Metrohm 862 Manuals

Manuals and User Guides for Metrohm 862. We have 2 Metrohm 862 manuals available for free PDF download: Manual

Metrohm 862 Manual (174 pages)

Compact Titrosampler

Brand: Metrohm | Category: Laboratory Equipment | Size: 4 MB

Table of Contents

5
- 1 Introduction
  
  11
  - Instrument Description
    11
  - Instrument Components
    11
  - Titration and Measuring Modes
    12
  - Intended Use
    12
  - About the Documentation
    13
  - Symbols and Conventions
    13
  - Safety Instructions
    14
  - General Notes on Safety
    14
  - Electrical Safety
    14
  - Tubing and Capillary Connections
    15
  - Personnel Safety
    15
  - Flammable Solvents and Chemicals
    17
  - Recycling and Disposal
    17
- 2 Overview of the Instrument
  
  18
  - Figure 1 Front 862 Compact Titrosampler
    18
  - Figure 2 Rear 862 Compact Titrosampler
    19
- 3 Installation
  
  20
- 4 Titration and Automation Sequences
  
  38
  - Dynamic Equivalence Point Titration (DET)
    38
  - Monotonic Equivalence Point Titration (MET)
    38
  - Figure 25 Reagent Dosing for DET
    38
  - Figure 26 Reagent Dosing for MET
    38
  - Endpoint Titration (SET)
    39
  - Automation Sequences
    39
  - Dipping in Special
    39
  - Figure 27 Reagent Dosing for SET
    39
  - Dipping in Special 2
    40
  - Double Dipping
    41
  - Rinsing in Sample
    42
  - Rinsing in Special
    42
  - Pump Control
    43
  - Dosing Auxiliary Solutions
    44
- 5 Operation
  
  45
  - Switching the Instrument on and off
    45
  - Fundamentals of Operation
    46
  - The Keypad
    46
  - Figure 28 Keypad 862 Compact Titrosampler
    46
  - Structure of the Dialog Windows
    47
  - Navigating in the Dialog
    47
  - Entering Text and Numbers
    48
  - Selecting from a Selection List
    49
  - Formula Editor
    49
  - Methods
    51
  - Creating a New Method
    51
  - Saving a Method
    52
  - Loading a Method
    53
  - Exporting a Method
    54
  - Sample Data
    55
  - Sample Table
    55
  - Entering Sample Data in the Main Dialog
    58
  - Performing a Sample Series
    59
  - Starting the Sample Series
    59
  - Pausing a Sample Series and Continuing
    60
  - Status of the Sample Series
    62
  - Special Case: Calibrations
    62
  - Live Modifications
    63
  - Editing the Sample Data of the Running Determination
    63
  - Editing the Sample Table While a Determination Is Running
    64
  - Live Parameters
    65
  - Results
    66
  - Statistics
    68
  - Printing a Report Manually
    69
  - Manual Control
    71
  - Rotating the Sample Rack
    71
  - Moving the Lift
    72
  - Dosing
    72
  - Measuring
    76
  - Stirring
    77
- 6 System Settings
  
  79
  - Basic Settings
    79
  - Lift Settings (Lift)
    82
  - Managing Sensors
    83
  - General
    83
  - Editing the Sensor Data
    84
  - Managing Solutions
    85
  - General
    85
  - Editing the Solution Data
    86
  - Managing Common Variables
    87
  - General
    87
  - Editing Common Variables
    88
  - File Management
    89
  - Configuring External Devices
    90
  - Figure 29 Directory Structure on the USB Stick
    90
  - Instrument Diagnosis
    93
  - Loading Program Versions and Language Files
    93
  - Diagnosis Functions
    94
- 7 Parameters
  
  95
  - Dynamic Equivalence Point Titrations (DET)
    95
  - Start Conditions
    95
  - Titration Parameters
    96
  - Stop Conditions
    101
  - Evaluation
    103
  - Calculation
    106
  - Figure 30 Tubbs Method for Determining the Equivalence Point
    106
  - Statistics
    108
  - Reports
    108
  - Monotonic Equivalence Point Titrations (MET)
    110
  - Start Conditions
    110
  - Titration Parameters
    111
  - Stop Conditions
    116
  - Evaluation
    117
Table of Contents

118
- Default Value
  119
- Measuring Mode Ph: Range -20.000
  119
- Measuring Mode U, Ipol: Range -1250.0
  119
  - Calculation
    120
  - Statistics
    122
  - Reports
    122
  - Endpoint Titrations (SET)
    124
  - Conditioning
    124
  - Start Conditions
    125
  - Titration Parameters
    127
  - Control Parameters EP1
    129
- Measuring Mode Upol: Range -125.00
  119
- Default Value
  130
- Measuring Mode Ph
  130
- Measuring Mode U, Ipol: Range 1
  130
- Measuring Mode Upol
  130
- Measuring Mode Upol: Range -125.00
  130
- Range 0.1
  130
  - Control Parameters EP2
    132
  - Stop Conditions
    132
  - Calculation
    133
  - Statistics
    135
  - Reports
    135
  - Ph Calibration (CAL)
    137
  - Calibration Parameters
    137
  - Buffers
    138
  - Reports
    139
  - Automation: Dipping in Special
    140
  - Automation: Dipping in Special 2
    141
  - Automation: Double Dipping
    142
  - Automation: Rinsing in Sample
    143
  - Automation: Rinsing in Special
    144
- Range 0.10
  130
- 8 Handling and Maintenance
  
  145
  - General
    145
  - Quality Management and Validation with Metrohm
    145
- 9 Troubleshooting
  
  147
  - SET Titration
    147
  - Miscellaneous
    148
- 10 Appendix
  
  149
  - Dosing Unit
    149
  - Maximum Dosing and Filling Rate
    149
  - Parameters for Preparing (PREP) and Emptying (EMPTY)
    149
  - Stirring Rate
    150
  - Balance
    150
  - Figure 31 Rotational Speed Depending on Stirring Rate
    150
  - USB Devices
    151
  - Numerical USB Keypad 6.2147.000
    151
  - Key Assignment of a USB Keyboard
    152
  - PC Mouse
    152
  - Printer
    153
  - System Initialization
    153
  - Remote Interface
    155
  - Pin Assignment of the Remote Interface
    155
  - Figure 32 Pin Assignment of Remote Socket and Plug
    155
  - Status Diagram of the Remote Interface
    156
  - Figure 33 Remote Status Diagram
    156
- 11 Technical Specifications
  
  157
  - Measuring Inputs
    157
  - Potentiometry
    157
  - Polarizer
    157
  - Temperature
    158
  - Dosing Drive
    159
  - Lift
    159
  - Turntable
    159
  - Interfaces and Connectors
    159
  - Mains Connection
    160
  - Safety Specifications
    160
  - Electromagnetic Compatibility (EMC)
    160
  - Ambient Temperature
    161
  - 11.10 Reference Conditions
    161
  - 11.11 Dimensions
    161
- 12 Conformity and Warranty
  
  162
  - Declaration of Conformity
    162
  - Warranty (Guarantee)
    163
  - Quality Management Principles
    164
- 13 Accessories
  
  166
  - Scope of Delivery 2.862.0010
    166
  - Optional Accessories
    170
- Index
  
  173

Metrohm 862 Manual (168 pages)

Compact Titrosampler

Brand: Metrohm | Category: Measuring Instruments | Size: 2 MB

Table of Contents
5
1 Introduction

11
- Instrument Description
  11
- Instrument Components
  11
- Titration and Measuring Modes
  12
- Intended Use
  12
- About the Documentation
  13
- Symbols and Conventions
  13
- Safety Instructions
  14
- General Notes on Safety
  14
- Electrical Safety
  14
- Tubing and Capillary Connections
  15
- Personnel Safety
  15
- Flammable Solvents and Chemicals
  17
- Recycling and Disposal
  17
2 Overview of the Instrument

18
- Figure 1 Front 862 Compact Titrosampler
  18
- Figure 2 Rear 862 Compact Titrosampler
  19
3 Installation

20
4 Titrations and Automation Runs

38
- Dynamic Equivalence Point Titration (DET)
  38
- Monotonic Equivalence Point Titration (MET)
  38
- Figure 25 Reagent Dosing for DET
  38
- Figure 26 Reagent Dosing for MET
  38
- Endpoint Titration (SET)
  39
- Automation Runs
  39
- Dipping in Special
  39
- Figure 27 Reagent Dosing for SET
  39
- Dipping in Special 2
  40
- Double Dipping
  41
- Rinsing in Sample
  42
- Rinsing in Special
  43
- Pump Control
  44
- Dosing Auxiliary Solutions
  44
5 Operation

45
- Switching the Instrument on and off
  45
- Fundamentals of Operation
  46
- The Keypad
  46
- Figure 28 Keypad 862 Compact Titrosampler
  46
- Structure of the Dialog Windows
  47
- Navigating in the Dialog
  47
- Entering Text and Numbers
  48
- Selecting from a Selection List
  49
- Formula Editor
  49
- Methods
  51
- Creating a New Method
  51
- Saving a Method
  52
- Loading a Method
  53
- Exporting a Method
  54
- Sample Data
  55
- Sample Table
  55
- Entering Sample Data in the Main Dialog
  58
- Performing a Sample Series
  59
- Starting the Sample Series
  59
- Pausing a Sample Series and Continuing
  60
- Status of the Sample Series
  62
- Special Case: Calibrations
  63
- Live Modifications
  63
- Editing the Sample Data of the Running Determination
  63
- Editing the Sample Table While a Determination Is Running
  64
- Editing the Live Parameters
  66
- Results
  67
- Statistics
  68
- Printing a Report Manually
  70
- Manual Control
  71
- Rotating the Sample Rack
  72
- Moving the Lift
  72
- Dosing
  72
- Measuring
  77
- Stirring
  79
6 System Settings

80
- Basic Settings
  80
- Lift Settings (Lift)
  83
- Managing Sensors
  84
- General
  84
- Editing the Sensor Data
  85
- Managing Solutions
  86
- General
  86
- Editing the Solution Data
  87
- Managing Common Variables
  88
- General
  88
- Editing Common Variables
  89
- File Management
  90
- Configuring External Devices
  91
- Figure 29 Directory Structure on the USB Flash Drive
  91
- Instrument Diagnosis
  94
- Loading Program Versions and Language Files
  94
- Diagnosis Functions
  96
7 Parameters

97
- Dynamic Equivalence Point Titrations (DET)
  97
- Start Conditions
  97
- Titration Parameters
  98
- Stop Conditions
  104
- Evaluation
  105
- Calculation
  108
- Figure 30 Tubbs Method for Determining the Equivalence Point
  108
- Statistics
  110
- Reports
  110
- Monotonic Equivalence Point Titrations (MET)
  112
- Start Conditions
  112
- Titration Parameters
  113
- Stop Conditions
  118
- Evaluation
  119
- Calculation
  122
- Statistics
  124
- Reports
  124
- Endpoint Titrations (SET)
  126
- Conditioning
  126
- Start Conditions
  127
- Titration Parameters
  129
- Control Parameters EP1
  131
- Control Parameters EP2
  134
- Stop Conditions
  134
- Calculation
  135
- Statistics
  137
- Reports
  137
- Ph Calibration (CAL)
  139
- Calibration Parameters
  139
- Buffers
  140
- Reports
  141
- Automation: Dipping in Special
  142
- Automation: Dipping in Special 2
  143
- Automation: Double Dipping
  144
- Automation: Rinsing in Sample
  145
- Automation: Rinsing in Special
  146
8 Operation and Maintenance

147
- General
  147
- Quality Management and Qualification with Metrohm
  147
9 Troubleshooting

148
- SET Titration
  148
- Miscellaneous
  149
10 Appendix

150
- Dosing Unit
  150
- Maximum Dosing and Filling Rate
  150
- Parameters for Preparing (PREP) and Emptying (EMPTY)
  150
- Stirring Rate
  151
- Balance
  151
- Figure 31 Rotational Speed Depending on Stirring Rate
  151
- USB Devices
  152
- 6.2147.000 Numerical USB Keypad
  152
- Key Assignment of a USB Keyboard
  153
- PC Mouse
  153
- Printer
  154
- System Initialization
  154
- Remote Interface
  156
- Pin Assignment of the Remote Interface
  156
- Figure 32 Pin Assignment of Remote Socket and Remote Plug
  156
- Status Diagram of the Remote Interface
  157
- Figure 33 Remote Status Diagram
  157
11 Technical Specifications

158
- Measuring Inputs
  158
- Potentiometry
  158
- Polarizer
  158
- Temperature
  159
- Dosing Drive
  160
- Lift
  160
- Turntable
  160
- Interfaces and Connectors
  160
- Power Connection
  161
- Safety Specifications
  161
- Electromagnetic Compatibility (EMC)
  162
- Ambient Temperature
  162
- 11.10 Reference Conditions
  162
- 11.11 Dimensions
  163
12 Accessories

164
Index

166

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Metrohm 862 Manuals

Metrohm 862 Manual (174 pages)

Table of Contents

Table of Contents

1 Introduction

2 Overview of the Instrument

3 Installation

4 Titration and Automation Sequences

5 Operation

6 System Settings

7 Parameters

Table of Contents

8 Handling and Maintenance

9 Troubleshooting

10 Appendix

11 Technical Specifications

12 Conformity and Warranty

13 Accessories

Index

Metrohm 862 Manual (168 pages)

Table of Contents

1 Introduction

2 Overview of the Instrument

3 Installation

4 Titrations and Automation Runs

5 Operation

6 System Settings

7 Parameters

8 Operation and Maintenance

9 Troubleshooting

10 Appendix

11 Technical Specifications

12 Accessories

Index

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