User Manuals: Christ 101704 Laboratory Equipment

Manuals and User Guides for Christ 101704 Laboratory Equipment. We have 1 Christ 101704 Laboratory Equipment manual available for free PDF download: Operating Manual

Christ 101704 Operating Manual (111 pages)

Freeze-dryer

Brand: Christ | Category: Laboratory Equipment | Size: 4 MB

Table of Contents
5
General Information
9
Importance of the Operating Manual
9
Intended Use
9
Freeze-Drying of Solvent-Containing Products (Non-Aqueous Media)
10
Freeze-Drying of Acid-Containing Products
11
Warranty and Liability
12
Copyright
12
Explanation of Symbols
12
Standards and Regulations
12
Scope of Supply
13
Layout and Mode of Operation
14
Layout of the Freeze-Dryer
14
Functional and Operating Elements
14
Name Plate
16
Mode of Operation
17
General Information on Freeze-Drying
17
Freeze-Drying Process
19
Preparation
19
Freezing
20
Main Drying
20
Final Drying
21
End of Drying and Aeration
21
Defrosting
22
Safety
23
Marking of the Unit
23
Explanation of the Symbols and Notes
24
Responsibility of the Operator
25
Freeze-Drying of Solvent-Containing Products
26
Requirements Concerning the Personnel
26
Informal Safety Notes
27
Safety Notes Concerning the Transport, Set-Up and Connection and Initial Start-Up of the Freeze-Dryer
28
General Hazards
28
Hazards Caused by Improper Transport
28
Hazards Caused by Improper Set-Up
28
Hazards Caused by Improper Connection
29
Safety Notes Concerning the Operation
29
Hazards Caused by Electricity
29
Hazards Caused by the Refrigeration System (Natural, Flammable Refrigerants)
30
Hazards Caused by Harmful Products
30
Hazards Caused by Solvents in the Products
30
Hazards Caused by Acids in the Products
31
Hazards Caused by Contaminated Condensate (Defrosting Water)
31
Oil-Sealed Vacuum Pump: Hazards Caused by Contaminated Vacuum Pump Exhaust Gases
31
Oil-Sealed Vacuum Pump: Hazards Caused by Hot and Contaminated Vacuum Pump Oil
32
Hazards Caused by Noise
32
3.7.10 Hazards Caused by Hot Surfaces
32
3.7.11 Hazards Caused by Cold Surfaces
32
Safety Devices
33
System Check
33
Earth Conductor Check
33
Procedures in the Event of Hazards and Accidents
33
Maintenance and Cleaning of the Freeze-Dryer
34
Measures to be Taken to Ensure Safe Operation of the Freeze-Dryer
34
Remaining Hazards
35
Storage and Transport
36
Dimensions and Weight
36
Storage Conditions
36
Notes on Transport
37
Packaging
38
Transport Safety Device
38
Set-Up and Connection
39
Location of Use
39
Power Supply
40
Type of Connection
40
Customer-Provided Fuses
40
Aeration and Media Drain Valve
41
Vacuum Sensor
41
Vacuum Pumps
43
Oil-Sealed Vacuum Pump and Exhaust Filter (Oil Mist Separator)
43
Use of an Interface Box
44
Pressure Control Valve
47
Rubber Valves
48
Operation
49
Initial Start-Up
49
Installation of Accessories
49
Preparation
49
Switching the Freeze-Dryer on
49
Lscbasic Control System
50
User Interface
50
Main Window "Process
51
Main Window "Options
59
Main Window
69
Starting a Freeze-Drying Process
69
Entering Set Values
70
Optional Extensions
72
Switching the Freeze-Dryer off
72
Malfunctions and Error Correction
73
General Malfunctions
73
Power Failure
74
Insufficient Vacuum
75
Small Flange Connections
75
Aeration Valve, Media Drain Valve
76
Pressure Control Valve
76
Rubber Valves
76
Vacuum Sensor
76
Insufficient Ice Condenser Temperature
77
Process and Error Messages
77
Service Contact
78
Maintenance and Service
79
Maintenance
79
General
79
Ice Condenser Chamber
80
Aeration Valve, Media Drain Valve
81
Heat Exchanger (Only for Air-Cooled Freeze-Dryers)
82
Electrical System
82
Vacuum Pump
82
Exhaust Filter (Oil Mist Separator)
83
Refrigeration System
83
Vacuum Sensor
84
8.1.10 Accessories
84
Disinfection of the Drying Chamber and Accessories
85
Service
85
Return of Defective Parts
86
Disposal
88
Disposal of the Freeze-Dryer
88
Disposal of the Packaging
88
10 Technical Data
89
Ambient Conditions
90
Technical Documentation
90
11 Appendix
91
Brief Operating Instructions
91
EC Declaration of Conformity in Accordance with the EC Machinery Directive
97
Declaration of Conformity - China Rohs 2
99
EC Declaration of Conformity in Accordance with the Pressure Equipment Directive
101
Table of the Sublimation Pressure Curve
103
12 Glossary
105
13 Index
107

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