Specifications

    1200 series module Safety and maintenance Extensive diagnostics, error detection and display (through control module and Agilent ChemStation), leak detection, safe leak handling, leak output signal for shutdown of pumping system. Low voltages in major maintenance areas. 1200 Series TCC User Manual...
  • Page 30 “Column-Identification System” page 15 Housing All materials recyclable. All specifications are valid for distilled water at ambient temperature (25 °C), set point at N O T E 40 °C and a flow range from 0.2–5 ml/min. 1200 Series TCC User Manual...

  • Page 31: Installing The Column Compartment

    Agilent 1200 Series Thermostatted Column Compartment User Manual Installing the Column Compartment Unpacking the Column Compartment Optimizing the Stack Configuration Installing the Column Compartment Flow Connections of the Column Compartment Installation of Heater and Cooling Devices This chapter describes the installation of the TCC.

  • Page 32: Unpacking The Column Compartment

    Ensure all parts and materials have been delivered with the column compartment. The delivery checklist is shown in Table 4. Please report missing or damaged parts to your local Agilent Technologies sales and service office. Table 4 Column Compartment Delivery Checklist...

  • Page 33: Optimizing The Stack Configuration

    Installing the Column Compartment Optimizing the Stack Configuration If your column compartment is part of a Agilent 1200 Series system, you can ensure optimum performance by installing the following configuration. This configuration optimizes the system flow path and ensures minimum delay...
  • Page 34 Installing the Column Compartment Solvent cabinet Vacuum degasser Pump Local User Interface Autosampler Column compartment Detector Figure 12 Recommended Stack Configuration (Front View) 1200 Series TCC User Manual...
  • Page 35 LAN to LC detector) ChemStation (location depends on detector) L A N I n i t M o d e L i n k C o n f i g Figure 13 Recommended Stack Configuration (Rear View) 1200 Series TCC User Manual...

  • Page 36: Installing The Column Compartment

    Figure 14 Front View of the Thermostatted Column Compartment 3 Connect the power cable to the power connector at the rear of the column compartment. 4 Connect the CAN cable to other Agilent 1200 Series modules. 1200 Series TCC User Manual...
  • Page 37 If a Agilent DAD/MWD/FLD is in the system, the LAN/GPIB should be connected to the N O T E DAD/MWD/FLD (due to higher data load). 6 Connect the APG Remote cable (optional) for non-Agilent 1200 Series instruments. 7 Turn ON power by pushing the button at the lower left side of the column compartment.
  • Page 38 WA R N I N G supply still uses some power, even if the power switch at the front panel is turned OFF. The column compartment was shipped with default configuration settings. N O T E 1200 Series TCC User Manual...

  • Page 39: Flow Connections Of The Column Compartment

    2 The column compartment is equipped with an access to heater area. column-identification system that can read column tags. Antennas Column tag Column clip For more information on column identification, see “Column-Identification System” on page 15. 1200 Series TCC User Manual...
  • Page 40 From autosampler To detector To connect the column selection valve, see “Column 5 Fix the column with the column clip from the accessory kit. Switching Valve (Optional)” on page 19. From autosampler To detector 1200 Series TCC User Manual...
  • Page 41 6 If the column compartment is not part of a Agilent 1200 7 Route tubings from modules above through the openings Series system, or if an Agilent 1200 Series Autosampler is in the funnel holder (top) and the plastic bottom part.

  • Page 42: Installation Of Heater And Cooling Devices

    Depending on the application, these heater and cooling devices can be fixed at various N O T E places. Information about the usage of these heater and cooling devices can be found in Technical Notes or in the Agilent 1200 Series Rapid Resolution LC System (1200 RRLC System) manual. L-shaped pre-column heater U-shaped Post-column cooler Volume: 1.6 µl...

  • Page 43: How To Optimize The Column Compartment

    Agilent 1200 Series Thermostatted Column Compartment User Manual How to optimize the Column Compartment Optimizing the Column Compartment Using Additional Heater and Cooling Devices This chapter gives hints on how to optimize the TCC. Agilent Technologies...

  • Page 44: Optimizing The Column Compartment

    • Assure that the front cover is always closed. Using Additional Heater and Cooling Devices The optimization (installation, interconnection, settings) is described in Technical Notes and the Agilent 1200 Series Rapid Resolution LC System (1200 RRLC System) manual. 1200 Series TCC User Manual...

  • Page 45: Troubleshooting And Diagnostics

    Agilent 1200 Series Thermostatted Column Compartment User Manual Troubleshooting and Diagnostics Overview of the Column Department’s Indicators and Test Functions Status indicators User Interfaces Agilent LC Diagnostic Software Overview about the troubleshooting and diagnostic features. Agilent Technologies...

  • Page 46: Overview Of The Column Department's Indicators And Test Functions

    Normally, temperature calibration is not required throughout the lifetime of the instrument. However, in order to comply with local regulatory requirements, calibration and verification may be required. The following sections describe these functions in detail. 1200 Series TCC User Manual...

  • Page 47: Status Indicators

    Figure 17 Location of Status indicators Power Supply Indicator The power supply indicator is integrated into the main power switch. When the indicator is illuminated (green) the power is ON. 1200 Series TCC User Manual...

  • Page 48: Instrument Status Indicator

    Usually, an error condition requires attention (for example, leak, defective internal components). An error condition always interrupts the analysis. 1200 Series TCC User Manual...

  • Page 49: User Interfaces

    Thermostat Function Test Temperature Calibration Yes (M) via command section Maintenance section Diagnose The Agilent Control Module (G1323B) does not do any calculations. So there will be no N O T E reports generated with passed/failed information. 1200 Series TCC User Manual...

  • Page 50: Agilent Lc Diagnostic Software

    The Agilent LC diagnostic software is an application independent tool that provides troubleshooting capabilities for the Agilent 1200 Series modules. It provides for all 1200 Series LC the possibility of a first guided diagnostic for typical HPLC symptoms and a status report stored as Adobe Acrobat pdf or as a printable file to assist users evaluating the instrument state.

  • Page 51: Test Functions

    Agilent 1200 Series Thermostatted Column Compartment User Manual Test Functions Thermostat Function Test Temperature Calibration This chapter describes the TCC’s built in test functions. Agilent Technologies...

  • Page 52: Thermostat Function Test

    The time required to reach 30 °C is a measure of heating efficiency. A typical thermostat function test profile is shown in Figure Temperature [°C] Right Peltier element Left Peltier element Time [minutes] Figure 18 Typical Thermostat Function Test Profile 1200 Series TCC User Manual...
  • Page 53 • Defective sensors on flex board. • Defective heater assembly. Suggested Actions Ensure cover is installed correctly. Ensure sufficient space is available for air circulation (“Bench Space” page 27). Exchange the heater assembly. 1200 Series TCC User Manual...

  • Page 54: Temperature Calibration

    The column thermostat is calibrated correctly when the measured temperature (using the external measuring device, “Temperature Calibration Procedure” on page 55) and the cross-over temperature (36 °C) of both heat exchangers (left and right) are within ± 0.5 °C 1200 Series TCC User Manual...

  • Page 55: Temperature Calibration Procedure

    Temperature measuring device (see note below) Parts required Calibrated temperature measuring device. For the measuring and calibration process Agilent Technologies recommends a measuring N O T E device that provides the necessary resolution and precision. Contact the local Agilent Technologies support representative for ordering information.

  • Page 56: Calibration Problems

    Hardware Failures Probable hardware failures leading to a failed calibration procedure are: • Defective or wrongly calibrated measuring device. • Defective heater assembly. • Defective ambient-temperature sensor. • Defective CCM board. 1200 Series TCC User Manual...

  • Page 57: Installing The Temperature Sensor

    The figures below refer to a specific type of temperature sensor (Heraeus, Quat340, quartz N O T E surface-temperature measurement sensor). Other sensors may require a different fixing. 1 Remove the front cover. 2 Install the temperature sensor at the measurement position on the left heat exchanger. 1200 Series TCC User Manual...
  • Page 58 Test Functions 3 Route the sensor wire through the slit in the leak tray. 4 Replace the front cover. 1200 Series TCC User Manual...

  • Page 59: Maintenance And Repairing

    Agilent 1200 Series Thermostatted Column Compartment User Manual Maintenance and Repairing Introduction to Maintenance and Repair Warnings and Cautions Cleaning the Column Compartment Using the ESD Strap This chapter provides general information on maintenance and repair of the TCC. Agilent Technologies...

  • Page 60: Introduction To Maintenance And Repair

    The security lever at the power input socket prevents that the column compartment cover is taken off when line power is still connected. These repairs are described in the Service Manual. 1200 Series TCC User Manual...

  • Page 61: Warnings And Cautions

    ESD Strap” on page 63. The column compartment has two heat exchanger assemblies that might be hot. If so, C A U T I O N allow them to cool down before starting repairs. 1200 Series TCC User Manual...

  • Page 62: Cleaning The Column Compartment

    Do not use an excessively damp cloth that liquid can drip into the column compartment. Do not let liquid drip into the column compartment. It could cause shock hazard and WA R N I N G it could damage the column compartment. 1200 Series TCC User Manual...

  • Page 63: Using The Esd Strap

    2 Unroll the rest of the band and peel the liner from the copper foil at the opposite end. 3 Attach the copper foil to a convenient and exposed electrical ground. Figure 20 Using the ESD Strap 1200 Series TCC User Manual...
  • Page 64 Maintenance and Repairing 1200 Series TCC User Manual...

  • Page 65: Maintenance

    Agilent 1200 Series Thermostatted Column Compartment User Manual Maintenance Overview of Maintenance Changing Column Identification Tags Replacing Head Parts of Column Switching Valve Adding Heater and Cooling Devices (G1316B SL) Correcting Leaks Replacing the Column Compartment’s Firmware This chapter describes the maintenance of the TCC.

  • Page 66: Overview Of Maintenance

    67 “Replacing Head Parts When the valve performance shows indication of of Column Switching leakage or wear Valve” on page 69 “Correcting Leaks” If leak has occurred Check for leaks page 73 1200 Series TCC User Manual...

  • Page 67: Changing Column Identification Tags

    Column identification tag, pack of 3, 5062-8588 The column compartment is equipped with an column-identification system, that stores column specific information. Two identification antennas are incorporated in the heat exchanger assemblies. Antennas Column-identification tag Figure 21 Location of Column Identification System 1200 Series TCC User Manual...
  • Page 68 Figure 22 Figure 23. The Agilent logo should be always at the front side. Column-identification tag Figure 22 Column-Identification Tag for Left Heat Exchanger Column-identification tag Figure 23 Column-Identification Tag for Right Heat Exchanger 1200 Series TCC User Manual...

  • Page 69: Replacing Head Parts Of Column Switching Valve

    9/64 inch hex key Parts required For parts refer to “Valve Options Overview” on page 76. Isolation seal Rotor seal Stator ring Stator face Spring shows to Stator head rear Stator screws Figure 24 Column Switching Valve Parts 1200 Series TCC User Manual...
  • Page 70 12 Reconnect the pump capillaries to the valve ports. Slide the waste tube into the waste holder in the leak tray. 13 Perform a pressure-tightness test to ensure the valve is pressure tight to 400 bar. 1200 Series TCC User Manual...

  • Page 71: Adding Heater And Cooling Devices (G1316B Sl)

    N O T E column identification system cannot be used. If the column identification system is required, fix the heater and cooling devices in the upper or lower locations or fix them right/left of the current location. 1200 Series TCC User Manual...
  • Page 72 Depending on the column type you have to use different fittings at the heater device inlet capillary. Fitting screw long Swagelock compatible colums (5065-4454, pk of 10, with ferrules) Nut seal tight Swagelock compatible colums, removable (0100-2086) Figure 27 Fitting type depends on column type 1200 Series TCC User Manual...

  • Page 73: Correcting Leaks

    3 Observe the capillary connections and the column switching valve for leaks and correct, if required. 4 Replace the front cover. Column switching valve Column Leak sensor assembly Waste outlet Figure 28 Possible Leak Areas 1200 Series TCC User Manual...

  • Page 74: Replacing The Column Compartment's Firmware

    2.10 or above and the documentation from the Agilent web http://www.chem.agilent.com/scripts/cag_firmware.asp. 2 Load the firmware into the TCC as described in the documentation. The G1316B TCC-SL requires firmware revision A.06.02 or above (main and resident). N O T E 1200 Series TCC User Manual...

  • Page 75: Parts And Materials For Maintenance

    Agilent 1200 Series Thermostatted Column Compartment User Manual Parts and Materials for Maintenance Valve Options Overview Heater and Cooling Devices for G1316B Column Switching Valve 2 Position/6 Port Micro Column Switching Valve 2 Postion/6 Port Micro Column Switching Valve 2 Position/10 Port...

  • Page 76: Valve Options Overview

    Micro Column Switching Valve 2 Position/10 Port 0101-1419 0101-1415 0101-1421 (600 bar) * re-build kit 0101-1258 includes 3-groove rotor seal, stator face assy, isolation seal, instructions. ** re-build kit 0101-1360 includes PEEK rotor seal, PEEK stator face, hex key. 1200 Series TCC User Manual...

  • Page 77: Heater And Cooling Devices For G1316B

    Parts and Materials for Maintenance Heater and Cooling Devices for G1316B The use of these heater and cooling devices is described in Technical Notes or in the Agilent 1200 Series Rapid Resolution LC System (1200 RRLC System) manual. Table 8...
  • Page 78 U-shaped Post-column cooler Volume: 1.6 µl Volume: 1.5 µl mounted on carrier mounted on Carrier (top for column 1, bottom for column 2) holes to attach carrier Figure 29 Heater and Cooling Devices for G1316B 1200 Series TCC User Manual...

  • Page 79: Column Switching Valve 2 Position/6 Port

    Stator screws 1535-4857 Stator Head 0100-1850 Stator face 0100-1851 Stator ring Rotor seal 3 grooves (Tefzel) 0100-1854 Rotor seal 3 grooves (Vespel) 0100-1855 Rotor seal 3 grooves (PEEK) 0100-2233 Isolation seal 0100-1852 1200 Series TCC User Manual...
  • Page 80 Parts and Materials for Maintenance Spring side shows to rear Figure 30 Column Switching Valve Parts 1200 Series TCC User Manual...

  • Page 81: Micro Column Switching Valve 2 Postion/6 Port

    Table 11 Micro Column Switching Valve 2PS/6PT for G1316B SL, 600 bar Item Description Part Number Micro Column Switching Valve 2PS/6PT, 600 bar 0101-1420 Stator, 600 bar 0101-1417 Rotor seal 3 grooves, 600 bar 0101-1409 1200 Series TCC User Manual...

  • Page 82: Micro Column Switching Valve 2 Position/10 Port

    Micro Column Switching Valve 2PS/10PT 600 bar for G1316B SL, 600 bar Item Description Part Number System, Column Switching Valve 2PS/10PT µ-LC 600 bar 0101-1419 Stator, 600 bar 0101-1421 Rotor seal 5 grooves, 600 bar 0101-1415 1200 Series TCC User Manual...
  • Page 83 10/pk fingertight fitting long 5062-8541 10/pk fitting screw long 5065-4454 10/pk fitting screw extra long 5065-9967 10/pk front ferrule 5180-4108 10/pk back ferrule 5180-4114 10/pk Peek tubing 1/16” 0.18 1500 0890-1763 Plastic tubing cutter 8710-1930 1200 Series TCC User Manual...
  • Page 84 Qty [EA] Part number Remark [mm] Hex key 3/32” 8710-2462 Rheotool Socket wrench 2 x 1/4” 8710-2391 * ALS - Autosampler ** TCC - Thermostatted Column Compartment (heat exchanger: 3 µl left or 6 µl right) 1200 Series TCC User Manual...

  • Page 85: Accessory Kits

    Capillary column-heat exchanger 90 mm lg, 0.17 i.d. G1316-87300 (not assembled) contains items 2, 3 and 4 Ferrule front SST, quantity=2 Ferrule back SST, quantity=2 Fitting SST, quantity=2 * re-order 5062-2418, pack of 10 each of fittings, front- and back ferrule 1200 Series TCC User Manual...

  • Page 86: G1316A Accessory Kit (2Ps/10Pt Modules)

    Wrench open end 1/4 – 5/16 inch 8710-0510 Wrench open end, 5/16 – 3/8 inch 8710-2409 PEEK Capillary 280 mm lg, 50 µ i.d., QTY=4 G1316-87309 MIC Valve Fitting, QT=2 5022-2186 Column holder for µ-LC columns, QTY=2 5001-3702 1200 Series TCC User Manual...

  • Page 87: G1316B Sl Accessory Kit (Standard)

    Capillary column-heat exchanger 170 mm lg, 0.17 i.d. G1316-87323 (not assembled) contains items 2, 3 and 4 Ferrule front SST, quantity=2 Ferrule back SST, quantity=2 Fitting SST, quantity=2 * re-order 5062-2418, pack of 10 each of fittings, front- and back ferrule 1200 Series TCC User Manual...

  • Page 88: G1316B Sl Capillary System Kit

    SS Capillary 50 mm x 0.12 mm, m/f G1316-87312 SS Capillary 170 mm x 0.12 mm, m/f G1316-87327 SS Capillary 500 mm x 0.12 mm, m/m G1316-87309 SS Capillary 500 mm x 0.12 mm, m/m G1315-87307 1200 Series TCC User Manual...

  • Page 89: G1316B Sl Micro Valve Kit 2 Position/10 Port

    (not assembled) contains items 2, 3 and 4 Capillary column-heat exchanger 115 mm lg, 0.17 i.d. G1316-87321 (not assembled) contains items 2, 3 and 4 Capillary column-heat exchanger 170 mm lg, 0.17 i.d. G1316-87323 (not assembled) contains items 2, 3 and 4 1200 Series TCC User Manual...

  • Page 90: Column Regeneration Kit

    SS Capillary, 75 mm x 0.12 mm, male/female 1/32 - 1/16, QTY=1 valve to detector G1316-87326 Seat Capillary, 100 mm x 0.12 mm, QTY=2 G1367-87303 PEEK fitting, special for Chip-LC, QTY=1 G4240-43200 Flexible PEEK Tubing, 450 mm x 0.4 mm, QTY=1 valve to waste 5022-6503 1200 Series TCC User Manual...
  • Page 91 Parts and Materials for Maintenance Figure 31 Connection Diagram for Column Regeneration 1200 Series TCC User Manual...

  • Page 92: Plastic Parts

    Parts and Materials for Maintenance Plastic Parts Table 22 Plastic Parts Item Description Part Number Front cover G1316A (1200 Series) G1316-68714 Front cover G1316B SL (1200 Series) G1316-68724 Name plate Agilent (1200 Series) 5042-8901 Figure 32 Plastic Parts 1200 Series TCC User Manual...

  • Page 93: Leak Parts

    Part Number Leak funnel 5041-8388 Leak funnel holder G1316-42300 Waste assembly, includes complete Y-tubing assembly with G1316-60002 leak funnel Waste tubing 1200 mm long (part of accessory kit), re-order 5 m 5062-2463 Figure 33 Leak Parts 1200 Series TCC User Manual...
  • Page 94 Parts and Materials for Maintenance 1200 Series TCC User Manual...
  • Page 95 Agilent 1200 Series Thermostatted Column Compartment User Manual Appendix General Safety Information Lithium Batteries Information Radio Interference Sound Emission Solvent Information Agilent Technologies on Internet This chapter provides addition information on safety, legal and web. Agilent Technologies...

  • Page 96: A Appendix

    Make sure that only fuses with the required rated current and of the specified type (normal blow, time delay, and so on) are used for replacement. The use of repaired fuses and the short-circuiting of fuseholders must be avoided. 1200 Series TCC User Manual...
  • Page 97 Capacitors inside the instrument may still be charged, even though the instrument has been disconnected from its source of supply. Dangerous voltages, capable of causing serious personal injury, are present in this instrument. Use extreme caution when handling, testing and adjusting. 1200 Series TCC User Manual...
  • Page 98 A caution alerts you to situations that could cause a possible loss of data. Do not C A U T I O N proceed beyond a caution until you have fully understood and met the indicated conditions. 1200 Series TCC User Manual...

  • Page 99: Lithium Batteries Information

    WA R N I N G av apparatfabrikanten. Brukt batteri returneres appararleverandoren. Bij dit apparaat zijn batterijen geleverd. Wanneer deze leeg zijn, moet u ze niet weggooien N O T E maar inleveren als KCA. 1200 Series TCC User Manual...

  • Page 100: Radio Interference

    If test and measurement equipment is operated with equipment unscreened cables and/or used for measurements on open set-ups, the user has to assure that under operating conditions the radio interference limits are still met within the premises. 1200 Series TCC User Manual...

  • Page 101: Sound Emission

    This product has a sound pressure emission (at the operator position) < 70 dB. • Sound Pressure Lp < 70 dB (A) • At Operator Position • Normal Operation • According to ISO 7779:1988/EN 27779/1991 (Type Test) 1200 Series TCC User Manual...

  • Page 102: Solvent Information

    • Halogenated solvents or mixtures which form radicals and/or acids, for example: → 2CHCl 2COCl + 2HCl This reaction, in which stainless steel probably acts as a catalyst, occurs quickly with dried chloroform if the drying process removes the stabilizing alcohol. 1200 Series TCC User Manual...
  • Page 103 For example, a 1-% solution of acetic acid in methanol will attack steel. • Solutions containing strong complexing agents (for example, EDTA, ethylene diamine tetra-acetic acid). • Mixtures of carbon tetrachloride with 2-propanol or THF. 1200 Series TCC User Manual...

  • Page 104: Agilent Technologies On Internet

    For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com Select “Products” - “Chemical Analysis” It will provide also the latest firmware of the Agilent 1200 series modules for download. 1200 Series TCC User Manual...
  • Page 105 GLP features, connector locations, cool-down time, cooling concept, parts identification cooling device heaterexchanger leak panels, post column, pre-column, plastics, coumn switching valve (optional) heatexchanger performance location, equilibration time, optimizing, 1200 Series TCC User Manual...
  • Page 106 28, environment, power considerations, power cords, specifications, stack configuration, front view, rear view, status indicators, 46, details, location, system overview, 1200 Series TCC User Manual...
  • Page 108 In This Book This manual contains technical reference information about the Agilent 1200 Series thermostatted column compartment. The manual describes the following: • introcduction and specifications, • installation, • using and optimizing, • troubleshooting overview, • maintenance, • parts identification, •...

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