Metrohm 792 Basic IC Ion Chromatography Manuals

Manuals and User Guides for Metrohm 792 Basic IC Ion Chromatography. We have 1 Metrohm 792 Basic IC Ion Chromatography manual available for free PDF download: Instructions For Use Manual

Metrohm 792 Basic IC Instructions For Use Manual (197 pages)

Brand: Metrohm | Category: Analytical Instruments | Size: 2 MB

Table of Contents
2
Introduction
10
Instrument Description
10
Parts and Controls
12
Fig. 1: Front of the 792 Basic IC
12
Fig. 2: Rear of the 792 Basic IC
13
Fig. 3: Interior of the 792 Basic IC
15
Information on the Instructions for Use
17
Organization
17
Notation and Pictograms
18
Safety Notes
19
Electrical Safety
19
General Precautionary Rules
19
Installation
20
Overview
20
Flow Chart
20
Connections in the 792 Basic IC
20
Fig. 4: Connecting Diagram for 792 Basic IC Without Suppressor
21
Fig. 5: Connecting Diagram for 792 Basic IC with Suppressor
21
Setting up the Instrument
22
Packaging
22
Check
22
Location
22
Attaching the Accessories
22
Connection of Detector Block
22
Connection of Syringe and Aspirating Tubing
23
Connection of the 6.5324.000 Bottle Rack (Option)
23
Connection of PEEK Capillaries
24
Fig. 6: Connectors for Capillaries
24
Filter Unit PEEK
25
Fig. 7: 6.2821.100 Filter Unit PEEK
25
Mains Connection
26
Setting the Mains Voltage
26
Fuses
27
Mains Cable and Mains Connection
27
On/Off Switching of the Instrument
27
Fig. 8: Setting the Mains Voltage
27
Connection to the PC
28
Connecting Cable
28
Software Installation
28
Basic Settings
29
High-Pressure Pump
32
Removing the Transport Security Screws
32
Installing the Pulsation Dampener (Option)
32
Fig. 9: Connection of the Pulsation Dampener (Option)
33
Connecting the Eluent Bottle
34
Deaerating the Pump and Rinsing the Pulsation Dampener
34
Precolumns and Separating Columns
37
General Information on Precolumns
37
Precolumns with Twin Cartridge Holder
37
Fig. 10: Installing Precolumn Cartridges
38
Precolumn Glass Cartridges with Cartridge Holder
39
IC Anion Precolumn SUPERSEP
40
Fig. 11: Installation of Precolumn Glass Cartridges with Cartridge Holder
40
General Information on Separating Columns
41
Selection of the Sample Loop
41
Installation of the Separating Column Without Suppressor
41
Fig. 12: Installation of Column Without Suppressor
42
Installation of the Separating Column with Suppressor
43
Suppressor Module
44
General Information on Suppressor Module
44
Preparation of the Peristaltic Pump
44
Fig. 13: Installing Pump Tubings
45
Fig. 14: Installation of Column with Suppressor
46
Connection of Supply Bottles
47
Connection of the Suppressor Module
48
Fig. 15: Connections at Suppressor Module
49
Putting into Operation
50
Putting into Operation Without Suppressor
50
Putting into Operation with Suppressor
51
Operating Tutorial
54
Requirements
54
Preparations
55
Calibration
56
Sample Determination
63
Operation
66
Fundamentals of the Operation
66
Starting/Closing the Program
66
Glossary
67
Overview of Program Windows
68
Main Window Elements
69
Icons of the Main Window
69
Overview of File Types
70
Context Sensitive Menus
71
Keyboard and Mouse Functions
71
Help
72
Instrument and Software Settings
73
Fonts
73
Security System
73
Global Settings
74
COM Port
76
Systems
77
System Window
77
System File Handling
77
System Functions
78
Start/Stop Hardware and Record Baseline
78
Start/Stop Determinations
78
Print System Parameters
79
PC Icon
80
Watch Window
80
Instrument Icon
81
Menu Options for Instrument Icon
81
System Parameters for Disconnected System
81
Instrument Control for Connected System
82
Time Program
83
Configuration
85
Hardware Settings
85
System State Window
87
Status Messages
87
Error Messages
88
Methods
89
Method File Handling
89
Passport
89
General
90
Sample
91
Column
92
Eluent
93
Comment
93
Method Log
94
Data Log
95
Method Setup
96
General
96
Processing
96
Math
97
Integration
99
Setup
100
Events
101
Calibration and Quantification
103
General Information
103
Notations
104
External Standard Calibration
105
Component Table
105
Peak Identification
107
Concentration Table
109
Calibration Curve
111
Update Calibration
113
Load and Save Calibration Data
114
Import and Export Calibration Data
114
Put out Calibration Curves
114
Report Output
115
Report Options
115
Chromatograms
127
Chromatogram Window
127
Chromatogram File Handling
128
Open Chromatogram
128
Save Chromatogram
129
Close Chromatogram
129
Delete Chromatogram
129
Export Chromatogram
130
Graphical Representation
131
Appearance
131
Other Graphical Functions
135
Peak Editor
136
Switching On/Off the Peak Editor
136
Peak Editor Functions
136
Moving the Cursor
137
Printing
138
Page Layout for Printing
138
Printer Settings
139
Print Preview
139
Printing
139
Miscellaneous Functions
139
Reintegration
139
Recalibration
139
Subtraction of a Chromatogram
140
Data Compression
140
Invert Chromatogram
140
Batch Reprocessing
141
Batch Reprocessing Queue File Handling
141
Open Batch Reprocessing Queue
141
Create New Batch Reprocessing Queue
141
Save Batch Reprocessing Queue
141
Perform Batch Reprocessing
142
Reprocess Options Window
142
Merge Chromatograms
145
Batch Reprocessing Queue Editor
146
Open Batch Reprocessing Queue Editor Window
146
Batch Reprocessing Queue Editor Functions
147
Print Batch Reprocessing Queue
147
Close Batch Reprocessing Queue Editor
147
Notes - Maintenance - Faults
148
Practical Notes on Ion Chromatography
148
Separating Columns
148
High-Pressure Pump
149
Eluents
150
Peristaltic Pump
150
Suppressor Module
151
Connections
151
Maintenance and Servicing
152
General Information
152
Passivation
152
Recycling
153
Shutdown
153
Changing Separating Columns
153
Maintenance Work at the Pump Head
155
Fig. 16: Components of the Pump Head
156
Fig. 17: Replacement of the Piston Seal 89
156
Fig. 18: Components of Inlet Valve
158
Regeneration of the Suppressor Module
159
Cleaning the Suppressor
160
Replacing the Suppressor
162
Fig. 19: Assembling the Suppressor
162
Exchanging the Pump Tubing
164
Faults and Malfunctions
165
Error Messages
165
Malfunctions and Their Rectification
165
Diagnostic Tests / Validation / GLP
167
Appendix
168
Technical Data
168
Conductivity Measurement
168
Conductivity Detector
168
Injection Valve
169
High-Pressure Pump
169
Peristaltic Pump
170
Suppressor Module
170
RS232 Interface
170
Mains Connection
171
Safety Specifications
171
Electromagnetic Compatibility (EMC)
171
Ambient Temperature
172
Housing
172
Standard Equipment
173
Optional Accessories
176
Accessories for 792 Basic IC
176
Separating Columns and Precolumns
178
Additional Devices and Cables
184
Warranty and Conformity
185
Warranty
185
EU Declaration of Conformity
186
Certificate of Conformity and System Validation
187
Index
188

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Metrohm 792 Basic IC Ion Chromatography Manuals

Metrohm 792 Basic IC Instructions For Use Manual (197 pages)

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