Metrohm 790 Personal IC Manuals

Manuals and User Guides for Metrohm 790 Personal IC. We have 1 Metrohm 790 Personal IC manual available for free PDF download: Instructions For Use Manual

Metrohm 790 Personal IC Instructions For Use Manual (207 pages)

Brand: Metrohm | Category: Laboratory Equipment | Size: 4 MB

Table of Contents
2
Introduction
10
Instrument Description
10
Parts and Controls
12
Fig. 1: Front of the 790 Personal IC
12
Fig. 2: Rear of the 790 Personal IC
13
Fig. 3: Interior of the 2.790.0010 Personal IC
15
Fig. 4: Interior of the 2.790.0020 Personal IC
17
Information on the Instructions for Use
19
Organization
19
Notation and Pictograms
20
Safety Notes
21
Electrical Safety
21
General Precautionary Rules
21
Installation
22
Overview
22
Flow Chart
22
Connections in the 790 Personal IC
22
Fig. 5: Connecting Diagram for 2.790.0010 Personal IC Without Suppressor
23
Fig. 6: Connecting Diagram for 2.790.0020 Personal IC with Suppressor
23
Setting up the Instrument
24
Packaging
24
Check
24
Location
24
Attaching the Accessories
24
Connection of Detector Block
24
Connection of Syringe and Aspirating Tubing
25
Connection of the 6.5324.000 Bottle Rack (Option)
25
Connection of PEEK Capillaries
26
Fig. 7: Connectors for Capillaries
26
Filter Unit PEEK
27
Fig. 8: 6.2821.100 Filter Unit PEEK
27
Mains Connection
28
Setting the Mains Voltage
28
Fuses
29
Mains Cable and Mains Connection
29
On/Off Switching of the Instrument
29
Fig. 9: Setting the Mains Voltage
29
Connection to the PC
30
Connecting Cable
30
Software Installation
30
Basic Settings
31
High-Pressure Pump
34
Removing the Transport Security Screws
34
Installing the Pulsation Dampener (Option)
34
Fig. 10: Connection of the Pulsation Dampener (Option)
35
Connecting the Eluent Bottle
36
Deaerating the Pump and Rinsing the Pulsation Dampener
36
Precolumns and Separating Columns
39
General Information on Precolumns
39
Precolumns with Cartridge Head
39
Fig. 11: Installation of Precolumn Cartridges with Cartridge Head
40
Precolumn Glass Cartridges with Cartridge Holder
41
IC Anion Precolumn SUPERSEP
42
Fig. 12: Installation of Precolumn Glass Cartridges with Cartridge Holder
42
General Information on Separating Columns
43
Selection of the Sample Loop
43
Installation of the Separating Column Without Suppressor
44
Installation of the Separating Column with Suppressor
45
Fig. 13: Installation of Column Without Suppressor
45
Suppressor Module
46
General Information on Suppressor Module
46
Preparation of the Peristaltic Pump
46
Fig. 14: Installing Pump Tubings
47
Fig. 15: Installation of Column with Suppressor
48
Connection of Supply Bottles
49
Connection of the Suppressor Module
50
Fig. 16: Connections at Suppressor Module
51
Putting into Operation
52
Putting into Operation Without Suppressor (Cation System)
52
Putting into Operation with Suppressor (Anion System)
53
Connection of External Devices
55
Connection of the 750 Autosampler
55
Connection of the 766 IC Sample Processor
56
Operating Tutorial
60
Requirements
60
Preparations
61
Calibration
62
Sample Determination
69
Operation
72
Fundamentals of the Operation
72
Starting/Closing the Program
72
Glossary
73
Overview of Program Windows
74
Main Window Elements
75
Icons of the Main Window
75
Overview of File Types
76
Context Sensitive Menus
77
Keyboard and Mouse Functions
77
Help
78
Instrument and Software Settings
79
Fonts
79
Security System
79
Global Settings
80
COM Port
82
Systems
83
System Window
83
System File Handling
83
System Functions
84
Start/Stop Hardware and Record Baseline
84
Start/Stop Determinations
84
Print System Parameters
85
PC Icon
86
Watch Window
86
Instrument Icon
87
Menu Options for Instrument Icon
87
System Parameters for Disconnected System
87
Instrument Control for Connected System
88
Time Program
89
Configuration
91
Hardware Settings
91
System State Window
93
Status Messages
93
Error Messages
94
Methods
95
Method File Handling
95
Passport
95
General
96
Sample
97
Column
98
Eluent
99
Comment
99
Method Log
100
Data Log
101
Method Setup
102
General
102
Processing
102
Math
103
Integration
105
Setup
106
Events
107
Calibration and Quantification
109
General Information
109
Notations
110
External Standard Calibration
111
Component Table
111
Peak Identification
113
Concentration Table
115
Calibration Curve
117
Update Calibration
119
Load and Save Calibration Data
120
Import and Export Calibration Data
120
Put out Calibration Curves
120
Report Output
121
Report Options
121
Chromatograms
133
Chromatogram Window
133
Chromatogram File Handling
134
Open Chromatogram
134
Save Chromatogram
135
Close Chromatogram
135
Delete Chromatogram
135
Export Chromatogram
136
Graphical Representation
137
Appearance
137
Other Graphical Functions
141
Peak Editor
142
Switching On/Off the Peak Editor
142
Peak Editor Functions
142
Moving the Cursor
143
Printing
144
Page Layout for Printing
144
Printer Settings
145
Print Preview
145
Printing
145
Miscellaneous Functions
145
Reintegration
145
Recalibration
145
Subtraction of a Chromatogram
146
Data Compression
146
Invert Chromatogram
146
Sample Queue
147
Sample Queue File Handling
147
Open Sample Queue
147
Save Sample Queue
147
Delete Sample Queue
147
Sample Queue Control
148
Sample Queue Overview Table
148
Start Sample Queue
149
Pause Sample Queue
150
Cancel Last Run
150
Reset Sample Queue
150
Sample Queue Editor
150
Open Queue Editor Window
150
Sample Queue Editor Functions
152
Print Sample Queue
152
Close Sample Queue Editor
152
Batch Reprocessing
153
Batch Reprocessing Queue File Handling
153
Open Batch Reprocessing Queue
153
Create New Batch Reprocessing Queue
153
Save Batch Reprocessing Queue
153
Perform Batch Reprocessing
154
Reprocess Options Window
154
Merge Chromatograms
157
Batch Reprocessing Queue Editor
158
Open Batch Reprocessing Queue Editor Window
158
Batch Reprocessing Queue Editor Functions
159
Print Batch Reprocessing Queue
159
Close Batch Reprocessing Queue Editor
159
Notes - Maintenance - Faults
160
Practical Notes on Ion Chromatography
160
Separating Columns
160
High-Pressure Pump
161
Eluents
162
Peristaltic Pump
162
Suppressor Module
163
Connections
163
Maintenance and Servicing
164
General Information
164
Passivation
164
Recycling
165
Shutdown
165
Changing Separating Columns
165
Maintenance Work at the Pump Head
167
Fig. 17: Components of the Pump Head
168
Fig. 18: Replacement of the Piston Seal 92
168
Regeneration of the Suppressor Module
171
Cleaning the Suppressor
172
Replacing the Suppressor
174
Fig. 20: Assembling the Suppressor
174
Exchanging the Pump Tubing
176
Faults and Malfunctions
177
Error Messages
177
Malfunctions and Their Rectification
177
Diagnostic Tests / Validation / GLP
179
Appendix
180
Technical Data
180
Conductivity Measurement
180
Conductivity Detector
180
Injection Valve
180
High-Pressure Pump
181
Peristaltic Pump
181
Suppressor Module
182
RS232 Interface
182
Remote Interface
182
Mains Connection
183
Safety Specifications
183
Electromagnetic Compatibility (EMC)
183
Ambient Temperature
183
Housing
184
Standard Equipment
185
Optional Accessories
188
Accessories for 790 Personal IC
188
Separating Columns and Precolumns
190
Additional Devices and Cables
194
Warranty and Conformity
195
Warranty
195
EU Declaration of Conformity
196
Certificate of Conformity and System Validation
197
Index
198

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Metrohm 790 Personal IC Manuals

Metrohm 790 Personal IC Instructions For Use Manual (207 pages)

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