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Summary of Contents for Parr Instrument 4540
- Page 1 No. 394M Parr Instrument Company Operating Instruction Manual for 4540 Pressure Reactors...
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Page 2: Table Of Contents
Parr Instrument Company 4540 Pressure Reactors Parts Lists......... 17 TABLE OF CONTENTS Reaction Vessel Parts List .... 17 Overarm Parts List ......19 Preface..........3 Cooling Coil Parts List....21 Scope ..........3 Vessel Heater Parts List ....22 Safety Information ......3 General Specifications ....3... -
Page 3: Preface
These instructions describe the Electrical ratings installation, operation and maintenance of Controller ratings are found in the Operating Parr Series 4540 Pressure Reactors offered Instructions for the controller supplied with in two sizes, 600 mL and 1200 mL. They your reactor. -
Page 4: Alert Symbols
Parr Instrument Company 4540 Pressure Reactors Alert Symbols This CAUTION symbol may be present on the Product Instrumentation and literature. If present on the product, the user must consult the appropriate part of the accompanying product literature for more information. -
Page 5: Intended Usage
Parr Instrument If this equipment is used in a manner Company. beyond its intended usage, the protection 2. -
Page 6: Installation
The standard material of Limits for vessels will be determined construction for Parr Instrument Company is by the physical characteristics of the vessel Type 316 stainless steel. material and will be prescribed on an The working pressure and individual basis. -
Page 7: Assemble The Reactor
Parr Instrument Company 4540 Pressure Reactors ASSEMBLE THE REACTOR These reactors require at least 10 sq. ft. of Set the 4840 Series Temperature work space in a well ventilated area with Controller near the reactor, leaving a convenient access to an electric outlet, space of at least six inches between running water and a drain. -
Page 8: Identify The Valves
Parr Instrument Company 4540 Pressure Reactors IDENTIFY THE VALVES Gas Inlet Valves Liquid Sampling Valve The gas inlet valve is easily identified The liquid sampling valve is attached when the bomb is open by noting that it is to the same fitting as the gas inlet valve and connected to a dip tube which extends to a connected to the same dip tube. -
Page 9: Other Vessel Head Fittings
Parr Instrument Company 4540 Pressure Reactors OTHER VESSEL HEAD FITTINGS Safety Rupture Disc Pressure Gage There is a safety rupture disc A pressure gage, usually 0-7500 psi attached to the head which is intended to with a T316 stainless steel Bourdon tube, is... -
Page 10: How To Use The Vessel
Parr Instrument Company 4540 Pressure Reactors Removable Head Vessels HOW TO USE THE VESSEL First, open the gas release valve to Fixed Head Vessels discharge any internal pressure. For vessels First, lower the heater and push it on a movable floor cart, lift the vessel out of... - Page 11 Parr Instrument Company 4540 Pressure Reactors the flow control valve on the gas tank closed, HOW TO USE THE VESSEL open the main valve on the gas tank only Continued about one-quarter turn; then use the flow control valve or the valve on a pressure...
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Page 12: Accessories
Always close the inlet valve before assembly to Parr Instrument Company. withdrawing a liquid sample and open the A single loop cooling coil is installed in sampling valve cautiously because liquid will the bomb with compression fittings on the be discharged with considerable force. -
Page 13: Air Motor
Parr Instrument Company 4540 Pressure Reactors ACCESSORIES Continued Air Motor Variable Speed Electric Motor Variable stirring speeds from 100 to Reactors are normally equipped with a 2000 rpm with no spark hazard can be DC variable speed motor supplied and obtained by replacing the standard motor controlled through the Series 4840 controller. -
Page 14: Explosion Proof Operation
Parr Instrument Company for further for use in Class 1, Groups C & D, and discussion and suggestions which might Class 2, Groups E, F, & G atmospheres. -
Page 15: Periodic Pressure Tests
Apparatus returned for testing particularly whenever the user suspects that and overhaul should be shipped prepaid to the equipment has been over-stressed or the Parr Instrument Company, 211-53 damaged. Street, Moline, Illinois 61265. An order or Some laboratories maintain hydraulic... -
Page 16: General Maintenance Notes
6. Do not use oil or anti-seize lubricant on 11. If servicing assistance is needed, threads or fittings if the vessel is to be contact Parr Instrument Company directly used with oxygen. at the address shown on the back of 7. -
Page 17: Parts Lists
Parr Instrument Company 4540 Pressure Reactors PARTS LISTS * For parts made from alternate materials use the codes shown below as a suffix to the standard Reaction Vessel Parts List part number. Consult the itemized list for your reactor CM -... - Page 18 Parr Instrument Company 4540 Pressure Reactors Split Rings and Accessories Gages A2305HC Split Ring Assembly 2304HC Compression Ring, Head 56HCPF Pressure gage, 4-1/2”, 0-2000 psi A2313HC Drop Band 56HCPG Pressure gage, 4-1/2”, 0-3000 psi A2315HC Split Ring Assembly 56HCPH Pressure gage, 4-1/2”, 0-5000 psi...
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Page 19: Overarm Parts List
Parr Instrument Company 4540 Pressure Reactors Drive Pulleys (Motor) Overarm Parts List 857HC Pulley 600 RPM 857HC3 Pulley 800 RPM Motor 857HC4 Pulley 1000 RPM 857HC5 Pulley 1700 RPM 1355EES Motor, VS/PM 130VDC 1/8HP 695HC5 Pulley 800 RPM .62 A1554EES... - Page 20 Parr Instrument Company 4540 Pressure Reactors Release Knob Tach Sensor Upper Drive Shaft Belt Assembly Drive Pulley Overarm Optical Wheel Plate Driven Pulley Collar Coupling Motor - 20 -...
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Page 21: Cooling Coil Parts List
Parr Instrument Company 4540 Pressure Reactors Cooling Loop Fittings Cooling Coil Parts List 511HC Elbow, Tube Connector, ¼” T 122HW Ferrule for 511HC Cooling Loops* 123HW Cap Nut for 511HC A138CA Male Connector 2306HC Cooling Loop, 600 mL 217VB Nut for A138CA ¼T... -
Page 22: Vessel Heater Parts List
Parr Instrument Company 4540 Pressure Reactors Vessel Heaters Parts List For Cart-mounted Vessels For Bench Top and Floor Stand Vessels A2256HC10EB Heater Assembly, 1000W A735HC3EB Heater Assembly, 1000W 115V, 600 mL 115V, for use with 600 mL A2256HC10EE Heater Assembly, 1000W... -
Page 23: Diagrams
Parr Instrument Company 4540 Pressure Reactors DIAGRAMS Diagram of Overarm for: 4544A, 4545A, 4546A & 4547A - 23 -... - Page 24 Parr Instrument Company 4540 Pressure Reactors Diagram of Overarm for: 4544A, 4545A, 4546A & 4547A - 24 -...
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- Page 35 PARR INSTRUMENT COMPANY 211 Fifty-Third Street Moline, Illinois 61265 USA 309/762-7716 800/872-7720 Fax 309/762-9453 • E-Mail: http://www.parrinst.com parr@parrinst.com Revision 02/21/08...
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