Veolia Sievers TOC-R3 Manuals

Manuals and User Guides for Veolia Sievers TOC-R3. We have 2 Veolia Sievers TOC-R3 manuals available for free PDF download: Operation And Maintenance Manua, Installation Manual

Veolia Sievers TOC-R3 Operation And Maintenance Manua (285 pages)

Online TOC Analyzer 1.16 firmware or later

Brand: Veolia | Category: Measuring Instruments | Size: 29 MB

Identification Records
3
Table of Contents
5
List of Tables
15
List of Figures
16
Confidentiality
19
Declaration of Conformity
19
Revision History
19
Standard Limited Warranty
19
Trademarks and Patents
19
English
24
Warnings
24
Chapter 1: Introduction

28
Chapter 2: System Description

30
- System Specifications
  30
- Important
  31
- Applications
  31
- Analyzer Highlights
  31
- Additional System and Operating Specifications
  32
- Carrier Gas
  32
- Reagent
  32
- Dilution and Rinsing Water
  33
- Analytical Methods Supported
  33
- Measurement Ranges
  33
- Sample Information
  33
- Communication
  34
- Electrical
  34
- Reagent Consumption
  34
- Compliance
  35
- System Overview
  35
- Analyzer Enclosure Rating - IP54
  35
- Major Subsystems
  35
- Optional Subsystems and Hardware
  36
- Sievers TOC-R3
  36
- Theory of Operation
  37
- TOC Parameter
  37
- Total Nitrogen (Tnb) Parameter
  38
- Measurement Principle
  38
- Carbon Measurements
  38
- Included Standard Operation Analytical Methods
  38
- Figure 2-1: Carbon Measurement Process Diagram
  38
- TC Method
  39
- NPOC Method
  39
- Purchasable Analytical Methods
  39
- TIC Method
  39
- TOC Diff Method (TOC)
  40
- TOC Add Method
  40
- Purgeable/Volatile Organic Carbon (POC/VOC) Measurement
  40
- Tnb Measurement
  40
- Sample Flow Path
  41
- Flow Diagram
  41
- Figure 2-2: Flow Diagram
  41
- Flow Path Components
  42
- B1 - NDIR Detector
  42
- Detection)
  42
- B2 - ECD Detector Option (for no Detection)
  43
- Table 2-1: Typical NDIR Detector Measuring Ranges
  43
- B2 - PID Detector Option (for POC/VOC Detection)
  44
- Table 2-2: Typical ECD Detector Measuring Ranges
  44
- Sensors
  45
- CM1 - Injection Accumulator
  45
- Table 2-3: Typical PID Detector Measuring Range
  45
- CM2 - Multi-Function Sample Vessel
  46
- EB1 - Furnace
  46
- EC1 - Gas Cooler Unit
  46
- Pumps
  46
- Filters
  47
- KH1 - Pressure Regulator
  47
- MFSV Vent
  48
- RM1 - Check Valve
  48
- Nozzles
  48
- Valves
  48
- Table 2-4: Valves List
  48
- Wetted Materials
  49
- Table 2-5: Wetted Materials List
  49
- Additional System Components
  51
- Microprocessor Controller and Electronics
  51
- Data Inputs / Outputs
  51
- Ethernet
  52
- Digital Input
  52
- Relay
  52
- Analog Output
  52
- Options and Accessories
  53
- Air Box
  53
- Coalescing Air Filter
  53
- Intake Air Filter
  53
- Air Scrubber
  53
- Sievers TOC-R3
  53
- Soda Lime
  53
- Activated Carbon
  54
- Communication Box
  54
- Particulate Sampler
  54
- Mounting Rack
  54
Chapter 3: Installation

56
Chapter 4: Basic Analyzer Operation

96
- Overview
  96
- Principles of Operation
  96
- Measurement Technique
  96
- Carbon Measurements
  96
- Poc/Voc
  97
- Tnb
  97
- Powering on and off the Analyzer
  97
- To Power on the Analyzer
  97
- To Shut down the Analyzer
  98
- Figure 4-1: Rotary Power Switch (off Position)
  98
- Rebooting the Analyzer
  99
- To Reboot the Analyzer
  99
- Power Cycling the Analyzer
  99
- To Power Cycle the Analyzer
  99
- Recommended Operational State
  100
- Figure 4-2: Rotary Power Switch
  100
- The Analyzer Menus and Screens
  101
- Navigating the Analyzer Screens
  101
- Touchscreen Components
  102
- Figure 4-3: Touchscreen Components
  102
- Table 4-1: Left Panel Icons
  103
- Table 4-2: Navigation Icons
  103
- To Unlock the Analyzer Touchscreen
  104
- Figure 4-4: PIN Dialog
  104
- Figure 4-5: Machine Unlocked Dialog
  104
- To Lock the Analyzer Touchscreen
  105
- Access to Functions While Locked
  105
- Figure 4-6: Confirm Lock Dialog
  105
- Data Inputs/Outputs from the Analyzer
  106
- Using the USB Port
  106
- To Take a "Screenshot
  106
- To "Unmount" the USB Memory Device
  107
- Using the Ethernet Port
  107
- Main Screen Selections
  107
- Table 4-3: Main Screens
  107
- Figure 4-7: Remove USB Dialog
  107
- Dashboard Screen
  108
- Figure 4-8: Dashboard Screen (Online View Example)
  108
- System Information Screen
  109
- Figure 4-9: System Information Screen
  109
- Acknowledging Errors
  110
- To Acknowledge Error(S)
  110
- Table 4-4: Status Icons and Actions
  110
- Figure 4-10: System Information Screen with Alerts (Example)
  111
- Figure 4-11: "Sampling" Functional Module Displaying Alerts (Example)
  111
- Figure 4-12: "Software" Functional Module "E1" Error Example
  112
- Figure 4-13: "Sampling" Functional Module "E2" Warning Example
  113
- Figure 4-14: "Sampling" Functional Module "E3" Maintenance Request Example
  113
- Maintenance Screen (Cockpit)
  114
- Figure 4-15: Maintenance Screen (Cockpit)
  114
- Gas Way
  115
- Soda Lime
  115
- Fan Filter
  116
- Sievers TOC-R3
  116
- Cartridge
  116
- Pump Tubing
  117
- Absorber
  117
- Menu Screen
  117
- Menu → Settings
  118
- Figure 4-16: Menu Screen
  118
- Measurement
  119
- Figure 4-17: Menu → Settings
  119
- Figure 4-18: Menu → Settings → Measurement
  119
- Signal Integration
  121
- Figure 4-19: Menu → Settings → Signal Integration (Defaults Displayed)
  121
- Methods
  123
- Figure 4-20: Injection Timing VS Integration
  123
- Figure 4-21: Menu → Settings → Methods
  124
- Calibration
  125
- Figure 4-22: Menu → Settings → Calibration
  125
- Limits
  126
- Figure 4-23: Injection Timing VS Integration
  126
- Figure 4-24: Menu → Settings → Limits (NPOC)
  127
- Figure 4-25: Menu → Settings → Limits (TC)
  127
- Auto Calibration
  128
- Figure 4-26: Menu → Settings → Auto Calibration
  128
- Check Function
  129
- Figure 4-27: Menu → Settings → Check Function
  129
- Rinsing
  130
- Figure 4-28: Menu → Settings → Rinsing
  131
- Menu → Service
  132
- Figure 4-29: Menu → Service
  132
- Signal
  133
- Result
  133
- Figure 4-30: Menu → Service → Signal → Signal
  133
- Sensors
  134
- Figure 4-31: Menu → Service → Signal → Result
  134
- Table 4-5: Sensor Details and Normal Readings
  135
- Figure 4-32: Menu → Service → Sensors
  135
- Valve Control
  136
- Pump Control
  137
- Figure 4-33: Menu → Service → Valve Control
  137
- Figure 4-34: Menu → Service → Pump Control
  138
- Analog Output
  139
- Figure 4-35: Menu → Service → Analog Output
  139
- To Set up the Analog Output(S)
  140
- Digital Input
  141
- Figure 4-36: Menu → Service → Analog Output → Test
  141
- To Set up the Digital Input(S)
  142
- Figure 4-37: Menu → Service → Digital Input
  142
- Relay
  143
- To Set up the Relay(S)
  144
- Figure 4-38: Menu → Service → Relay
  144
- Table 4-6: Digital Relay Condition Codes and Descriptions, Short List
  145
- Figure 4-39: Menu → Service → Relay → Relay Definition Screen
  145
- Furnace Control
  147
- To Check the Furnace Temperature While the Furnace Is off
  147
- Figure 4-40: Menu → Service → Furnace Control
  147
- Maintenance
  148
- Menu → Archive
  148
- Figure 4-41: Menu → Service → Maintenance
  148
- System Log
  149
- Figure 4-42: Menu → Archive
  149
- Error Log
  150
- Figure 4-43: Menu → Archive → System Log
  150
- Figure 4-44: Menu → Archive → Error Log
  150
- Measurement Log
  151
- Figure 4-45: Menu → Archive → Measurement Log
  151
- Measurement History
  152
- Figure 4-46: Menu → Archive → Measurement Log → Details
  152
- Calibration Log
  153
- Figure 4-47: Menu → Archive → Measurement History
  153
- Calibration Log Details Screen
  154
- Figure 4-48: Menu → Archive → Calibration Log
  154
- Figure 4-49: Menu → Archive → Calibration Log → Details
  154
- Menu → General
  155
- System Settings
  156
- Language
  156
- Figure 4-50: Menu → General
  156
- Figure 4-51: Menu → General → System Settings
  156
- Factory Settings
  157
- Dark Mode
  157
- Connectivity
  157
- Auto Lock
  157
- Auto Lock Duration
  157
- Sievers TOC-R3
  157
- Machine PIN
  157
- Stream 1 Name
  158
- Stream 2 Name
  158
- Info
  158
- Machine Configuration
  158
- Figure 4-52: Menu → General → Info
  158
- Figure 4-53: Menu → General → Machine Configuration
  159
- Time/Date Settings
  160
- Software
  160
- Figure 4-54: Menu → General → Time/Date Settings
  160
- Ethernet
  161
- Figure 4-55: Menu → General → Software
  161
- Offline Mode
  162
- Figure 4-56: Menu → General → Ethernet
  162
- Running a Calibration in Offline Mode
  163
- Figure 4-57: Dashboard → Offline Mode
  163
- Settings
  164
- Figure 4-58: Dashboard → Offline Mode → Calibration → Settings
  164
- Figure 4-59: Dashboard → Offline Mode → Calibration →Signal
  165
- Figure 4-60: Dashboard → Offline Mode → Calibration →Result
  165
- Running a Grab Sample in Offline Mode
  166
- Figure 4-61: Dashboard → Offline Mode → Calibration →Fit
  166
- Figure 4-62: Dashboard → Offline Mode → Sample → Settings
  167
- Figure 4-63: Dashboard → Offline Mode → Sample → Signal
  167
- Online Mode
  168
- Running in Online Mode
  168
- Figure 4-64: Dashboard → Offline Mode → Sample → Result
  168
- Figure 4-65: Dashboard → Online Mode (Example)
  169
Chapter 5: Method Development

170
- Overview
  170
Chapter 6: Maintenance

172
- Overview
  172
- Reagent Considerations and Preparation
  173
- Acid Type by Analytical Method
  173
- Primary Analytical Methods
  173
- Table 6-1: Primary Analytical Methods and Acid Type
  173
- Secondary Analytical Methods
  174
- Table 6-2: Secondary Analytical Methods and Acid Type
  174
- Acid Preparation
  175
- 1% Hydrochloric Acid (Hcl)
  175
- 1% Phosphoric Acid (H 3 PO 4 )
  175
- Calibration Standards
  176
- Stock Composition
  176
- Standards Preparation
  176
- Mg/L TC Standard
  176
- 1,000 Mg/L TIC Standard
  176
- Mg/L Tnb Standard (50/50 Blend of (NH so and KNO )
  177
- 250 Mg/L POC/VOC Standard
  177
- TOC Diff (TC+IC) Standard
  177
- Toca (NPOC + POC/VOC) Standard
  177
- Predictive Maintenance
  178
- Figure 6-1: Maintenance Screen (Cockpit)
  178
- Consumables
  179
- Table 6-3: Consumables Table and Details
  179
- Cleaning the Analyzer
  182
- To Inspect and Clean the Analyzer Exterior
  183
- To Inspect and Clean the Analyzer Interior
  183
- Cleaning the Touchscreen
  183
- Prepare the Analyzer for Quick Maintenance
  183
- Quick Maintenance Task List
  184
- Backing up the Analyzer Settings
  184
- To Backup the Analyzer Settings
  184
- Preparing the Analyzer for Quick Maintenance
  185
- To Prepare the Analyzer for Quick Maintenance
  185
- Quick Maintenance Procedures
  185
- Absorber - Aerosol Absorber (HS1)
  186
- Figure 6-2: HS1 - Aerosol Absorber
  186
- Absorber - Halogen Trap (HS2)
  187
- To Replace the Halogen Trap Filter Packing
  187
- Figure 6-3: HS2 - Halogen Trap
  187
- Dilution/Rinse Water
  189
- To Refill the Dilution/Rinse Carboy
  189
- Fan Filters
  189
- To Replace the Fan Filters
  190
- MFSV Vent Absorber Cartridge
  190
- Figure 6-4: Remove Vent Cover and Replace Filter Material (Example)
  190
- NDIR Disk Filter (HS3)
  191
- Figure 6-5: MFSV Vent Absorber Cartridge
  191
- Pump Head (GP4)
  192
- Figure 6-6: HS3 - NDIR Disk Filter Cartridge
  192
- Pump Tubing (GP1)
  193
- Figure 6-7: GP4 Pump Head
  193
- Reagent - Acid
  194
- To Refill the Acid Carboy
  194
- Figure 6-8: Sample Pump (GP1) Pump Tubing
  194
- Soda Lime and Activated Carbon (Air Scrubber)
  195
- To Replace the Soda Lime and Activated Carbon
  195
- Prepare the Analyzer for Extended Maintenance
  196
- Perform an Initial Analyzer Inspection
  196
- Errors and Sensor Readings
  196
- Important Sensor Values - Analyzer On, Analysis Stopped
  196
- Run a Single Measurement Cycle
  197
- Perform a Visual Inspection and Diagnostics
  198
- Preparing the Analyzer for Extended Maintenance
  199
- To Prepare the Analyzer for Extended Maintenance
  199
- Extended Maintenance Procedures
  199
- Accessing the Furnace Head Assembly
  200
- To Access the Furnace Head Assembly
  200
- Injection Needle
  202
- To Clean or Replace the Injection Needle
  202
- Figure 6-9: Furnace Head Assembly
  203
- Figure 6-10: Furnace Head O-Ring
  203
- Figure 6-11: Connect Injection Needle to Injection Block
  204
- Furnace Cartridge
  205
- To Clean or Replace the Furnace Cartridge
  205
- Figure 6-12: Z-Brackets, Thumb Screws, and Furnace Head O-Ring
  207
- Figure 6-13: Furnace Head Assembly
  208
- Figure 6-14: Connect Injection Needle to Injection Block
  208
- Accessing the Furnace Foot Assembly
  209
- To Access the Furnace Foot Assembly
  210
- To Inspect the Bottom of the Furnace Cartridge
  211
- Sievers TOC-R3
  211
- To Clean or Replace the Furnace Foot Assembly
  212
- Figure 6-15: Furnace Foot Assembly Correct Orientation
  213
- Pre-NDIR Membrane Filter (HS4)
  214
- Cleaning Procedures
  214
- Cleaning the Gas Cooler Unit Glass Tubes
  214
- Cleaning the Multi-Function Sample Vessel (MFSV)
  215
- Update the Analyzer
  216
- Firmware
  216
- To Update the Analyzer Firmware
  216
Chapter 7: Troubleshooting

218
- Overview
  218
- Step 1: Review Rrors and Warnings
  218
- 2: Visual Inspection
  218
- Inspecting Externally
  219
- Inspecting Internally
  219
- Olutions for Basic Problems
  220
- Low Gas Flow and High Reactor Pressure
  220
- When Pressure Reactor Increase Is Observed
  221
- MFSV Not Draining
  221
- Gas Cooler Unit Condensate Not Draining
  222
- Increased Sample Recovery (NPOC)
  222
- Measurement Drift
  222
- The Analyzer will Not Power on
  222
- Diagnostics
  222
- Step 4: Contact Technical Support
  223
- Step
  223
- Eturning the
  224
- Nalyzer to Sievers
  224
Appendix A: Dimensions and Locations

226
- Overview
  226
- Analyzer Dimensions
  226
- Analyzer Dimensions - Front View
  227
- Figure A-1: Analyzer Dimensions, Front View
  227
- Analyzer Dimensions - Right Side View
  228
- Figure A-2: Analyzer Dimensions, Right Side View
  228
- Analyzer Dimensions - Left Side View
  229
- Figure A-3: Analyzer Dimensions, Left Side View
  229
- Analyzer Dimensions - View from above
  230
- Figure A-4: Door Swing Dimensions, View from above
  230
- Optional Hardware Dimensions
  231
- Communication Box Dimensions
  232
- Figure A-5: Communication Box Dimensions
  232
- Air Box and Air Scrubber Dimensions
  233
- Figure A-6: Air Box and Air Scrubber Dimensions
  233
- Particulate Sampler Dimensions
  234
- Figure A-7: Particulate Sampler Dimensions
  234
- Mounting Rack Dimensions
  235
- Figure A-8: Mounting Rack Dimensions
  235
- Analyzer External Connections
  236
- External Connections and Ports
  236
- Table A-1: External Connections and Ports List
  236
- Figure A-9: External Connections and Ports (View from Below)
  236
- Internal Views of Analyzer
  238
- Overall Internal View
  239
- Figure A-10: Overall Internal View
  239
- Figure A-11: Furnace Compartment
  239
- Furnace Compartment
  240
- Injection Block, above the Furnace
  241
- Figure A-12: Injection Block, above the Furnace
  241
- Furnace Head Assembly, Exploded
  242
- Figure A-13: Furnace Head Assembly, Exploded
  242
- Furnace Foot, below the Furnace
  243
- Figure A-14: Furnace Foot, below the Furnace
  243
- Furnace Foot, View from below
  244
- Figure A-15: Furnace Foot, View from below
  244
- Fluidics Compartment (1 of 2)
  245
- Figure A-16: Fluidics Compartment (1 of 2)
  245
- Fluidics Compartment (2 of 2)
  246
- Figure A-17: Fluidics Compartment (2 of 2)
  246
- Fluidics Compartment
  246
- Mfsv (Cm2)
  247
- Figure A-18: MFSV (CM2)
  247
- Figure A-19: Dilution Pump (GP4)
  247
- Figure A-20: Acid Pump (GP3)
  247
- Dilution Pump (GP4)
  248
- Acid Pump (GP3)
  248
- Gas Cooler Unit (EC1)
  249
- Figure A-21: Gas Cooler Unit (EC1), View from above
  249
- Gas Cooler Unit (EC1), View from above
  249
Appendix B: Errors and Warnings

250
Appendix C: Modbus Configuration

262
- Overview
  262
- Enabling Modbus TCP/IP Communication
  263
- To Enable Modbus
  263
- Modbus Register Data Types
  264
- Table C-1: Modbus Register Data Types
  264
- Modbus Register Map and Descriptions
  265
- Table C-2: Modbus Register Table
  266
Appendix D: Glossary

278
- Overview
  278
- Glossary
  278
- Index
  284

Veolia Sievers TOC-R3 Installation Manual (12 pages)

Online TOC Analyzer

Brand: Veolia | Category: Measuring Instruments | Size: 2 MB

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Veolia Sievers TOC-R3 Manuals

Veolia Sievers TOC-R3 Operation And Maintenance Manua (285 pages)

Table of Contents

Chapter 1: Introduction

Chapter 2: System Description

Chapter 3: Installation

Chapter 4: Basic Analyzer Operation

Chapter 5: Method Development

Chapter 6: Maintenance

Chapter 7: Troubleshooting

Appendix A: Dimensions and Locations

Appendix B: Errors and Warnings

Appendix C: Modbus Configuration

Appendix D: Glossary

Veolia Sievers TOC-R3 Installation Manual (12 pages)

Table of Contents

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