Agilent Technologies 5100 Site Preparation Manual

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Agilent 5100 and 5110
ICP-OES
Site Preparation Guide

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Summary of Contents for Agilent Technologies 5100

  • Page 1 Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 2 1995), or as a “commercial item” as defined in FAR 2.101(a) or as “Restricted computer software” as defined in FAR 52.227-19 (June 1987) or any equivalent agency regulation or Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 3: Request For Installation

    I understand that if the installation site is not prepared in accordance with the enclosed instructions, additional installation charges may apply. Company name: Company address: Name: Position: Telephone: Preferred installation date: Signed: Date: Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 4: Site Preparation Checklist

     VGA Vapor Generation Accessory  5 Channel Peristaltic Pump  Air Inlet Duct Filter  External Inlet Duct Adapter  Multimode Sample Introduction System (MSIS)  Argon Saturator Accessory (ASA)  Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 5: Table Of Contents

    Compressed Gas Hazards Electrical Hazards Other Precautions Warning Symbols CE Compliance Electromagnetic Compatibility EN55011/CISPR11 ICES/NMB-001 South Korean Class A EMC declaration 2. Introduction Installation Guidelines 3. Laboratory Environment Environmental Conditions Installation category Pollution level Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 6 5. Laboratory Facilities Exhaust System Agilent Exhaust System Electrical Power Supplies Electrical Requirements Single phase requirement Power plugs and cords Other Connections Circuit Breaker Gas Supplies Storage Cylinder Instructions Water Chiller System Location Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 7 Valve SVS 2+ Productivity Package Accessory 5-Channel Peristaltic Pump External Inlet Duct Adapter Vapor Generation Accessory (VGA) Recommended Gases Multimode Sample Introduction System (MSIS) Argon Saturator Accessory (ASA) Appendix A: Power Cords Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 8 Safety Practices and Hazards This page is intentionally left blank. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 9: Safety Practices And Hazards

    The safety practices described below are provided to help the user operate the instrument safely. Read each safety topic thoroughly before attempting to operate the instrument and always operate the spectrometer in accordance with these safety practices. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 10: Plasma

    Agilent’s design criteria. Use of non-approved components in the plasma compartment may render the system inoperative and/or hazardous. It may also invalidate the warranty on the instrument. Use only torches and related components supplied or authorized by Agilent. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 11: Heat, Vapors And Fumes

    Other gases may be required for future options and accessories. Use only ‘instrument grade’ gases with your spectrometer. If using cryogenic gases (for example, liquid argon), prevent severe burns by wearing suitable protective clothing and gloves. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 12: Electrical Hazards

    In case of uncertainty about a specific fluid, that fluid should not be used until confirmation by the manufacturer that it will not present a hazard. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 13 Use only Agilent-supplied spares with your instrument. Only trained operators should use the instrument. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 14: Warning Symbols

    The following symbol may be used on warning labels attached to the instrument. When you see this symbol, refer to the relevant operation or service manual for the correct procedure referred to by that warning label. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 15: Ce Compliance

    Directive and the Machinery Directive (MD) of the European Union. Agilent has confirmed that each product complies with the relevant Directives by testing a prototype against the prescribed EN (European Norm) standards. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 16: Electromagnetic Compatibility

    Relocate the radio or antenna. Move the device away from the radio or television. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 17: Ices/Nmb-001

    의하시기 바라 며 , 가정외의 지역에서 사용하는 것을 목적으 로 합니다 .  After all safety regulations have been met, check the checklist box: Principal installation area is in compliance with all relevant safety regulations. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 18 Safety Practices and Hazards This page is intentionally left blank. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 19: Introduction

    The installation will include the following: Spectrometer installation  Water chiller connection  Instrument software installation and registration  Accessory installation  Spectrometer installation performance tests  Basic customer training  Maintenance overview  Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 20 Introduction This page is intentionally left blank. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 21: Laboratory Environment

    The pollution level is 2, based on IEC61010-1. Pollution level describes the degree to which a solid, liquid or gas that deteriorates dielectric strength is adhering. ‘2’ applies to a normal indoor atmosphere, where only non-conductive pollution occurs. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 22: Temperature Control

    This is equivalent to a very clean office.  After the cleanliness requirements have been met, check the checklist box: Laboratory is free of excessive particulate matter. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 23: Instrument Cooling Air Supply

    If an external cooling air supply system is required, an air inlet duct attachment NOTE must be ordered with the instrument.  After the instrument cooling air supply requirements have been met, check the checklist box: Cooling air system is set up. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 24: Workbench

    Generally, for comfortable working conditions and easy access to the instrument sample introduction system, Agilent recommends that the height of the workbench be approximately 900 mm (36 in) high. Refer to Figure 1. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 25: Location

    The following diagrams show the relative dimensions of the main instrument including the space needed for service access. These dimensions should be considered during the preparation for installation of your spectrometer. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 26 The location of the workbench may be determined by the position of the exhaust flue required to remove fumes and vapors from the spectrometer sample compartment (see Section 4). Figure 2. Front view of instrument Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 27 Laboratory Environment Figure 3. Top view of instrument Figure 4. Rear view of instrument Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 28: Pc Requirements

    Windows 7 Professional 64-bit Windows 7 Professional 64-bit Higher rated PC components can be substituted for those listed above for example, processor type, amount of memory, screen size and resolution and operating system version. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 29: Instrument Shipping Information

    Figure 5 provides an indication of the minimum turning clearance and minimum door width required for the spectrometer in its shipping crate. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 30 After the in-house transit route requirements have been met, check the checklist box: Entrance to the lab is at least 1050 mm (41.3 in) wide for packaged instrument, or 800 mm (31.5 in) wide for unpackaged instrument. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 31: Insurance After Delivery

    500 mm 840 mm 31 kg 29.9 in 19.7 in 33.1 in 68.4 lb SPS 3 and SPS 4 trolley 580 mm 412 mm 400 mm 23 in 17 in 16 in Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 32 The Agilent ICP-OES weighs approximately 106 kg (234 lb). To avoid injury to personnel or damage to equipment, always use a fork lift or other suitable lifting device when moving the instrument. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 33: Transit Damage

    In transit, sharp jolts and shocks must be avoided and the packages must not be inverted or tilted unnecessarily. Markings on the shipping cartons generally indicate the required orientation of the carton. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 34: Seismic Requirements

    Seismic brackets are not supplied by Agilent. Prepare these items separately. NOTE Right side Left side 3 mm 30 mm 17 mm Bracket (example) Figure 6. Slots for seismic tie down Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 35: Laboratory Facilities

    The external vent must be fitted with a back draft damper and the outlet location must be clear of doors, windows and heater or air- conditioning units. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 36: Agilent Exhaust System

    To allow for personal preferences, control gear switch and pilot light assemblies are not supplied by Agilent. Table 3. Agilent exhaust kits Exhaust kit Exhaust kit for 240 V, 50 Hz supply Exhaust kit for 115 V, 60 Hz supply Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 37 Exhaust fan (for 115 V, 60 Hz supply only) Flexible ducting 1 meter length, aluminum Coupling for joints in ducting Ducting clamp two required per coupling Figure 8. Agilent exhaust kit components Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 38 Installation instructions for the exhaust fan are included with the Agilent-supplied Exhaust Kit.. Figure 9 details exhaust fan wiring information for the 115 V 60 Hz fan only. Figure 9. Electrical wiring information for 115 VAC 60 Hz fan only Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 39: Electrical Power Supplies

    Avoid using power supplies from a source that may be subject to electrical interference from other services (such as large electric motors, elevators, welders and air conditioning units). Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 40: Electrical Requirements

    The Agilent ICP-OES is supplied with a power cord set appropriate for the country from which the order originates. For example, if an order originates from an Agilent Technologies sales office in Germany, the power cord and plug supplied will be compatible with the standard voltage and outlet configuration in Germany.
  • Page 41: Other Connections

    Gas Supplies The installation of compressed or liquid gas supplies must comply with the rules and/or regulations imposed by the local authorities responsible for such use in the workplace. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 42 <5 ppm Nitrogen (argon only) <20 ppm Water vapor <4 ppm <4 ppm Permissible pressure range* 500–600 kPa (73–88 psi) Recommended pressure* 550 kPa (80 psi) regulated *When supplying required gas flows Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 43: Storage Cylinder Instructions

    Fittings for the regulator end must be supplied by the customer. Alternatively, a fittings kit can be ordered from Agilent Technologies. See the Agilent website at www.agilent.com for ordering information. Customers will provide connection from the gas supply to a shutoff valve.
  • Page 44: Water Chiller System

    Solid State RF oscillator, load coil, camera Peltier assembly and Axial sample cone interface. The instrument incorporates an in-line particulate filter and water flow sensors on the water supply line. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 45 400 kPa (58 psi) Pressure regulation is recommended for water chiller systems that may exceed NOTE the maximum permissible pressure of 400 kPa (58 psi) or may be subject to pressure fluctuations. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 46: Location

    Please see the Agilent website for part numbers for ordering additional hose by the meter and clamps: www.agilent.com  After the water cooling requirements have been met, check the checklist box: Water cooling/circulation system and power connections are set up. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 47: Waste Fluid Container

    Initial instrument software installation is also included as part of the system installation. For information on installing the Agilent ICP-OES system software, consult the ICP Expert software installation instructions or the ICP Expert CFR software installation instructions supplied with the instrument software. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 48 Laboratory Facilities This page is intentionally left blank. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 49: Accessories And Options

    Environmental Conditions The SPS accessory is suitable only for indoor use. The site should be selected to avoid dusty or corrosive atmospheres. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 50: Advanced Switching Valve-Avs 4, Avs 6 Or Avs 7 Switching Valve

    (or dilution) effects are minimized. SVS 2+ Productivity Package Accessory For safety information and to prepare the SVS 2+ for installation, please see the instructions that came with the accessory. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 51: 5-Channel Peristaltic Pump

    The VGA allows a 45 mL/min flow of argon to pass through it even when it is NOTE switched off. It is recommended that the argon gas line is fitted with a stop valve to shut off the gas supply to the VGA. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 52: Multimode Sample Introduction System (Msis)

    This has been found to be beneficial by reducing the build-up of salt and other dissolved solids in the sample introduction system. By reducing blockages, the ASA helps to ensure uninterrupted, maintenance-free operation. Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 53: Appendix A: Power Cords

    UK / Hong Kong / Singapore, BS 1363 (Agilent Part Number 8120-8620) Switzerland / Denmark, 1302 (Agilent Part Number 8120-8622) Australia, AS 3112 (Agilent Part Number 8120-8619) China, GB 1002 (Agilent Part Number 8121-0070) Argentina, IRAM 2073 (Agilent Part Number 8121-0675) Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 54 Israel, SI 32 (Agilent Part Number 8121-0161) Japan, NEMA L6-20P (Agilent Part Number 8120-6903) Taiwan/S America, NEMA 6-20P (Agilent Part Number 8120-6360) Europe/Korea, CEE7 VII (Agilent Part Number 8121-1222) Thailand, NEMA 5-15P (Agilent Part Number 8121-1301) (Not Shown) Agilent 5100 and 5110 ICP-OES Site Preparation Guide...
  • Page 56 In This Book The manual describes the following: Safety Practices and Hazards  Introduction  Laboratory Environment  Requirements Instrument Shipping Information  © Agilent Technologies 2014, 2016 03/16 *G8010-90001* *G8010-90001* G8010-90001 Issue 2...

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