Agilent Technologies 5973N Site Preparation Manual
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Agilent Technologies 5973N Site Preparation Manual

Mass selective detectors
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5973N and 5973 inert
Mass Selective
Detectors
Site Preparation Guide
Agilent Technologies

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Summary of Contents for Agilent Technologies 5973N

  • Page 1 5973N and 5973 inert Mass Selective Detectors Site Preparation Guide Agilent Technologies...
  • Page 2 Notices © Agilent Technologies, Inc. 2003 Warranty Safety Notices No part of this manual may be reproduced in The material contained in this docu- any form or by any means (including elec- ment is provided “as is,” and is sub-...

  • Page 3: Table Of Contents

    Contents General Information Instrument Identification 5973N MSD version 5973 inert MSD version Important Safety Warnings Many internal parts of the MSD carry dangerous voltages Electrostatic discharge is a threat to MSD electronics Many parts are dangerously hot Hydrogen Chemical safety...
  • Page 4 Communications Requirements Telephone Building network Electrical Requirements Voltage ranges of major components Power configurations Power requirements Power plugs and cords Other electrical considerations Air Conditioning Requirements Temperature and humidity Airborne dust Exhaust venting Fume (exhaust) hood Carrier and Reagent Gas Requirements Regulators, tubing, and fittings Laboratory Supply Requirements Cleaning solvents...
  • Page 5 5973N and 5973 inert Mass Selective Detectors Site Preparation Guide General Information Instrument Identification Important Safety Warnings Safety and Regulatory Certifications Cleaning Recycling the Product This section provides information on how to identify specifically what type of MSD you are working with as well as how to properly clean and dispose of the instrument.

  • Page 6: General Information

    10-character serial numbers. Write the serial number of your 5973 MSD here for reference: 5973N MSD version The 5973N MSD is equipped with a diffusion pump. The serial number label displays a product number that tells what kind of MSD you have:...

  • Page 7: Important Safety Warnings

    General Information Important Safety Warnings Before moving on, there are several important safety notices that you should always keep in mind when using the 5973 Series Mass Selective Detector. Many internal parts of the MSD carry dangerous voltages If the MSD is connected to a power source, even if the power switch is off, potentially dangerous voltages exist on: •...

  • Page 8: Electrostatic Discharge Is A Threat To Msd Electronics

    General Information Make sure the power cords supplied with the MSD are appropriate for your country and site before using them. Maintain easy access to the power cords so they can be disconnected during maintenance. The use of incorrect or makeshift fuses or the short-circuiting of fuse holders creates a shock hazard for the operator and can damage the instrument.

  • Page 9: Hydrogen

    General Information Be careful when working behind the gas chromatograph (GC). WA R N I N G During cool-down cycles, the GC emits hot exhaust which can cause burns. The insulation around the GC inlets, detectors, valve box, and the WA R N I N G insulation cups is made of refractory ceramic fibers.

  • Page 10: Chemical Safety

    General Information When using hydrogen gas, check the system for leaks as described by your local Environmental Health and Safety (EHS) requirements to prevent possible fire and explosion hazards. Always check for leaks after changing a tank or servicing the gas lines.

  • Page 11: Safety And Regulatory Certifications

    The 5973 Series Mass Selective Detector is designed and manufactured under a quality system registered to ISO 9001. Information The Agilent Technologies 5973 Series Mass Selective Detector meets the following IEC (International Electro-technical Commission) classifications: Safety Class I, Transient Overvoltage Category II, Pollution Degree 2.

  • Page 12: Symbols

    Failure to comply with these precautions violates safety standards of design and the intended use of the instrument. Agilent Technologies assumes no liability for the customer’s failure to comply with these requirements. See accompanying instructions for more information.

  • Page 13: Electromagnetic Compatibility

    4 Make sure that all peripheral devices are also certified. 5 Make sure that appropriate cables are used to connect the device to peripheral equipment. 6 Consult your equipment dealer, Agilent Technologies, or an experienced technician for assistance. 7 Changes or modifications not expressly approved by Agilent Technologies could void the user’s authority to operate the...

  • Page 14: Cleaning

    General Information Cleaning To clean the unit, disconnect the power and wipe down with a damp, lint-free cloth. Recycling the Product For recycling, contact your local Agilent sales office. Site Preparation Guide...

  • Page 15: Site Preparation

    5973N and 5973 inert Mass Selective Detectors Site Preparation Guide Site Preparation Overview Space and Weight Requirements Communications Requirements Electrical Requirements Air Conditioning Requirements Carrier and Reagent Gas Requirements Laboratory Supply Requirements Receiving the System Installation and Verification This section describes how to properly prepare your site for a new MSD.

  • Page 16: Overview

    Delays due to inadequate site preparation could cause loss of instrument use during the warranty period. In extreme cases, Agilent Technologies may ask to be reimbursed for the additional time required to complete the installation. Agilent Technologies provides service during the warranty period and under maintenance agreements only if the specified site requirements are met.

  • Page 17: Agilent Responsibility

    • Providing someone to help lift the MSD onto the laboratory bench • Providing adequate secure storage space for the system until it can be installed by an Agilent Technologies representative Agilent responsibility An Agilent Technologies service representative will install the MSD and verify its performance.
  • Page 18 • Connecting or verifying the performance of hardware and software not provided by Agilent Technologies Items that do not include installation by Agilent Technologies must be N O T E installed by the customer. • Connecting the MSD/ChemStation system to the building network •...

  • Page 19: Other Documentation

    Additional information is contained in the following documentation: • 5973N or 5973 inert Mass Selective Detector Hardware Manual, which is located on the 5973N and 5973 inert Mass Selective Detector User Information CD-ROM • 5973 Network Mass Selective Detector Site Preparation...

  • Page 20: Space And Weight Requirements

    Site Preparation Space and Weight Requirements Table 1 lists dimension and weight information for the MSD and related components. Your site must have enough bench space for the MSD, GC, data system, and accessories. In addition, there must be sufficient space around the system for ventilation and maintenance access.
  • Page 21 Site Preparation Table 1 Product dimensions Product Dimensions, cm (in) Height Width Depth Weight, kg (lb) † 5973 Series MSD G2577A Diffusion pump EI MSD 40.6 (16) 29.8 (11.75) 54 (21.25) 36 (80) G2578A Standard turbo EI MSD 40.6 (16) 29.8 (11.75) 54 (21.25) 39 (85)

  • Page 22: Communications Requirements

    If you intend to connect your MSD system to your building’s network, you must have an additional shielded twisted pair (STP) network cable. Agilent Technologies is not responsible for connecting to or establishing N O T E communication with your building network. The representative will test the 5973 Series MSD’s ability to communicate on a mini-hub only.

  • Page 23: Electrical Requirements

    For example, if an order originates from an Agilent Technologies sales office in Germany, the foreline pump supplied will be configured to operated on the standard voltage and frequency of electrical power in Germany.

  • Page 24: Power Configurations

    Site Preparation If an instrument is being ordered from one location, but is to be C A U T I O N installed in another location with different electrical power characteristics, this must be noted on the order. A special note must also be made if the electrical power at the site is different from the standard electrical power in that country.

  • Page 25: Power Requirements

    Site Preparation Table 2 Power configurations Configuration Measurement Nominal voltage Single phase, Line to neutral 120 VAC 120 VAC Line to ground 120 VAC* Ground to neutral < 0.5 V rms Single phase, Line to neutral 200, 220, or 240 VAC* 200-240 VAC Line to ground 200, 220, or 240 VAC*...

  • Page 26: Power Plugs And Cords

    The MSD is supplied with a power cord and plug appropriate for the country from which the order originates. For example, if an order originates from a Agilent Technologies sales office in Germany, the power cord and plug supplied will be compatible with the standard voltage and outlet configuration in Germany.

  • Page 27: Other Electrical Considerations

    Site Preparation Power cord lengths for the MSD and the data system components and accessories are approximately 2.3 m (7.5 ft). If an instrument is being ordered from one location, but is to be C A U T I O N installed in another location with different electrical power characteristics, this must be noted on the order.
  • Page 28 Site Preparation • Provide separate convenience outlets for building maintenance and other appliances. Convenience outlets must be on circuits separate from the MSD system. Convenience outlets must share the normal building distribution ground, not the MSD system ground. • In some geographical areas it may be advisable to install lightning protection for personnel and equipment.

  • Page 29: Air Conditioning Requirements

    Site Preparation Air Conditioning Requirements Air conditioning considerations include temperature, humidity, airborne dust, and exhaust venting. Each of these is considered in more detail in the following material. Temperature and humidity The 5973 Series MSD is specified for operation under the following conditions: •...

  • Page 30: Airborne Dust

    Site Preparation Airborne dust Agilent Technologies recommends a maximum airborne particle density of 55 µg/m . If you suspect your site exceeds this limit, contact your local Agilent Technologies Customer Service Organization. Customer Engineers with special training and equipment can test for airborne particle density. They can offer suggestions for reducing airborne dust.

  • Page 31: Fume (Exhaust) Hood

    Site Preparation If a negative pressure vent is not available, the length of tubing from the foreline pump to an ambient pressure vent should not exceed 460 cm (15 ft). The exhaust can be connected to a positive pressure vent. Exhaust gas venting must comply with all local environmental and safety codes.

  • Page 32: Carrier And Reagent Gas Requirements

    Site Preparation Carrier and Reagent Gas Requirements Table 5 lists the specifications for the carrier and reagent gases. Table 5 Carrier and reagent gas requirements Purity Typical pressure range (psi) Typical flow (mL/min) Helium 99.999% or better and 50 to 80 20 to 50 (column and split flow) (required) hydrocarbon free...

  • Page 33: Regulators, Tubing, And Fittings

    The regulator must be able to supply gas in the specified pressure range. It must have one outlet with 1/4-inch Swagelok fittings. See the Agilent Technologies Chemical Analysis Columns and Supplies Catalog or visit the Agilent Technologies Chemical Analysis website at http://www.agilent.com/chem for dual-stage regulators...

  • Page 34: Laboratory Supply Requirements

    Site Preparation Laboratory Supply Requirements Laboratory supply requirements vary with applications. Cleaning solvents Cleaning tasks for the MSD require the following HPLC-grade (or better) solvents: • Methylene chloride • Isopropyl alcohol • Methanol • Acetone • Water Proper storage, handling, and disposal of these chemicals is required for personal and environmental safety.

  • Page 35: Spare Parts And Consumables

    Site Preparation Agilent Technologies does not include CD writers with MSD systems. N O T E These are available from many suppliers. Spare parts and consumables The supplies and parts listed in Table 6 are used in the operation and maintenance of a 5973 Series MSD system.
  • Page 36 Site Preparation Table 6 Maintenance supplies and consumables (continued) EI filament (2/pk) 05972-60053 EI high temp filament G2590-60053 Chemical Consumables PFTBA (EI calibration fluid) 05971-60571 PFDTD (CI calibration fluid) 8500-8130 EVAL A (evaluation sample) 05990-60045 OFN (Octafluoronapthalene) 8500-5441 Benzophenone 8500-5440 Diffusion pump fluid (2 required) 6040-0809 Foreline pump oil, Inland 45, 1 liter...
  • Page 37 Site Preparation Table 6 Maintenance supplies and consumables (continued) 0.4-mm id, 85% Vespel 15% graphite, for 0.20-mm id and 5062-3508 0.25-mm id columns 0.5-mm id, 85% Vespel 15% graphite, for 0.32-mm id 5062-3506 columns 0.8-mm id, 85% Vespel 15% graphite, for 0.53-mm id 5062-3538 columns Injection port...

  • Page 38: Receiving The System

    Site Preparation Receiving the System When your MSD system is delivered, it is your responsibility to provide for removal of the shipping containers from the truck and their storage until installation. Contact your Agilent Technologies service representative as soon as your shipment arrives to arrange an installation date.

  • Page 39: Storage

    Site Preparation Do not open any of the shipping containers unless a representative of Agilent Technologies is present. Opening any of the containers without an Agilent Technologies representative being present will void the receiving warranty on the instrument. Storage It is your responsibility to store the containers until installation.

  • Page 40: Installation And Verification

    Once the installation has begun, it should progress in a timely manner to completion. Delays due to inadequate site preparation could cause loss of instrument use during the warranty period. In extreme cases, Agilent Technologies may ask to be reimbursed for the additional time required to complete the installation.

  • Page 41: Sensitivity Specifications

    Site Preparation Sensitivity specifications See the appropriate sensitivity specifications for your instrument type: 5973N: Request Agilent publication 5968-7358E 5973 inert: Request Agilent publication 5988-9991EN SIM performance verification is not performed at installation and must be N O T E purchased if desired.
  • Page 42 Site Preparation Site Preparation Guide...
  • Page 43 5973N and 5973 inert Mass Selective Detectors Site Preparation Guide Power Cords This appendix shows the power cords available for the 5973 Series MSD. See page 26 for information about ensuring that the correct power cord is supplied with your system.
  • Page 44 Power Cords UK / Hong Kong, BS 1363 (Part number 8120-1351) Denmark/Greenland, IEC 309 (Part number 8120-3997) Australia / New Zealand, AS 3112-1981 (Part number 8120-1369) India / South Africa, BS 546 (Part number 8120-4211) Israel, SI 32 (Part number 8120-5182) Site Preparation Guide...
  • Page 45 Power Cords Japan, NEMA L6-20P (Part number G2025-60189) Site Preparation Guide...
  • Page 46 Power Cords Site Preparation Guide...
  • Page 48 Agilent Technologies © Agilent Technologies, Inc. Printed in USA, August 2003 G2589-90070...

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5973 inert

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