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Analytik Jena PlasmaQuant PQ 9000
Endress+Hauser Analytik Jena PlasmaQuant PQ 9000 Manuals
Manuals and User Guides for Endress+Hauser Analytik Jena PlasmaQuant PQ 9000. We have
1
Endress+Hauser Analytik Jena PlasmaQuant PQ 9000 manual available for free PDF download: Operating Manual
Endress+Hauser Analytik Jena PlasmaQuant PQ 9000 Operating Manual (87 pages)
High-Resolution Array ICP-OES
Brand:
Endress+Hauser
| Category:
Laboratory Equipment
| Size: 3 MB
Table of Contents
Table of Contents
3
1 Basic Information
7
User Manual Notes
7
Intended Use
8
2 Safety
9
Safety Markings on the Plasmaquant PQ 9000
9
Requirements for the Operating Personnel
10
Safety Instructions, Transport and Commissioning
10
Safety Instructions - Operation
11
General Safety Instructions for Operation
11
Safety Instructions Relating to Ambient Conditions
11
Safety Instructions - Electrical Equipment
11
Hazards Caused by Plasma Operation
12
Behavior in Case of Ring Plasmas
12
Safety Instructions Relating to the Formation of Ozone and Toxic Vapors
13
Safety Instructions Relating to Compressed Gas Containers and Systems
13
Handling of Samples, Auxiliary and Operating Materials
13
Safety Instructions Relating to Cleaning and Decontamination Measures
14
Safety Instructions - Maintenance and Repair
14
Behavior During Emergencies
15
3 Function and Setup of the Plasmaquant PQ 9000
16
Physical Functional Principle of ICP-OES
16
Figure 1 Sampling Compartment and Plasma Compartment
17
Figure 2 Concentric Nebulizer and Spray Chamber
18
Figure 3 Schematic Structure of the Torch with Gas Flows
18
Figure 4 Demountable Torch
19
Figure 5 One-Piece Torch
19
Autosampler ASPQ 3300
20
Figure 6 Autosampler ASPQ 3300
20
4 Installation and Commissioning
22
Installation Conditions
22
Environmental Conditions
22
Energy Supply
22
Environmental Conditions for Operation
22
Gas Supply
23
Overview 2 Power Supply
23
Overview 3 Gas Supply
23
Exhaust Unit
24
Recirculating Chiller
24
Exhaust Unit Requirements
24
Cooling Circuit Requirements
24
Device Layout and Space Requirements
25
Figure 7 Dimensions of the Plasmaquant PQ 9000 - Front View
26
Supply and Control Connections
27
Figure 8 Dimensions of the Plasmaquant PQ 9000 - Top View
27
Figure 9 Overview of Connections on the Left Side of the Device
28
Figure 10 Interfaces and Fuses
29
Figure 11 Connections for Cooling Water and Gases
29
Figure 12 Plug-In Connectors for Gas Connections
30
Figure 13 Ventilation Openings and Air Filter on the Rear-Side
30
Connections in the Plasma Compartment, Sampling Compartment and Type Plate
31
Figure 14 Plasma Compartment
31
Figure 15 Data on the Type Plate
31
Installing the Plasmaquant PQ 9000
32
Connecting and Comissioning the Plasmaquant PQ 9000
32
Figure 16 Sampling Compartment
32
Installation of the Torch, Nebulizer with Spray Chamber and Sample Supply
33
Initial Operation of the Autosampler ASPQ 3300
36
Figure 17 ASPQ 3300- Overview
36
Figure 18 Connections on the Right Side of the Autosampler
36
Figure 19 Wash Cup und Pump at the ASPQ 3300
37
Installing Additional Accessories
39
Installing Isomist
39
Installing the Argon Humidifier
41
Figure 20 Isomist in the Sampling Compartment
41
Installing the In-Line Filter
42
Figure 21 Argon Humidifier in the Sampling Compartment
42
Figure 22 In-Line Filter in Sampling Compartment
43
Figure 23 Position of the Ferrule in the Banjo Bolt
43
Installing the Kit for Internal Standard (KIS)
44
Installing the Hg/Hydride Systems
44
Figure 24 KIS in Sampling Compartment
44
5 Operation
46
Switching on the Plasmaquant PQ 9000 and Igniting the Plasma
46
Switching off the Plasmaquant PQ 9000
47
Using the Plasma Deactivation Switch in the Event of Faults
48
Starting a Measurement Routine
48
6 Maintenance and Care
50
Maintenance Intervals
51
Base Device Maintenance
52
Cleaning the Demountable Torch
52
Replacing the Torch Body
54
Servicing the One-Piece Torch
57
Cleaning the Nebulizer
59
Cleaning the Sampling Compartment and the Plasma Compartment
60
Replacing Pump Tubes
60
Figure 25 Nebulizer Cleaning Tool with Installed Nebulizer
60
Changing the Plasma Compartment Windows
61
Checking the Gas System for Leaks
63
Changing Fuses
63
Figure 26 Plug-In Connectors for Gas Connections
63
Figure 27 Gas Distribution
63
6.2.10 Replacing the Air Filter of the PQ 9000
64
6.2.11 Servicing the Water Filter
64
6.2.12 Replacing the Argon Hose
65
Maintenance of the Autosampler ASPQ 3300
65
Replacing the Cannula and the Sample Tube
65
Replacing the Pump Tubing of the Autosampler Pump
66
Figure 28 ASPQ 3300 Cannula and Sample Tube Dismantled
66
Replacing the Fuses
67
Figure 29 Autosampler Pump
67
Maintenance of the Recirculating Chiller - Changing the Cooling Water
68
Figure 30 Replacing the Fuses of the Autosampler
68
7 Fault Removal
70
Device Faults and Error Messages in the Software
70
Equipment Faults and Analytical Problems
73
8 Transport and Storage
76
Preparing the Plasmaquant PQ 9000 for Transport
76
Ambient Conditions for Transport and Storage
77
Recommissioning after Transport or Storage
77
Installing the Recirculating Chiller
78
9 Disposal
79
10 Specification
80
10.1 Technical Data
80
10.1.1 Plasmaquant PQ 9000 Data
80
10.1.2 Control Computer Data
82
10.1.3 Cooling System Data
82
10.1.4 Autosampler Data
83
10.2 Guidelines and Standards
84
11 Index
85
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