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Waters HPLC manual available for free PDF download: Installation And Maintenance Manual
Waters HPLC Installation And Maintenance Manual (198 pages)
Brand:
Waters
| Category:
Laboratory Equipment
| Size: 1.88 MB
Table of Contents
Copyright Notice
2
Trademarks
2
Customer Comments
3
Safety Considerations
3
Safety Advisories
4
Operating this Instrument
4
Audience and Purpose
4
Intended Use of the Waters Prep Series HPLC System
5
Calibrating
5
ISM Classification
5
ISM Classification: ISM Group 1 Class B
5
EC Authorized Representative
6
Table of Contents
7
1 Overview
11
Waters Prep Series
12
Preplc System
12
Delta-Prep System
13
Waters Prep Series
13
Delta-Prep
14
Waters Prep Series Modules
15
Inject Start
19
Waters 746 Integrator
20
Chassis Ground
21
Signal Ground
21
Accessories
23
Getting Started
24
Starting the System
24
Using the Front Panel
26
Displaying Help
29
Shutting down the System
29
Configuring the Controller
29
2 Installing the System
35
Setting up and Inspecting
36
Unpacking and Installing the System
36
Selecting the Site
37
Electrical Requirements
39
Electrical Conditions
39
Voltage Selections
39
Assembling the System
41
Connecting Rheodyne Injectors
41
Connecting the M-1000 Preppak Module (Optional)
43
Connecting Additional Devices
43
Attaching the Interface Cable and Power Cord
47
Connecting IEEE-488 Interfaces
49
Connecting to the Waters 746 Data Module
54
Liquid Line Connections
55
Connecting a Helium Tank to the Fluid Handling Unit
64
Helium Specifications
64
Sparging
65
Connecting Compression Fittings
65
Setting up the Plunger Wash
67
Considerations
68
Connecting the Plunger Wash Tube
68
Connecting to the Injection Panel (Preplc System)
69
Connecting to the Column Rack (Delta-Prep System)
71
Installing Sample Injection Options
74
Installing the Small-Scale Sample Injection Valve Option (Preplc System)
74
Using an Autoinjector
75
Making Electrical Connections
75
Connecting Liquid Lines When Using a Waters Autoinjector
75
Connecting a Fraction Collector
76
Making the Remote Start Connection
76
Making Chart Mark Connections
76
Installing Analytical and Preparative Columns
77
Preplc System
77
Delta-Prep System
79
Making Detector Connections
82
Preplc or Delta-Prep System
82
Connecting Detector Semi-Prep Cells
82
Using the RI Detector with the Flow Splitter Option
83
3 Troubleshooting, Testing, and Maintenance
85
Troubleshooting
86
Troubleshooting Steps
86
Troubleshooting Flowcharts
87
Troubleshooting Flowcharts
89
Baseline Noise
89
High System Pressure
91
Troubleshooting Chromatography
93
Poor Peak Resolution
97
Chromatography Troubleshooting
100
Hardware Troubleshooting
107
Software Troubleshooting
115
Replace with New Table
116
Illegal Vial Number
117
Number out of Range
117
Program Method Table Saved
117
Step Does Not Exist
117
First Vial Greater than Last Vial
118
Invalid Injection Number
118
Invalid Vial Number
118
Performance Tests
120
Self-Diagnostics
120
Extended Tests
121
Maintenance Procedures
131
Column Rack Tubing Configuration
131
Fluid Handling Unit Maintenance
132
Replacing Fuses
151
Maintaining Rheodyne Manual Injectors
155
Warning Symbols
161
A Safety Advisories
162
Warning Symbols
162
Task-Specific Hazard Warnings
162
Specific Warnings
163
Caution Symbol
165
Warnings that Apply to All Waters Instruments
166
Electrical and Handling Symbols
172
Electrical Symbols
172
Handling Symbols
173
B Specifications
175
C Spare Parts
179
Gradient
180
D Solvent Considerations
182
Clean Solvent
182
Solvent Miscibility
183
Viscosity
183
How to Use Miscibility Numbers (M-Numbers
185
Buffered Solvents
186
Solvent Head Height
186
Solvent Viscosity
186
Solvent Degassing
187
Solvent Degassing Methods
188
Index
191
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