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Parr Instrument 4555 Operating Instructions Manual
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Parr Instrument 4555 Operating Instructions Manual

2.6 & 5 gallon reactor systems
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4555-4558
2.6 & 5 Gallon Reactor Systems
Operating Instruction Manual

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Summary of Contents for Parr Instrument 4555

  • Page 1 4555-4558 2.6 & 5 Gallon Reactor Systems Operating Instruction Manual...
  • Page 2 4555-58 Pressure Reactors PREFACE HOW TO USE THE VESSEL Scope Flat Gasket or Self Sealing O-ring Closure Related Instructions Open the Vessel Intended Usage Before Closing the Vessel Safety Information Close the Vessel General Specifications Gas Connections Explanation of Symbols...
  • Page 3 2. Ensure that the equipment is connected to installation and operation of standard Models electrical service according to local national 4555, 4556, 4557, and 4558 (2.6 and 5 Gallon volume) electrical codes. Failure to properly connect may Reactors. It should be noted that these reactors can create a fire or shock hazard.
  • Page 4 Use proper and safe Caution! lifting techniques and equipment when installing Do not use in hazardous atmospheres. or moving the Series 4555-58 Reactors and/ or its components. Operating: 15 ºC to 35 ºC; maximum relative humid- Cleaning & Maintenance ity of 80% non-condensing.
  • Page 5 4555-58 Pressure Reactors Users Responsibility All r eactors and pressure vessels are designed and manufactured with great care to assure safe operation when used within their prescribed temperature and pressure limits. But… the basic responsibility for safety when using this equipment rests entirely with the user; who must: 1.
  • Page 6 4555-58 Pressure Reactors INSTALLATION Assemble the Reactor These reactors require a work area in a well ven- Pressure and Temperature Limits tilated area with convenient access to an electric outlet, running water and a drain. This unit needs The working pressure and temperature at which...
  • Page 7 4555-58 Pressure Reactors Install the Split-Rings per instructions in sec- 6. Lift “up” on joystick to raise cylinder, push tion, "How to Use the Vessel" (p. 11-13). “down” to lower. The joystick can provide speed control up to the maximum preset 8.
  • Page 8 4555-58 Pressure Reactors IDENTIFY THE VALVES Gas Inlet Valve Liquid Sampling Valve The gas inlet valve is easily identified when the The liquid sampling valve is attached to the same vessel is open by noting that it is connected to a...
  • Page 9 Two types of drive systems are available on the tion. Now hold the fitting firmly in place and close 4555 Series Reactors. They are the direct drive and the joint by tightening the 209HC4 bushing. This the gearbox drive. The direct drive has the motor...
  • Page 10 4555-58 Pressure Reactors Quick Disconnect Drive Coupler If the motor becomes sluggish, flush it with a non- flammable solvent in a well ventilated area. Dis- The top coupler half is stationary mounted with connect the airline and muffler and pour a small a set screw to the drive motor shaft.
  • Page 11 Before Closing the Vessel Examine the head gasket carefully to be sure that The vessels used in Model 4555, 4556, 4557, and it is in good condition. In flat gasket designs, after 4558. Reactors have two types of closures: fixed considerable use, some of the PTFE gasket may head and moveable head.
  • Page 12 4555-58 Pressure Reactors Gas Connections Releasing Pressure Gas connections are dependent on applications. Use the gas release valve to reduce the pressure in For general usage, use the pressure hose furnished the vessel if the reactor is accidentally overcharged with the reactor. Screw the Type "A" coned pressure when filling.
  • Page 13 4555-58 Pressure Reactors A1761HCEE 3-Zone Slave Control Box Initial Operating Test The A1761HCEE slave control box is supplied with Read all operating instructions carefully so as to a 250 volt, 50 amp (NEMA 6-50P) power plug. A be well acquainted with the correct procedures for...
  • Page 14 4555-58 Pressure Reactors MAINTENANCE 5. NPT (National Pipe Taper) threads should not be disassembled any more than necessary. It will become increasingly difficult to maintain a General Maintenance Notes tight seal with these tapered threads if the joint is made and broken repeatedly.
  • Page 15 4555-58 Pressure Reactors Periodic Pressure Tests Technical Support Company strives provide Each cylinder used in a stirred reactor is tested customers with world class support. When con- under hydrostatic pressure to the higher of 1.43 tacting for technical support, please provide...
  • Page 16 4555-58 Pressure Reactors PARTS LIST For special material reactor vessels, add material code as a suffix to the standard part number for head, cylinder, and/or internal fittings made from alternate materials CA - Titanium CG - Alloy B-2 CX - Zirconium...
  • Page 17 4555-58 Pressure Reactors Internal Parts External Fittings Thermowell Part No. Description Part No. Description 94CAAD Plug, Hex Head, 1/4NPTM, T316SS 265HC15 Thermowell, 5G 15.94”L A278VBAD Valve, Straight 3/8" NPTM (Liquid Sampling) 265HC10 Thermowell, 2.6G 12.12”L A279VBAD Valve, Angled 3/8" NPTM x 3/8" NPTM...
  • Page 18 4555-58 Pressure Reactors Vessel Parts (Moveable Head Vessel Shown) 56HC SERIES PRESSURE GAGE A279VBAD 94CAAD ANGLE VALVE PLUG, 1/4 NPT 420HC6 A279VBAD ADAPTER ANGLE VALVE 208HC18 1566HC ADAPTER ADAPTER A278VBAD 208HC15 STRAIGHT VALVE GAGE ADAPTER 209HC4 209HC4 ADAPTER BUSHING ADAPTER BUSHING...
  • Page 19 4555-58 Pressure Reactors Drive Parts List Floor Stand Parts (Fixed Head Vessel) Motor Part No. Description Part No. Description A2760HC2 Pneumatic Lift Package with A388E2ES Motor, 1/2 HP VS 90VDC Regulator, Hand Lever & Tubing A388E2EQ Motor, 1/2 HP EXP VS 90VDC...
  • Page 20 4555-58 Pressure Reactors Drawings Motor/Drive Detail MOTOR OPTIONS A388E2ES 1/2 HP 90VDC VAR SPEED A388E2ET 1/2 HP 90VDC VAR SPEED A388E2EQ 1/2 HP 90VDC VAR SPEED EXP PROOF A388E2ER 1/2 HP 180VDC VAR SPEED EXP PROOF A388E3ET 3/4 HP 180VDC...
  • Page 21 4555-58 Pressure Reactors Moveable Head Vessel Reactor 5 Gallon Assembly Layout View 1680HC 1593HC PIVOT STOP LIFT RING (4) SB3118HX20 SB3118HX20 SN5013HX 5/16-18 X 1.25 HHCS 5/16-18 X 1.25 HHCS 1/2-13 HEX JAM NUT (3) TN3118HL TW31NL 5/16-18 UNITORQUE 5/16 LOCK WASHER,...
  • Page 22 21.01 REF (TYP) 1.50 REF .41 REF A2610HC SERIES TYP (8) PLACES FLOOR STAND ASSY Ceramic Heater 3-Zone, 5 Gallon 230V/7550 Watt For use with 4555 Reactor 173F HOT SURFACE SYMBOL LABEL 230F LABEL ZONE 2 230F 230F LABEL ZONE 3...
  • Page 23 4555-58 Pressure Reactors Ceramic Heater 3-Zone, 5 Gallon 230V/7550 Watt (Continued) For use with 4555 Reactor SHELL SEAM 7X SP12DM02 1/8 X 1/8 RIVET 1583HC HEADER, TOP MARANITE ME1587HC SHELL, HEATER XC0090 INSULATION, CERABLANKET 1582HC TIE BOLT 1/2-13 THD 19.0" LG...
  • Page 24 4555-58 Pressure Reactors Fixed Head Vessel Reactor Drawings 5 Gallon Fixed Head Reactor Stand General Arrangement SEE PAGES 30-32 FOR MOTOR SUPPORT PACKAGE SEE PAGE 33 FOR HINGED SPLIT-RING SUPPORT PACKAGE 94.13 DIRECT DRIVE SEE PAGE 27 FOR SEE PAGE 29 FOR 79.75...
  • Page 25 4555-58 Pressure Reactors 2.6 Gallon Fixed Head Reactor Stand General Arrangement SEE PAGE 33 FOR HINGED SPLIT-RING SUPPORT PACKAGE 86.13 SEE PAGE 29 FOR CYLINDER SLIDE SEE PAGE 27 FOR DIRECT PACKAGE MAIN SUPPORT DRIVE FRAME PACKAGE 13.62 (TRAVEL) 70.75 *12.32 (TRAVEL)*...
  • Page 26 4555-58 Pressure Reactors 5 Gallon Fixed Head Reactor Stand General Arrangement, Detailed (3) TW50SL 1/2 LOCK WASHER 1798HC (3) SN5013HX 1/2-13 HEX JAM NUT OPTICAL SHIELD (OPTIONAL) (FOR SUPPORT RODS) 1564HC OPTICAL WHEEL (OPTIONAL) (3) 3156HC SUPPORT ROD SEE NOTE:...
  • Page 27 4555-58 Pressure Reactors Fixed Head Reactor Stand Basic Main Support Frame Package 3137HC2 RAIL, MAIN SUPPORT TOP (17") (4) 3790HC2 DOUBLE SHORT ANCHOR (2) 3172HC BRACKET, CORNER W/GUSSET 8-HOLE (4338) (4) 3167HC T-NUTS, DOUBLE (1379) (8) 3193HC 5/16-18 X 5/8 FBHSCS BLK...
  • Page 28 4555-58 Pressure Reactors Fixed Head Reactor Stand Pneumatic Vertical Lift Package (2) 3813HC PLATE, COVER, ALUM (4) 3193HC 5/16-18 X 5/8 FBHSCS (4) 3147HC BRACKET, CORNER 6-HOLE, SLOT (4285) (12) 3167HC 3145HC T-NUTS, DOUBLE (3279) RAIL, MAIN SUPT, 16" LG...
  • Page 29 4555-58 Pressure Reactors Fixed Head Reactor Stand Horizontal Slide Package 3153HC2 (4) 3148HC CYLINDER SUPPORT PLATE LINEAR BEARING, DBL FLG (4) SW16NL #8 LOCK WASHER INT TOOTH (4) SA1632RD06 8-32 X 3/8 RHMS (2) 2759HC GROMMET (2) 2548HC3 HANDLE, LIFT...
  • Page 30 4555-58 Pressure Reactors Motor Support Platform Package For Reactors with 56C Motors (Direct Drive) PART NO. DESCRIPTION 1774HC COUPLER HALF , MACHINED 1746HC SPIDER COUPLING 3161HC2 MOTOR SUPPORT PLATE, 56C 3162HC3 ADAPTER PLATE, 56C MOTOR, 2.6 G 1/2 HP XPF 3163HC3 SHAFT ADAPTER, 56C MOTOR, 2.6 G...
  • Page 31 4555-58 Pressure Reactors Motor Support Platform Package For Reactors with 56C Motors (Gear Boxes) PART NO. DESCRIPTION 1774HC COUPLER HALF , MACHINED 1746HC SPIDER COUPLING 1890HC2 GEARBOX, 3:1 INLINE 2025HC GEARBOX, 5:1 OFFSET 1/2 HP XPF 2025HC2 GEARBOX, 10:1 OFFSET...
  • Page 32 4555-58 Pressure Reactors Motor Support Platform Package (Continued) For Reactors with 56C Motors (Gear Boxes) (4) SB3118HX24 5/16-18 X 1-1/2 HHCS (4) SB3716HX16 (4) SW31FT 3/8-16 X 1 HHCS 5/16 FLAT WASHER (4) SW37NL (4) TW31NL 3/8 LOCK WASHER 5/16 FLAT WASHER...
  • Page 33 4555-58 Pressure Reactors Hinged Split-Ring Assembly, HD For 4557 and 4558 Fixed Head Reactors 4X SD5013SC08 3289HC2 1/2-13 SHSB UNIVERSAL PIVOT NUB, HD 4X SB3118SC24 2X 3167HC 4X 3493HC2 PIVOT WASHER, TOP, HD 4X 3288HC2 SEE NOTE 2 PIVOT ARM, HD...
  • Page 34 4555-58 Pressure Reactors Controller Cart For 4557 and 4558 Fixed Head Reactors 4848M A2500HC15 MASTER CONTROL CONTROLS CART A1761HCEE OR A1761HC3 3 ZONE SLAVEBOX NOTE: CART DIMENSIONS (WITH CASTERS) 2' SQUARE X 29.67" TALL 4557_S3 R1...
  • Page 35 4 0 3 M R 0 8 0 3 / 2 8 / 1 7...

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4558