Particulate Systems NanoPlus Manuals

Manuals and User Guides for Particulate Systems NanoPlus. We have 1 Particulate Systems NanoPlus manual available for free PDF download: Operator's Manual

Particulate Systems NanoPlus Operator's Manual (252 pages)

Zeta Potential/Nano Particle Analyzer

Brand: Particulate Systems | Category: Laboratory Equipment | Size: 15 MB

Table of Contents
3
General Information
9
Operator's Manual
9
Organization
9
Conventions
10
Equipment Description
11
Nanoplus at
11
Specifications
12
User Interface
13
Controls, Connectors, and Indicators
13
Top Panel
13
Side Panel
14
Front Panel
14
Rear Panel
14
Labels
15
Precautions
16
During Operation
16
After Use
16
For Storage
16
Turning the System on and off
17
Using the Software
18
User Operating Modes
18
Commands
18
Main Menu
19
Shortcut Keys
20
Pop-Up Menu
20
Software Commands
21
SOP Designer
22
Panel Task Options
23
SOP Listing Panel
28
Measurement Parameters Panel
29
Size Parameters
29
Zeta Parameters
35
Analysis Parameters Panel
39
Size Parameters
39
Zeta Parameters
43
Cell Parameters Panel
45
Common Parameters
46
Size Parameters
47
Zeta Parameters
50
Diluent Parameters Panel
53
Data Acquisition
54
Size Analysis
55
Analysis
55
Data Select Panel
56
Results Panel
59
Data Select Panel
61
Results Panel
62
Temperature Gradient Analysis
63
Zeta Analysis
66
Analysis
66
Low Conductivity Cell Analysis
67
Temperature Gradient Analysis
68
Ph Maintenance
69
Maintenance
70
System Parameters
71
Cell Listing
73
System Registration Information
74
Security
75
User Management
75
Buttons
76
Window Contents
78
Security Settings
78
Data Mirroring
79
Operating Procedures
81
Specifying the SOP Designer Display Mode
81
Working with Sops
81
Creating Sops
81
Copying Sops
82
Deleting Sops
82
Renaming Sops
82
Editing SOP Parameters
82
Exporting Sops
83
Importing Sops
84
Saving and Using Favorite Sops
85
Using the SOP Designer for Other Functions
86
Detecting the Optimal Cell Position
86
Measuring the Cell Constant
87
Measuring the Electrical Conductivity
88
Measuring Particle Size and Zeta Potential
89
Preparing for Measurement
89
Starting and Stopping the Measurement
92
Viewing and Printing Measurement Results
93
Working with Analysis Data
94
Size and Zeta Potential Analysis
94
Opening an Analysis Data File
95
Deleting an Analysis Data File
95
Exporting an Analysis Data File
96
Importing an Analysis Data File
97
Modifying Analysis Parameters
98
Overlaying Analysis Data
100
Printing Analysis Data
101
Displaying Statistical Summary
102
Temperature Gradient Data
103
Specifying a Second Axis
104
Using the Temperature Marker
105
Adding a New Data Table
106
Overlaying Analysis Data
107
Adding and Deleting Diluents
108
Adding a Diluent
108
Deleting a Diluent
109
Specifying Security Settings
110
Selecting the Security Level
110
Adding Users
111
Deleting Users
112
Editing a User Profile
113
Troubleshooting and Maintenance
115
Troubleshooting
115
Maintenance
120
Cleaning the Analyzer
120
Cleaning the Cell Temperature Adjustment Block
120
Replacing the Fuses
120
Cell Maintenance
121
Flow Cell
122
Disassembling the Flow Cell
122
Assembling the Flow Cell
124
Washing the Glass Cell
125
High Concentration Cell
126
Disassembling the High Concentration Cell
126
Assembling the High Concentration Cell
128
12 Flat Surface Cell
130
Disassembling the Flat Surface Cell
131
Assembling the Flat Surface Cell
132
Washing the Flat Surface Cell
135
Coating the Flat Surface Cell with Polyacrylamide
136
Small Volume Disposable Cell for Zeta Potential
137
Disassembling the Disposable Cell
138
Low Conductivity Cell
140
Assembling the Low Conductivity Cell
140
Cleaning the Low Conductivity Cell
142
Small Volume Size Cell
143
Assembling the Small Volume Size Cell
144
NANOPLUS at Precautions and Environment Specifications
147
Site Requirements
147
Equipment Components
149
Autotitrator
149
Stirrer LED Indicators
149
Titration LED Indicators
149
Ph Electrode
149
Ph Maintenance Commands
151
Preparing for Measurement
155
Inspecting the Ph Electrode
155
Configuring Titration Solutions
156
Calibrating the Ph Electrode
156
Filling the Titration Solution
157
Loading and Circulating the Sample Solution
159
Degassing the Tube
160
Degassing the Cell
160
Performing a Measurement
162
Setting Measurement Conditions
162
Preparing for Ph Titration
163
Reviewing Ph Analysis Results
164
Calibrating the Ph Electrode
165
Resetting Temperature Constants of Ph Electrode
167
Maintenance
168
Cleaning the Instrument
168
Applying Grease to Pump Tubing
168
Replacing the Fuses
169
Replacing the Syringe O-Ring
169
Ph Electrode
170
Precautions for Daily Use
170
Precautions for First-Time Use or after Long-Term Storage
170
Storage Conditions
170
Daily Maintenance
171
Improving Response Time
172
Size Flow Cell
172
Consumables
175
Tubing
176
Detail
177
Identification and Schematic
178
Diluent Physical Constants
179
Water
179
Refractive Index
179
Viscosity
180
Dielectric Constant
180
Other Liquids
187
Alpha / Beta Values
189
Table of Values
189
Determining Alpha and Beta
190
References
191
Graph and Table Examples
193
Real-Time Size Displays
194
Real-Time Size Monitor
194
Real-Time Size Table
194
Intensity Distribution Graphs
195
Differential Intensity Distribution
195
Cumulative Intensity Distribution
196
Volume Distribution Graphs
196
Differential Volume Distribution
197
Cumulative Volume Distribution
197
Number Distribution Graphs
198
Differential Number Distribution
198
Cumulative Number Distribution
199
Size Distribution Tables
200
Differential Size Distribution Table
200
Cumulative Size Distribution Table
201
Autocorrelation (ACF) Function
201
ACF Listing
201
Normal Linear ACF
202
ACF with Short Sampling Time
202
Normal Log ACF
203
ACF Noisy - Low Sample Concentration
203
ACF for Small Particles (Less than 10 Nm
204
Condition Summary
204
Distribution Graph
205
Distribution Graph with Zeta Potential of the Sample
205
Distribution Graph with Mobility of the Sample
206
ACF (Base
207
Test Measurement
208
3D Graph
209
With Zeta Potential and Top View
209
With Mobility and 3D View
210
Peak Value Table
211
Temperature Gradient Plot
212
With Second Axis
212
With Temperature Marker
213
Graph Options
214
Using the Pop-Up Menus
214
Editing Graph Axes
215
Editing Graph Parameters
216
Theory of Operation
217
Particle Sizing by Dynamic Light Scattering
217
Particles in Brownian Motion
217
Light Scattering from Particles in Brownian Motion
217
The Autocorrelation Function
218
Correlator
220
The Correlation Method
220
The Time Domain Method
221
The Time Interval Method
221
Particle Size/Size Distributions
222
The Cumulants Method
222
Particle Size Distribution Methods
222
The CONTIN Method
222
The Marquardt Method
222
The NNLS (Non-Negative Least-Squares) Method
223
Molecular Weight Analysis
223
Zeta Potential Determination by Electrophoretic Light Scattering
224
Electrical Double Layer
224
Zeta Potential
224
Electrophoretic Light Scattering
226
Power Spectrum for Zeta Potential Measurements
227
Zeta Potential Measurement Using Electrophoretic Light Scattering
229
21 CFR Part
233
Activating 21 CFR Part 11
233
Obtaining an Authentication Code
233
Applying the Authentication Code
234
Enabling CFR Part 11
235
Software Additions
236
Main Menu Bar
236
Using the CFR Part 11 Functions
237
Adding Users
237
Disabling and Enabling Users
238
Editing a User Profile
239
Generating Electronic Signatures
240
Viewing Audit Trails
241
Changing Audit Trail Options
242
Exporting Details for Audit Trails
242
Viewing File History
244
Using Playback
245

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Particulate Systems NanoPlus Operator's Manual (252 pages)

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