Christ Epsilon 2-6D LSCplus Manuals

Manuals and User Guides for Christ Epsilon 2-6D LSCplus. We have 1 Christ Epsilon 2-6D LSCplus manual available for free PDF download: Operating Manual

Christ Epsilon 2-6D LSCplus Operating Manual (156 pages)

Freeze-dryer

Brand: Christ | Category: Laboratory Equipment | Size: 5 MB

Table of Contents
5
General Information
9
Importance of the Operating Manual
9
Further Applicable Documents
9
Intended Use
9
Freeze-Drying of Solvent-Containing Products (Non-Aqueous Media)
11
Freeze-Drying of Acid-Containing Products
12
Freeze-Drying of Azide-Containing Products
12
Warranty and Liability
12
Copyright
13
Explanation of Symbols
13
Standards and Regulations
13
Scope of Supply
13
Layout and Mode of Operation
14
Layout of the Freeze-Dryer
14
Functional and Operating Elements
14
Name Plate
19
Mode of Operation
20
General Information on Freeze-Drying
20
Freeze-Drying Process
22
Preparation
22
Freezing
23
Main Drying
23
Final Drying
24
End of Drying and Aeration
24
Defrosting
24
Safety
25
Marking of the Unit
25
Explanation of the Symbols and Notes
26
Responsibility of the Operator
27
Freeze-Drying of Solvent-Containing Products
28
Requirements Concerning the Personnel
29
Informal Safety Notes
30
Safety Notes Concerning the Transport, Set-Up and Connection and Initial Start-Up of the Freeze-Dryer
30
General Hazards
30
Hazards Caused by Improper Transport
31
Hazards Caused by Improper Set-Up
31
Hazards Caused by Improper Connection
31
Hazards During the Initial Start-Up
31
Safety Notes Concerning the Operation
32
Hazards Caused by Electricity
32
Hazards Caused by Natural, Flammable Refrigerants
32
Hazards Caused by Nitrogen
33
Hazards Caused by Harmful Products
33
Hazards Caused by Solvents in the Products
33
Hazards Caused by Acids in the Products
34
Hazards Caused by Azides in the Products
34
Hazards Caused by Contaminated Condensate (Defrosting Water)
35
Oil-Sealed Vacuum Pump: Hazards Caused by Contaminated Vacuum Pump Exhaust Gases
35
Oil-Sealed Vacuum Pump: Hazards Caused by Hot and Contaminated Vacuum Pump Oil
36
3.7.11 Dry-Running Vacuum Pump: Hazards Caused by Contaminated Exhaust Air
36
3.7.12 Hazards Caused by Noise
36
3.7.13 Hazards Caused by the Loading Door
37
3.7.14 Hazards Caused by Shelves
37
3.7.15 Hazards Caused by Hot Surfaces
37
3.7.16 Hazards Caused by Cold Surfaces
37
3.7.17 Hazards Caused by Overpressure in the Chamber
38
Safety Devices
38
Procedures in the Event of Hazards and Accidents
39
Maintenance and Cleaning of the Freeze-Dryer
40
Additions or Conversions of the Freeze-Dryer
40
Measures to be Taken to Ensure Safe Operation of the Freeze-Dryer
41
Remaining Hazards
42
Storage and Transport
43
Dimensions and Weight
43
Storage Conditions
43
Unpacking the Freeze-Dryer
44
Transport
45
Transport Safety Devices
46
Set-Up and Connection
47
Installation Site
47
Supply and Disposal Connections
48
Power Supply
48
Connection
48
Customer-Provided Fuses
48
Aeration
49
Drain
49
Vacuum Pump
50
Oil-Sealed Vacuum Pump and Exhaust Filter (Oil Mist Separator)
50
Dry-Running Vacuum Pump and Silencer
51
Pressure Control Valve
52
Vacuum Sensor
53
Drying Cartridge (Adsorption Filter)
54
Operation
55
Initial Start-Up
55
Installation of Accessories
55
Preparation
55
Switching the Freeze-Dryer on
55
Loading Door
56
Lscplus Control System
58
User Interface
58
Main Window "Manual
59
Main Window "Program
72
Main Window "Options
73
Main Window
88
Manual Freeze-Drying
88
Entering Set Values in the Manual Mode
89
Freeze-Drying with the Pgmplus Programmer Module
91
Creating a Program
95
Editing a Program
103
Copying a Program
104
Loading a Program
104
Deleting a Program
105
Optional Extensions and Special Equipment
106
Switching the Freeze-Dryer off
109
Malfunctions and Error Correction
110
General Malfunctions
110
Power Failure
111
Insufficient Vacuum
112
Small Flange Connections
112
Aeration Valve, Media Drain Valve
113
Pressure Control Valve
113
Vacuum Sensor
113
Insufficient Ice Condenser Temperature
114
Process and Error Messages
114
Service Contact
115
Maintenance and Service
116
Maintenance
116
General
116
Ice Condenser Chamber
118
Drying Chamber
118
Lamination of the Loading Door with a Special Film
118
Door Latch
119
Aeration Valve, Media Drain Valve
120
Heat Exchanger (Only Air-Cooled Freeze-Dryers)
121
Electrical System
121
Vacuum System with an Oil-Sealed Vacuum Pump
122
Vacuum System with a Dry-Running Vacuum Pump
123
Refrigeration System
124
8.1.10 Heat Transfer Medium System
124
Vacuum Sensor
125
8.1.12 Accessories
125
Disinfection of the Drying Chamber and Accessories
126
Maintenance Schedule (Oil-Sealed Vacuum Pump)
127
Maintenance Schedule (Dry-Running Vacuum Pump)
132
Service
137
Return of Defective Parts
137
Disposal
139
Disposal of the Freeze-Dryer
139
Disposal of the Packaging
139
10 Technical Data
140
Ambient Conditions
141
Technical Documentation
141
11 Appendix
142
Mathematical Relations
142
EC Declaration of Conformity in Accordance with the EC Machinery Directive
143
EC Declaration of Conformity in Accordance with the Pressure Equipment Directive
145
Table of the Sublimation Pressure Curve
147
12 Glossary
149
13 Index
151

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