Related Manuals for Parr Instrument 4590
Summary of Contents for Parr Instrument 4590
- Page 1 (217) 352-9330 | Click HERE Find the Parr Instrument 4592 at our website:...
- Page 2 399M 4590 Micro Bench Top Reactors Operating Instruction Manual Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
- Page 3 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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Page 4: Table Of Contents
Flat Gasket or Self Sealing O-Ring Closure General Maintenance Notes Periodic Pressure Tests INSTALLATION Technical Support Pressure and Temperature Limits SERIES 4590 VESSEL PARTS LISTS Assemble The Reactor Standard Reaction Vessel Parts List IDENTIFY THE VALVES High Pressure Reaction Vessel Parts List Gas Inlet Valve... -
Page 5: Preface
These instructions describe the installation, opera- 2. Ensure that the equipment is connected to tion and maintenance of Parr Series 4590 Bench Top electrical service according to local national Micro Reactors which are offered in three sizes 25, electrical codes. -
Page 6: Explanation Of Symbols
Environmental Conditions Provisions for Lifting and Carrying This instrument is intended to be used indoors. The 4590 and its components are very heavy. Before moving ensure all cables are disconnected. Use proper and safe lifting techniques when installing or moving the 4590 and/or its components. -
Page 7: User's Responsibility
Parr Instrument Company. P a r r I n s t r u m e n t C o m p a n y... -
Page 8: Fixed Head Or Removable Head Vessel Design
4590 Micro Reactors Parr Series 4590 Micro Reactors are furnished with two structural options in addition to the size, pressure range, stirrer motor, controller and similar options. These are: Fixed Head or Removable Head Vessel Design Flat Gasket or Self Sealing O-Ring Closure... -
Page 9: Installation
& 100 mL reactors must not exceed the following which it applies. The standard material of construc- maximum limits: tion for Parr Instrument Company is Type 316 Stain- less Steel. Pressure Vessel and Temperature Limits In the standard pressure and temperature setup, the... -
Page 10: Assemble The Reactor
See Instruction Manual The Parr Cooling output connector is to be used 231M. only with Parr Instrument Company cooling solenoid valve assemblies supplied with the 9. Note the voltage and amperage requirement appropriate cooling power cord. -
Page 11: Identify The Valves
4590 Micro Reactors IDENTIFY THE VALVES Liquid Sampling Valve Gas Inlet Valve The liquid sampling valve is attached to the same The gas inlet valve is easily identified when the fitting as the gas inlet valve and connected to the vessel is open by noting that it is connected to a dip same dip tube. -
Page 12: Other Vessel Head Fittings
They can be ordered from where a gage is selected with a range under 1000 any Parr Dealer or direct from the Parr Instrument psi, a relief valve is added and set to protect the Company. The order must specify the reactor size gage. -
Page 13: Air Motor
4590 Micro Reactors Air Motor If the motor becomes sluggish, flush it with a non-flammable solvent in a well ventilated area. Variable stirring speeds from 100 to 2000 rpm Disconnect the air line and muffler and pour a small with no spark hazard can be obtained by replacing amount of solvent into the inlet port. - Page 14 Notes w w w . p a r r i n s t . c o m Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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Page 15: How To Use The Vessel
4590 Micro Reactors HOW TO USE THE VESSEL Sealing with Flexible Graphite Gaskets Removable Vessels Tighten the cap screws with enclosed wrench in Always remove removable vessels from the support same criss-cross pattern as the PTFE gasket. Initially stand before attempting to open or close them. -
Page 16: Gas Connections
4590 Micro Reactors Note: The following steps are common to both head configurations. Gas Connections Do Not Overfill the Vessel Always watch the pressure gage closely when admit- For a gas connection to the vessel, use the A495HC pressure hose (A506HC in high pressure reactors) ting gas so as not to exceed the maximum working limit. -
Page 17: Maintenance
8. Clean all threads and gas passages thoroughly pect parts should be replaced by components and remove all tape fragments when overhaul- only supplied by Parr Instrument Company. ing a vessel. An ultrasonic bath is excellent for cleaning metal parts, but do not place a thermo- 2. -
Page 18: Periodic Pressure Tests
Reactor. Do not discard this Parts List. You should use this parts list for reordering consumable and To return a vessel for repair, contact Parr Instrument replacement parts to ensure that you order the cor- Company for a return authorization number (RMA). -
Page 19: Series 4590 Vessel Parts Lists
4590 Micro Reactors SERIES 4590 VESSEL PARTS LISTS Standard Vessel Fittings (3000 psig / 350 °C) Standard Reaction Vessel Parts List Cylinders* Consult the itemized list for your reactor provided along Part No. Description Code with this manual. For purpose of reactor identification,... - Page 20 4590 Micro Reactors Heads* Shaft/Impeller Assembly Part No. Description Code Part No. Description Code 2432HC Head RV FG A1987HC Shaft/Impeller, 25/50 mL 2902HC Head RV OR A1987HC2 Shaft/Impeller, 100 mL 2772HC Head FH FG A1987HC3 Shaft/Impeller, 25/50 mL 2774HC Head...
- Page 21 4590 Micro Reactors High Pressure Vessel Fittings (5000 psig / 350 °C) 593HC SERIES GAGE A1120HC6 MAG DRIVE A451VB VALVE 836HC GAGE ADAPTER 420HC2 ADAPTER A455VB2 VALVE 1401HC HEX RED NIPPLE 2432HC HEAD 195VBAD 555VBAD RED ADAPTER A1357E_STYLE 302VBAD FEMALE...
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Page 22: High Pressure Reaction Vessel Parts List
4590 Micro Reactors High Pressure Reaction Vessel Parts List Dip Tube* Consult the itemized list for your reactor provided Part No. Description Code along with this manual. For purpose of reactor identifi- 1443HC Dip Tube, 25 mL cation, the following abbreviation/codes are used:... - Page 23 4590 Micro Reactors High Pressure / High Temperature Vessel Fittings (5000 psig / 500 °C) 491HCAD 593HC SERIES NIPPLE, HEX 1/4 NPTM GAGE, PRESSURE 420HC2 ADAPTER, A SKT X 1/4 NPTF 154VB2 ELBOW 1/4NPTM-F A176VB VALVE, STRAIGHT 491HCAD 1/4 NPTF-F...
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Page 24: Hp/Ht Reaction Vessel Parts List
4590 Micro Reactors High Pressure / High Temperature Reaction Thermowell* Vessel Parts List Part No. Description Code Consult the itemized list for your reactor provided A2067HC5 Thermowell, 25/50mL along with this manual. For purpose of reactor identi- A2067HC4 Thermowell, 100mL... -
Page 25: Overarm And Stand Parts List
4590 Micro Reactors TACH SENSOR ASSEMBLY RELEASE KNOB Overarm and Stand Parts List BELT GUARD OPTICAL WHEEL DRIVE PULLEY OVERARM PLATE DRIVEN PULLEY BELT ISOLATOR HUB ASSEMBLY ENCASEMENT SNAP RING UPPER DRIVE SHAFT MOTOR COLLAR UNIVERSAL COUPLING BACK PLATE Driven Pulley Assembly Part No. -
Page 26: Support Stands
4590 Micro Reactors Support Stands 4591/4592 Micro Reactor with 1/8 hp Variable Speed Motor 147C4 CONDENSER ROD (OPTIONAL) A2262E TACH PKG 845HC2 RELEASE KNOB 2231HC BUSHING (OPTIONAL) (OPTIONAL) SW51FT WASHER (OPTIONAL) SN5013HX HEX NUT (OPTIONAL) 1.49 (DOWN POSITION) 2224HC BELT GUARD (STD) 857HC5 DRIVE PULLEY (SHOWN) 2.05 (UP POSITION) - Page 27 4590 Micro Reactors 4591/4592 Micro Reactor with Variable Speed 1/4 HP and Explosion Proof Motors 4X TW19NL LOCK WASHER 4X SB1932BT06 10-32 X 3/8 BHSCS A3443HC BEARING HOUSING ASSEMBLY (REF) 2221HC HOUSING, BEARING 2187HC BEARING 2226HC SNAP RING 2222HC DRIVE SHAFT...
- Page 28 4590 Micro Reactors 4593 Micro Reactor with Fixed Head w w w . p a r r i n s t . c o m Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
- Page 29 399M R06 01/22/15 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
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