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TECHNICAL SERVICE CONTACTS
Australia:
Tel. (03) 9769.0666 • Fax (03) 9769.0699
e-mail: hannains@hannainst.com.au
China:
Tel. (10) 88570068 • Fax (10) 88570060
e-mail: hannachina@vip.sina.com
Egypt:
Tel. & Fax (02) 2758.683
e-mail: hannaegypt@go.com.eg
Germany:
Tel. (07851) 9129-0 • Fax (07851) 9129-99
e-mail: hannager@aol.com
Greece:
Tel. (210) 823.5192 • Fax (210) 884.0210
e-mail: hannagr@otenet.gr
Indonesia:
Tel. (21) 4584.2941 • Fax (21) 4584.2942
e-mail: transit@dnet.net.id
Japan:
Tel. (03) 3258.9565 • Fax (03) 3258.9567
e-mail: sales@hanna.co.jp
Korea:
Tel. (02) 2278.5147 • Fax (02) 2264.1729
e-mail: mccoyhan@chollian.net
Malaysia:
Tel. (603) 5638.9940 • Fax (603) 5638.9829
e-mail: hannamal@tm.net.my
Norway:
Tel. (23) 3811.00 • Fax (23) 3811.01
e-mail: hanna@hannainst.no
Singapore:
Tel. 6296.7118 • Fax 6291.6906
e-mail: hannaap@pacific.net.sg
South Africa:
Tel. (011) 615.6076 • Fax (011) 615.8582
e-mail: hannasa@mweb.co.za
United Kingdom:
Tel. (01525) 850.855 • Fax (01525) 853.668
e-mail: salesteam@hannainst.co.uk
USA:
Tel. (401) 765.7500 • Fax (401) 765.7575
e-mail: sales@hannainst.com
For additional Technical Support in your local lan-
guage, see www.hannainst.com
Instruction Manual
C 214
Multiparameter Bench
Photometer
for
Wastewater Treatment
Application
These Instruments are in
w w w . h a n n a i n s t . c o m
Compliance with the CE Directives
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Table of Contents
Related Manuals for Hanna Instruments C 214
Summary of Contents for Hanna Instruments C 214
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Page 1: Instruction Manual
Instruction Manual TECHNICAL SERVICE CONTACTS Australia: Tel. (03) 9769.0666 • Fax (03) 9769.0699 e-mail: hannains@hannainst.com.au C 214 China: Tel. (10) 88570068 • Fax (10) 88570060 e-mail: hannachina@vip.sina.com Multiparameter Bench Egypt: Photometer Tel. & Fax (02) 2758.683 e-mail: hannaegypt@go.com.eg Germany: Tel. (07851) 9129-0 • Fax (07851) 9129-99 e-mail: hannager@aol.com Wastewater Treatment Greece:... -
Page 2: Table Of Contents
ABBREVIATIONS ......3 NITROGEN, TOTAL HR ....42 If the instrument is to be returned to Hanna Instruments, first obtain a GENERAL DESCRIPTION ....4 OXYGEN DEMAND, CHEMICAL LR ..47 Returned Goods Authorization Number from the Customer Service SPECIFICATIONS ...... -
Page 3: Preliminary Examination
CE DECLARATION OF CONFORMITY PRELIMINARY EXAMINATION Please examine this product carefully. Make sure that the instrument is not damaged. If any damage occured during shipment, please notify your Dealer. Each Meter is supplied complete with: • Five Sample Vials • Two 9 V Batteries •... -
Page 4: General Description
GENERAL DESCRIPTION ACCESSORIES REAGENT SETS C 99 & C 200 Series is a line of 17 different bench, microprocessor- based photometers to measure more than 50 different parameters in HI 93701-01 100 free chlorine tests water and wastewater. These multipurpose meters are manufactured HI 93701-03 300 free chlorine tests to measure the most important parameters of the application they HI 93711-01 100 total chlorine tests... -
Page 5: Specifications
STANDARD METHODS SPECIFICATIONS Light Life Life of the instrument Description Range Method Ammonia LR 0.00 to 3.00 mg / L Nessler Light Detector Silicon Photocell Ammonia HR 0 to 100 mg / L Nessler Chlorine, Free 0.00 to 5.00 mg / L Environment 0 to 50°C (32 to 122°F);... -
Page 6: Principle Of Operation
/PUP - Program Up PRINCIPLE OF OPERATION /PDN - Program Down /PTM - Turn Test Mode On Absorption of Light is a typical phenomenon of interaction between electromagnetic radiation and matter. When a light beam crosses a /Brx - Set the baud rate substance, some of the radiation may be absorbed by atoms, molecules 1 - 300 2 - 600... - Page 7 ® , it is possible to remotely control your Hanna Instruments bench It is necessary that the surface of the vial is clean and not scratched. meter. Use HI 920010 cable to connect the meter to the PC, start the...
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Page 8: Functional Description
• Wait for a few seconds and the FUNCTIONAL DESCRIPTION display will show “-0.0-”. Now the meter is zeroed and ready for FRONT PANEL measurement. • Remove the blank vial. • Place the sample vial into the holder and push it completely down. •... -
Page 9: Guide To Display Codes
• At the end of the digestion place the GUIDE TO DISPLAY CODES vials carefully in the test tube rack and allow to cool to room temperature. Note: The secondary LCD below shows a generic "P– –", whereas the Warning: as the vials are still hot, meter will indicate the exact program number (e.g. - Page 10 Reagent Blank Correction: This method needs a reagent blank The lamp is not working properly. Contact correction. A single blank vial may be used more than once; the blank your dealer or the nearest Hanna Customer vial is stable up to one day (room temperature). For most accurate Service Center.
- Page 11 A zero reading was not taken. Follow the PHOSPHORUS, TOTAL HIGH RANGE instruction described in the measurement procedures for zeroing the meter. SPECIFICATIONS Range 0.0 to 100.0 mg/L (as PO Under range. A blinking "0.00" indicates Resolution 0.1 mg/L that the sample absorbs less light than the Precision ±3.0 @ 75.0 mg/L zero reference.
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Page 12: Measurement
• Place the sample vial into the holder TIPS FOR AN ACCURATE MEASUREMENT and push it completely down. The instructions listed below should be carefully followed during testing to ensure most accurate results. • Press READ DIRECT and "SIP" will blink on the display. COLLECTING AND MEASURING SAMPLES •... - Page 13 • Select the program number corresponding to Reactive Phosphorus 2. In order to measure exactly e.g. 0.5 mL of reagent with the 1 mL High Range on the secondary LCD by pressing PROGRAM M and L. syringe: (a) push the plunger completely into the syringe and insert the •...
- Page 14 • Proper use of the powder reagent packet: PHOSPHORUS, REACTIVE HIGH RANGE (a) use scissors to open the powder packet; (b) push the edges of the packet to form a spout; SPECIFICATIONS (c) pour out the content of the packet. Range 0.0 to 100.0 mg/L (as PO Resolution...
- Page 15 • Press TIMER and the display will show the countdown prior to the (b) shake the vial: move the vial up and down. The movement measurement. Alternatively, wait for 3 minutes and press READ may be gentle or vigorous. DIRECT. In both cases "SIP" will blink during measurement. •...
- Page 16 • Do not let the reacted sample stand too long after reagent is • Replace the cap tightly and mix by added, or accuracy will be lost. inverting the vial a couple of times. This is the blank. • It is possible to take multiple readings in a row, but it is recommended to take a new zero reading for each sample and to •...
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Page 17: Phosphorus, Total
• Preheat the Hanna Reactor C 9800 to 150 °C (302°F). For correct PARAMETERS REFERENCE TABLES use of the reactor follow Reactor Instruction Manual. Use of the optional HI 740217 safety shield is strongly recommended. C 214 - WATER TREATMENT APPLICATION Do not use an oven or microwave because leaking samples can generate a corrosive and possibly explosive atmosphere. - Page 18 • The letter refers to: PHOSPHORUS, TOTAL : ammonia : nitrate; total nitrogen SPECIFICATIONS : phosphorus Range 0.00 to 3.50 mg/L (as PO (no letter) : chemical oxygen demand (COD) and generic empty Resolution 0.01 mg/L vials. Precision ±0.06 @ 2.50 mg/L Typical EMC ±0.01 mg/L •...
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Page 19: Health & Safety
• The instrument directly displays concentration in mg/L of HEALTH & SAFETY phosphate (PO ) on the Liquid Crystal Display. The method detects free (orthophosphate) and condensed inorganic The chemicals contained in the reagent kits may be forms (meta-, pyro- and other polyphosphates) of phosphates hazardous if improperly handled. -
Page 20: Operational Guide
• Mark the vial with a pencil on the OPERATIONAL GUIDE white band to place an orientation sign. Use this sign to insert the test POWER CONNECTION vial always in the same position into Plug the 12VDC adapter (HI 710005 - 110VDC, or HI 710006 - the holder. - Page 21 • Preheat the Hanna Reactor C 9800 to 150 °C (302°F). For correct • After the desired program number appears on the secondary display, use of the reactor follow Reactor Instruction Manual. follow the measurement procedure described in the related chapter. Use of the optional HI 740217 safety shield is strongly recommended.
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Page 22: Ammonia Low Range
AMMONIA LOW RANGE PHOSPHORUS, ACID HYDROLYZABLE SPECIFICATIONS SPECIFICATIONS Range 0.00 to 3.00 mg/L (as NH Range 0.00 to 5.00 mg/L (as PO Resolution 0.01 mg/L Resolution 0.01 mg/L Precision ±0.03 @ 1.50 mg/L Precision ±0.06 @ 2.50 mg/L Typical EMC ±0.01 mg/L Typical EMC ±0.01 mg/L... - Page 23 • The instrument directly displays concentration in mg/L of • Mark the vial with a pencil on the phosphate (PO ) on the Liquid Crystal Display. white band to place an orientation • To convert the reading to mg/L of P , multiply by a factor of sign.
- Page 24 • The instrument directly displays concentration in mg/L of ammonia • Mark the vial with a pencil on the nitrogen (NH -N) on the Liquid Crystal Display. white band to place an orientation sign. Use this sign to insert the test •...
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Page 25: Ammonia High Range
PHOSPHORUS, REACTIVE AMMONIA HIGH RANGE SPECIFICATIONS SPECIFICATIONS Range 0.00 to 5.00 mg/L (as PO Range 0 to 100 mg/L (as NH Resolution 0.01 mg/L Resolution 1 mg/L Precision ±0.05 @ 2.50 mg/L Precision ±3 @ 50 mg/L Typical EMC ±0.01 mg/L Typical EMC ±1 mg/L Deviation... - Page 26 • Mark the vial with a pencil on the • Select the program number corresponding to Oxygen Demand, white band to place an orientation Chemical HR (COD) on the secondary LCD by pressing PROGRAM sign. Use this sign to insert the test M and L.
- Page 27 • Choose a homogeneous sample. Samples containing settleable solids • The instrument directly displays concentration in mg/L of ammonia need to be homogenized with a blender. nitrogen (NH -N) on the Liquid Crystal Display. • To convert the reading to mg/L of ammonia (NH ), multiply by a •...
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Page 28: Chlorine, Free
CHLORINE, FREE OXYGEN DEMAND, CHEMICAL HIGH RANGE SPECIFICATIONS SPECIFICATIONS Range 0.00 to 5.00 mg/L Range 0 to 15000 mg/L Resolution 0.01 mg/L from 0.00 to 0.99 mg/L; Resolution 10 mg/L 0.1 mg/L above 0.99 mg/L Precision ±220 @ 10000 mg/L Precision ±0.04 @ 1.00 mg/L Typical EMC... - Page 29 • Select the program number corresponding to Oxygen Demand, • Place the vial into the holder and Chemical MR (COD) on the secondary LCD by pressing PROGRAM push it completely down. M and L. • Press ZERO and “SIP” will blink on the display. •...
- Page 30 Oxidized forms of Chromium and Manganese • Choose a homogeneous sample. Samples containing settleable solids Ozone (O need to be homogenized with a blender. Alkalinity above 250 mg/L CaCO or acidity above 150 mg/L CaCO will • Preheat the Hanna Reactor C 9800 to 150 °C (302°F). For correct not reliably develop the full amount of color or it may rapidly fade.
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Page 31: Chlorine, Total
OXYGEN DEMAND, CHEMICAL MEDIUM CHLORINE, TOTAL R A N G E SPECIFICATIONS SPECIFICATIONS Range 0 to 1500 mg/L Range 0.00 to 5.00 mg/L Resolution 1 mg/L Resolution 0.01 mg/L from 0.00 to 0.99 mg/L; 0.1 mg/L above 0.99 mg/L Precision ±22 @ 1000 mg/L Precision ±0.04 @ 1.00 mg/L... - Page 32 • Place the vial into the holder and • Select the program number corresponding to Oxygen Demand, push it completely down. Chemical LR (COD) on the secondary LCD by pressing PROGRAM M and L. • Press ZERO and “SIP” will blink on the display. •...
- Page 33 • Choose a homogeneous sample. Samples containing settleable solids INTERFERENCES need to be homogenized with a blender. A positive interference may be caused by: Bromine (Br • Preheat the Hanna Reactor C 9800 to 150 °C (302°F). For correct Iodine (I use of the reactor follow Reactor Instruction Manual.
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Page 34: Nitrate
NITRATE OXYGEN DEMAND, CHEMICAL LOW RANGE SPECIFICATIONS SPECIFICATIONS Range 0.0 to 30.0 mg/L (as NO Range 0 to 150 mg/L Resolution Resolution 0.1 mg/L 1 mg/L Precision ±0.5@ 25.0 mg/L Precision ±4 @ 150 mg/L Typical EMC ±0.1 mg/L Typical EMC ±1 mg/L Deviation Deviation... - Page 35 • Place the blank vial into the holder • Replace the cap tightly and invert and push it completely down. the vial 10 times. This is the blank. Warning: as the vial becomes hot during mixing, be careful in handling •...
- Page 36 • Place the vial into the holder and • Remove the cap from the vials and add the content of one packet push it completely down. Ensure that of HI 93767-0 Total Nitrogen Reagent to each vial. Replace the the vial orientation respect to the cap tightly and shake gently the vials for 15 seconds.
- Page 37 • Replace the cap tightly and shake vigorously the vials for about NITROGEN, TOTAL LOW RANGE 30 seconds until all the powder is completely dissolved. SPECIFICATIONS Range 0.0 to 25.0 mg/L Resolution 0.1 mg/L Precision ±0.5 @ 15.0 mg/L Typical EMC ±0.1 mg/L Deviation Light Source...
- Page 38 MEASUREMENT PROCEDURE MEASUREMENT PROCEDURE Before starting to use the reagent kit it is recommended Before starting to use the reagent kit it is recommended to read carefully all the instructions and the Health & to read carefully all the instructions and the Health & Safety Data Sheet (HSDS).
- Page 39 • Replace the cap tightly and shake the vials vigorously for about NITROGEN, TOTAL HIGH RANGE 30 seconds until all the powder is completely dissolved. SPECIFICATIONS Range 10 to 150 mg/L Resolution 1 mg/L Precision ±3 @ 75 mg/L Typical EMC ±1 mg/L Deviation Light Source...
- Page 40 • Remove the cap from the vials and add the content of one packet • Place the blank vial into the holder of HI 93767-0 Total Nitrogen Reagent to each vial. Replace the and push it completely down. cap tightly and shake gently the vials for 15 seconds. •...
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