Venting with flame and particle retention (25 pages)
Summary of Contents for Fike PROINERT 2
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FILL AND PACKAGING PROCEDURES For Inert Gas Suppression System Cylinders With IG‐55, IG‐100, and IG‐541 Agents 200 and 300 Bar Underwriters Laboratories (UL) and Underwriters Laboratories Canada (ULC) Listed Factory Mutual (FM) Approved National Fire Protection Assoc. (NFPA) 2001 Standard Applied Rev. 11 / March 2020 P/N 06‐312 SOLUTIONS Fire Protection Explosion Protection Overpressure Protection Pressure Activation ...
1.0 INTRODUCTION 1.1 Scope This section of the manual contains the minimum requirements and procedures for filling and packaging PROINERT® inert gas suppression containers. The information contained herein is prepared for the use and guidance of Fike‐ authorized sales outlets and will be strictly followed to ensure the PROINERT container functions properly throughout its life. 1.2 Purpose This manual is intended to provide Fike‐approved filling stations with the information necessary to properly and safely charge a PROINERT container for service. 1.3 Safety Precautions An understanding of the physical properties of inert gas clean agents (gas mixtures of argon, nitrogen, and carbon dioxide), and the safe and proper use of techniques for handling high‐pressure compressed gases, will allow safe recharge of PROINERT containers. Prior to handling inert gas clean agents and the PROINERT container, all supplementary manuals, relevant Safety Data Sheets (SDSs), and the safety precautions listed below must be read and understood by all individuals handling the product. WARNING Containers associated with this procedure will be filled with a non‐liquefiable gas under high pressure. Safe handling procedures associated with pressurized containers must be observed at all times. CAUTION Suitable pressure relief devices will be incorporated into the charging system to prevent accidental over pressurization of the system. In pipe sections where high pressure inert gas could become trapped, suitable pressure relief devices will be provided. CAUTION PROINERT filling areas must be well ventilated at all times. CAUTION Safety glasses and gloves will be worn at all times when handling high‐pressure inert gas. CAUTION Before filling, all containers will be inspected for evidence of weak or corroded areas and the date of the last hydrostatic test or inspection will be noted on the container. See Section 3.1 for testing details. CAUTION The shipping/safety cap will be installed on the cylinder at all times except during the filling process. 2.0 EQUIPMENT The following equipment is required for the proper filling of PROINERT containers from bulk storage containers: ...
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Item 6: Valve Filling Adaptor (P/N IG71‐064) – Adaptor required to keep the valve in the “open” position during the filling operation. Item 7: Fill Adaptor (FasTest® METHP0198A or equivalent) – Adaptor required to connect the fill hose to a PROINERT container valve. Item 8: Fittings, Valves, and Hoses, as Required – Components essential to the functionality of PROINERT cylinders. Must have a minimum working pressure of 6,000 psi (415 bar). Item 9: Thermometer or Thermocouple – Instruments used to measure temperature. Must be accurate to ±2.0F (±1.0C) and located in the PROINERT filling area. Item 10: Pressure Gauge Assembly (P/N IG71‐125) – Assembly that includes a 0‐5,000 psi (0‐345 bar) pressure gauge with an accuracy of 0.1% of full scale reading, calibrated in 5 psi (.4 bar) increments or less, with all the fittings, adapters, and O‐rings attached to properly connect to the container. Item 11: Pressure vs. Temperature Chart – Chart detailing the relationships of IG‐55, IG‐100, and IG‐541 pressure vs. temperature. See Appendix A.2 for information. Item 12: Valve Lockout Tool (P/N IG71‐235) – Tool required to mechanically lock the valve in the “closed” position to prevent a discharge when removing the fill hose and installing the discharge port recoil cap. Item 13: Log Book – Permanent record containing the following information (see Appendix A.3 for example): o Date filled o Customer o Valve Lot Number o Container Serial Number o Initial fill or recharge o Container pressure o Leak test results o Name/initials of person performing the initial fill/recharge procedure ...
2.1 Equipment Calibration A program will be established by the Fike‐authorized filling station to assure that testing and measuring equipment used in the production and/or inspection process is kept clean, maintained in good working order, and is within calibration. The following calibration frequencies will be adhered to at minimum: Frequency Calibration Schedule Once every Once every 6 months 12 months Scales X Pressure gauges X Leak standards X Thermometers X Thermocouples X Wrenches X Equipment When subjected to abuse, such as being dropped or struck with an object, or when its accuracy is questionable. Calibration may be performed by the sales outlet or an outside laboratory. Calibration will be by comparison with a ...
3.0 CONTAINER AND VALVE PREPARATION 3.1 Test and Inspection PROINERT inert gas containers will not be filled without re‐testing if more than 10 years have elapsed since the date of the last test and inspection. WARNING: PROINERT container contents are under high pressure. Never attempt to fill the container until the contents have been discharged and the pressure gauge reads 0. CAUTION: Care should be taken when handling valve components to avoid damage of any kind. 3.2 Valve Installation Procedure The procedure detailed below describes the steps necessary to install a new valve to a cylinder: Visually inspect cylinder threads and chase any burrs or debris using a 1" NGT tap. Vacuum all cylinders prior to valve installation to remove any debris. Prepare the PROINERT valve with three wraps of ¾" wide, high‐density PTFE thread seal tape onto the 1" NGT male thread. Wrap the threads with tape clockwise when viewed from the valve inlet. Compress the tape against the threads securely by hand. Using a brush, apply Gasoila SS‐16 Soft‐Set thread sealant onto the taped portion of thread. Apply enough thread sealant to cover the first 2‐3 threads of the valve (Figure 3.2‐1). Thread the valve into the cylinder hand‐tight and then tighten to a torque of 166 to 207 lbf‐ft (225 to 280 N‐m). Figure 3.2‐1 Gas Sealant on Threads NOTE: Install the valve on the cylinder immediately after the Gasoila thread sealant is applied onto the PTFE tape to prevent the Gasoila thread sealant from setting prior to the valve being installed on the cylinder. Check for proper valve installation with the cylinder/valve engaugement gauge. Use the gauge to check the gap between the cylinder neck boss and the shoulder above the 1" NGT thread (Figure 3.2‐2). o Valve is properly installed if the “max/no‐go” side of the gauge cannot fit in the gap AND the “min/go” can. o Valve is improperly installed if the “max/no‐go” side of the gauge can fit in the gap OR the “min/go” cannot. The container is now ready for filling. ...
(bar @ 15°C) (psi @ 59°F) IG71‐103‐200‐55 80 PROINERT IG71‐103‐300‐100 200 2,900 IG71‐103‐200‐541 IG71‐103‐300‐55 80 PROINERT IG71‐103‐300‐100 300 4,351 IG71‐103‐300‐541 The following is a step‐by‐step procedure suggested by Fike Corporation for the filling of PROINERT containers. Refer to Appendix A.2 for the pressure vs. temperatures chart for the various inert gases being filled. NOTE: Containers and valves to be recharged must be reconditioned in accordance with Section 3.0 of this manual. CAUTION: Suitable precautions, such as wearing safety glasses and gloves, must be taken. For additional information, refer to CGA P‐1 Safe Handling of Compressed Gases in Containers. CAUTION: The marking on the valve must read “WP 300 BAR”, while the marking on the container must indicate a minimum allowable service pressure of 300 bar (4,351 psi). CAUTION: Prior to filling, verify that the container has no residual pressure by installing a pressure gauge into the gauge port. CAUTION: The maximum fill pressure must not exceed 5,308 psi (366 bar) at a temperature of 122°F (50°C) for PROINERT IG71‐103‐XXX‐XXX containers. CAUTION: Filling gases at high pressure causes the container temperature to rise. DO NOT exceed a container temperature of 122°F (50°C) during the filling process. CAUTION: Do not leave container unattended while filling. ...
4.1 Container Valve Preparation There are two methods available for filling the containers, either by pressure or by weight. The preferred method is to fill by weight, as this is more accurate and not temperature‐dependent. Detailed below are the steps necessary to prepare the container valve assembly for filling: Connect the fill adaptor (FasTest® METHP0198A or equivalent) to the valve outlet port (valve outlet is a G ⅝" male thread and the fill adaptor is a G ⅝" female thread with a swivel adaptor on one end and 3/8" NPT on the other end). The fill adapter should be connected to the fill manifold via the 3/8" NPT port. 3/8" NPT Male Thread (for fill hose connection) G 5/8" Female Swivel (for G 5/8" male discharge port) Figure 4.1‐1 Fill Adapter Connections Connect the filling hose to the fill adapter. Step 3: Assemble the valve filling tool to the spring washer on top of the valve (see Figure 4.1‐2). Ensure both screws on the bottom half of the filling tool sit flat on top of the valve body. Secure the top cap onto the base assembly with the ¼‐20 UNC cap screw. Ensure the top cap is fully engaged, with the cap screw head resting firmly against the top thrust washer and the bottom thrust washer resting firmly against the top cap. ¼‐20 UNC Cap Screw (1) Needle‐Roller Thrust Bearing Top Cap Assembled Container (2) M6x1 Cap Screws Base Assembly Figure 4.1‐2 Valve Filling Components PAGE / 6 Doc. P/N 06‐312 Rev. 11 / March 2020 ...
4.2 Fill by Weight IG‐55 (50% Argon and 50% Nitrogen Mixture) IG‐55 inert gas mixture consists of 50±5% nitrogen and 50±5% argon. Detailed below are the steps necessary to fill the PROINERT container assembly with IG‐55. Connect to the valve outlet and pull 25" to 27" of the vacuum to remove residual atmosphere and moisture. Fill the container via the valve inlet with argon and then nitrogen per the table below for the system pressure required: Size Argon Nitrogen Resultant IG‐55 System Pressure System Pressure (Liters) (kg) (kg) (kg) (bar @ 15°C) (psi @ 59°F) 80 12.87 – 13.43 9.43 – 9.79 22.66 – 22.87 200 2,900 80 18.91 – 19.73 13.23 – 13.73 32.64 – 32.96 300 4,350 NOTE: Perform a preliminary leak check at the neck of the cylinder with a soap solution (SwageLok Snoop or its equivalent) once it has been filled with argon. If a leak is detected, discontinue the fill for that particular cylinder. Verify the container by ensuring the final fill pressure is as detailed above at 59°F (15°C). If required, refer to the pressure vs. temperature chart for IG‐55 in Appendix A.2. Close the valve by unscrewing the central screw on the filling adaptor and removing the top half of the ...
IG‐100 (100% Nitrogen) The IG‐100 inert gas consists of 100% nitrogen. Detailed below are the steps necessary to fill the PROINERT container with IG‐100 by pressure: Connect the valve outlet and pull 25" to 27" of the vacuum to remove residual atmosphere and moisture. Fill the container with nitrogen via the valve inlet, as detailed in the table below: Size (Liters) Fill Weight Units Final Pressure @ 59°F (15°C) 80 2,900 psi (200 bar) 18.34 kg 80 4,350 psi (300 bar) 24.97 kg NOTE: Perform a preliminary leak check at the cylinder’s neck with a soap solution (SwageLok Snoop or its equivalent) once it has been filled halfway. If a leak is detected, discontinue the fill for that particular cylinder. Verify the gases by ensuring that the final fill pressure is as detailed above at 59°F (15°C). If required, refer to the pressure vs. temperature chart for IG‐100 in Appendix A.2. Close the valve by unscrewing the central screw on the filling adaptor and remove the top half of the adaptor. Notice the dowel on the internal piece of the filling adaptor move downwards during this operation. Proceed with removing the bottom half of the filling adaptor by unscrewing the two M6 set screws. Remove this adaptor from the valve and check that the spring washer has dropped lower than its original depth. Vent the filling hose and check that there is no flow from the valve outlet. Fit the Valve Lockout Assembly (P/N IG71‐235; Figure 4.2.2‐1) onto the valve prior to removing the filling hose. Remove the filling hose and screw the recoil cap on to the discharge outlet. Remove the valve lockout assembly from the valve after the recoil cap has been fitted. Check the container pressure (Section 6). Once testing is complete, screw the shipping/safety cap onto the cylinder. Valve Lockout Figure 4.2.2‐1 IG‐100 Container with Valve Lockout Assembly Installed PAGE / 8 ...
IG‐541 (52% Nitrogen, 40% Argon, and 8% Carbon Dioxide Mixture) The IG‐541 inert gas mixture consists nominally of 52% nitrogen, 40% argon, and 8% carbon dioxide. The mixture specification is nitrogen 52 ±4%, argon 40 ±4%, carbon dioxide 8 +1% / ‐0%. Detailed below are the steps necessary to fill the PROINERT container with IG‐541. Connect to the valve outlet and pull 25" to 27" of vacuum to remove residual atmosphere and moisture. Fill the container via the valve inlet with the individual gases in the following order: Carbon dioxide, then argon, and then nitrogen, as detailed in the table below for the system pressure required: Carbon Resultant Final Fill Size Argon Nitrogen Final Fill Pressure Dioxide IG‐541 Pressure (Liters) (kg) (kg) @ 59°F (psi) (kg) (kg) @ 15°C (bar) 80 2.47 – 2.49 10.76 – 11.66 9.81 – 10.63 23.04 – 24.78 200 2,900 80 3.50 – 3.54 14.82 – 16.06 13.49 – 14.61 31.81 – 34.21 300 4,350 NOTE: ...
4.3 Fill by Pressure IG‐55 (50% Argon and 50% Nitrogen Mixture) The IG‐55 inert gas mixture consists nominally of 50% argon and 50% nitrogen. The mixture specification is argon 50±5% nitrogen 50±5%. Detailed below are steps necessary to fill the PROINERT container with IG‐55 by pressure: Connect to the valve outlet and pull 25" to 27" of the vacuum to remove residual atmosphere and moisture. Fill the container via the valve inlet with argon to the pressure indicated in the table below for the system pressure required. Top off the container with nitrogen to the final fill pressure per the table below. If necessary, refer to the pressure vs. temperature chart for IG‐55 in Appendix A.2. Final Pressure @ 59°F (15°C) Size (Liters) Argon Pressure @ 59°F (15°C) (Top up with Nitrogen) 80 1,450 to 1,670 psi (100 to 111.5 bar) 2,900 psi (200 bar) 80 2,045 to 2,263 psi (141 to 156 bar) 4,350 psi (300 bar) NOTE: Perform a preliminary leak check at the cylinder neck with a soap solution (SwageLok Snoop or its equivalent) once it has been filled with argon. If a leak is detected, discontinue filling the cylinder. Verify the container by ensuring the final fill pressure is as detailed above at 59°F (15°C). If required, refer to the pressure vs. temperature chart for IG‐55 in Appendix A.2. Close the valve by unscrewing the central screw on the filling adaptor and removing the top half of the adaptor. The dowel on the internal piece of the filling adaptor should move downward during this operation. Proceed with removal of the bottom half of the filling adaptor by unscrewing the two M6 cap screws. Remove this adaptor from the valve and check that the spring washer has dropped lower than its original depth. Vent the filling hose and check that there is no flow from the valve outlet. Fit the valve lockout assembly onto the valve (Figure 4.3.1.‐1) prior to removing the filling hose. Remove the filling hose and screw the recoil cap on to the discharge outlet. Remove the valve lockout assembly from the valve after the recoil cap has been fitted. Proceed to leak checking (Section 5). Check container pressure (Section 6). Once testing is complete, screw the Valve Lockout shipping/safety cap onto the cylinder. ...
IG‐100 (100% Nitrogen) The IG‐100 inert gas consists of 100% nitrogen. Detailed below are the steps necessary to fill the PROINERT container with IG‐100 by pressure: Connect the valve outlet and pull 25" to 27" of the vacuum to remove residual atmosphere and moisture. Fill with nitrogen to the pressure indicated in the table below for system pressure required. If required, refer to the pressure vs. temperature chart for IG‐100 in Appendix A.2. Size (Liters) Final Pressure @ 59°F (15°C) 80 2,900 psi (200 bar) 80 4,350 psi (300 bar) NOTE: Perform a preliminary leak check at the cylinder’s neck with a soap solution (SwageLok Snoop or equivalent) once it has been filled halfway. If a leak is detected, discontinue the fill for that particular cylinder. Close the valve by unscrewing the central screw on the filling adaptor, then remove the top half of the adaptor. Notice the dowel on the internal piece of the filling adaptor move downwards during this operation. Proceed with removing the bottom half of the filling adaptor by unscrewing the two M6 set screws. Remove this adaptor from the valve and check that the spring washer has dropped lower than its original depth. Vent the filling hose and check that there is no flow from the valve outlet. Fit the valve lockout assembly onto the valve (Figure 4.3.2‐1) prior to removing the filling hose. Remove the filling hose and screw the recoil cap onto discharge outlet. Remove the valve lockout assembly from the valve after the recoil cap has been fitted. Check the container pressure (Section 6). Once testing is complete, screw the shipping/safety cap onto cylinder. Valve Lockout Figure 4.3.2‐1 IG‐100 Container with Valve Lockout Assembly Installed Doc. P/N 06‐312 ...
5.0 LEAK DETECTION After the container has been filled with the required quantity of agent, it must be carefully checked for leaks. All potential leak points on each container must be carefully inspected with an argon leak detector checked against a calibrated leak standard to the minimum leak rate of 1.26 x 10‐3 cc/sec. Be sure to pay particular attention to the valve recoil cap vent holes, the ports containing high‐pressure valve cores, and the valve NGT threads. Soap solutions (e.g., SwageLok Snoop or its equivalent) can be used in conjunction with the argon leak detector as a secondary leak detection method to help isolate leaks picked up the by the detector. NOTE: Valve must be dry prior to using the argon leak detector, since standing soap solution can cause a false positive reading on the argon leak detector. Containers with NO indication of leakage are acceptable for shipment and system use. Record container acceptance date, any comments or remarks, and the inspector’s initials in the fill station logbook. Containers with leaks will be inspected and repaired or rebuilt after they have been emptied safely via a pipe network that is terminated with a controlled orifice. 6.0 CONTAINER PRESSURE CHECK Once leak testing is complete, verify that container pressure is within the limits as detailed in the pressure vs. temperature chart for the appropriate agent in Appendix A.2. The container fill pressure will be within ±43 psi (3 bar) of the nominal fill pressure. 6.1 Procedure to Install Pressure Gauge Remove and retain the plug from the pressure gauge port. Prior to installing the pressure gauge, lubricate the O‐ring on the pressure gauge assembly with Molykote 55 or its equivalent. Use care not to get lubricant into the pressure gauge port (Figure 6.1‐1). IMPORTANT: DO NOT apply PTFE tape to the external threads on the pressure gauge assembly. Screw in the pressure gauge assembly by hand until resistance is felt and pressure registers on gauge. Use a wrench to screw in the pressure gauge assembly two additional turns, then check the pressure. CAUTION: DO NOT cross‐thread the pressure gauge assembly during installation. Remove the pressure gauge assembly and reinstall the plug in the pressure gauge port. WARNING: When removing the pressure gauge assembly from a pressurized PROINERT cylinder, a “pop” sound will be heard. This is normal and the result of a minor amount of gas being trapped in the pressure gauge port. Secure the shipping/safety cap to the cylinder. ...
7.0 CYLINDER IDENTIFICATION LABEL The fill station will update the cylinder identification label with the information shown below using a medium‐ or fine‐ point permanent black marker. Figure 7.0‐1 Sample Cylinder Identification Label 7.1 Label Placement Safety Cap Label Step 1. Clean the surface and apply the label approximately 45 left of the CE mark on the valve assembly. Step 2. Apply the safety cap label to the safety cap. NOTE: The cylinder ID label should be attached 47” (1194mm) from the bottom of the cylinder. Cylinder ID Label Step 3. Position the overlayment over the cylinder ID label so it covers the original fill date and the fill date and UL fill station code number. Overlayment Step 4. Apply the fill pressure and hazard class labels below the cylinder ID label as shown. Fill Pressure Hazard Class 47" (1194mm) ...
Wood pallet, heat‐treated per ISPM 15 Corrugated cardboard and nylon sleeves 2x4 lumber, heat‐treated per ISPM 15 8‐penny (8D) ring shank nails 3" drywall or wood screws 1.25"‐wide steel banding 2"‐wide ratchet strap DOT Class 2 label UN label OVERPACK label SDS with plastic pouch 8.2 Packaging Procedure Prior to palletizing PROINERT container assemblies, validate the strength and quality of the skid and wooden frame. All boards will be joined using a minimum of three equally spaced nails per joint. Palletize the PROINERT container assemblies per the configurations below or a Fike‐approved configuration (not shown). NOTE: One or two cylinder orders may be packaged AGENT UN LABEL individually without a pallet; however, 3+ UN 1956 cylinder orders cannot. COMPRESSED GAS IG‐55 N.O.S. One (1) DOT label, one (1) UN label, and one IG‐55 (NITROGEN, (1) OVERPACK label must be applied to the ...
APPENDIX A – Support Information This appendix contains details that are referred to throughout this manual. A.1 Safety Data Sheets A.1.1 PROINERT IG‐55 PROINERT IG‐55 SECTION 1: Identification of the substance/mixture and of the company/undertaking Product identifier PROINERT IG‐55 Use of the substance/preparation Fire extinguishing agent Company/undertaking identification Fike Corporation 704 SW 10th Street P.O. Box 610 Blue Springs Missouri 64013‐0610 USA Tel : +1 816 229 3405 SECTION 2: Hazards identification Classification of the substance or mixture Gases under pressure H280 : Contains gas under pressure; may explode if heated. Label elements Warning H280 : Contains gas under pressure; may explode if heated. ...
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SECTION 4: First aid measures General advice If person is unconscious, place in recovery position and seek medical advice. Never give anything by mouth to an unconscious person. If breathing is irregular or stopped, administer artificial respiration. If symptoms persist, call a physician. Inhalation May cause asphyxiation at high concentrations. Symptoms may include loss of mobility/consciousness. Victim may not be aware of asphyxiation. Remove victim to an uncontaminated area wearing self‐contained breathing apparatus. Keep person warm and at rest. Seek medical assistance. Apply artificial respiration if breathing has stopped. Skin/eye contact Compressed gas directed at the skin can enter the body through small wounds or even penetrate the skin, causing serious or fatal injuries. Seek medical advice immediately. Ingestion Ingestion is not considered a potential route of exposure. SECTION 5: Fire‐fighting measures Suitable extinguishing media All known extinguishants can be used. Specific methods If possible, stop the flow of product. Move the container away or cool with water from a protected position. Specific hazards during firefighting Pressure buildup Fire of intense heat may cause violent rupture of containers. No hazardous combustion products. Advice for fire fighters In confined spaces, use a self‐contained breathing apparatus. Use personal protective equipment. SECTION 6: Accidental release measures Personal precautions Evacuate personnel to safe areas. Ventilate area, especially low or enclosed places where the mixture might collect. Refer to protective measures listed in Sections 7 and 8. Environmental precautions Provided it is safe to do so, try to stop release. Prevent from entering sewers, basements, and work pits or any place where accumulation can be dangerous. Methods for cleaning up Ventilate area. ...
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Storage Do not drag, slide, or roll containers. Never attempt to lift cylinder by its cap. Use a check valve in the discharge line to prevent hazardous back flow into the container. Storage temperature Keep containers in a dry, cool, and well‐ventilated place at a temperature of between ‐20°C and 50°C. Containers should be stored in designated racks or secured to a rigid surface with straps or chains. SECTION 8: Exposure controls/personal protection Exposure limits No exposure limit specified, but atmosphere must have a minimum of 18% free oxygen. Exposure controls Ensure adequate ventilation, especially in confined areas. Eye protection ‐ Wear safety glasses complying with EN 166 or ANSI Z87.1 Hand protection – Wear leather gloves that are resistant to low temperature complying with EN 374 or US OSHA guidelines. The choice of the gloves also depends on other quality features other than material and is different from one manufacturer to another. Consideration must be given to specific local conditions, such as the danger of cuts, abrasion, and contact time with the substance. Skin and body protection – Wear suitable protective equipment. Protective measures – Required to wear a self‐contained breathing apparatus if a large release is experienced. Respiratory protection – For rescue, use a self‐contained breathing apparatus. The mixture is heavier than air and can cause suffocation by reducing the oxygen concentration available for breathing. Apparatus must comply with EN 137 or OSHA 29 CFR 1910.134. SECTION 9: Physical and chemical properties Physical and chemical properties Form : Colorless gas Odor : None Molecular weight : 33.95 Melting point ...
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SECTION 11: Toxicological information General No toxicological effects from this product. LC50/ih No acute toxicity. SECTION 12: Ecological information No ecological damage is caused by this product. Nitrogen and argon are natural components of air. Nitrogen constitutes approximately 78% and argon constitutes approximately 0.9% of the earth’s atmosphere. SECTION 13: Disposal considerations Dispose to atmosphere in a well‐ventilated area. Consider noise and pressure hazards. Do not discharge into any place where accumulation could be dangerous. Contact your Fike Corporation supplier if guidance is required or you are unsure of the best disposal method. SECTION 14: Transport information UN No. : 1956 Class : 2.2 Proper shipping name : Compressed gas, N.O.S. ADR/RID Item No.1 : 2.1a Other transport information : Avoid transport on vehicles where the load space is not separated from the driver’s compartment. Ensure vehicle driver is aware of the potential hazards of the load and knows what to do in an emergency. Before transporting product containers ensure: Cylinder valve is closed and not leaking. Valve outlet recoil cap, actuation port blanking plug and, shipping/safety cap is correctly fitted. Adequate ventilation. Compliance with applicable regulations.
A.1.2 PROINERT IG‐100 PROINERT IG‐100 SECTION 1: Identification of the substance/mixture and of the company/undertaking Product identifier PROINERT IG‐100 Use of the substance/preparation Fire extinguishing agent Company/undertaking identification Fike Corporation 704 SW 10th Street P.O. Box 610 Blue Springs Missouri 64013‐0610 USA Tel : +1 816 229 3405 SECTION 2: Hazards identification Classification of the substance or mixture Gases under pressure H280 : Contains gas under pressure; may explode if heated. Label elements Warning H280 : Contains gas under pressure; may explode if heated. P410 + P403 : Protect from sunlight. Store in a well‐ventilated place. Other Hazards The gas can cause suffocation by reducing oxygen available for breathing. SECTION 3: Composition/information on ingredients 100% nitrogen. ...
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SECTION 4: First aid measures General advice If person is unconscious, place in recovery position and seek medical advice. Never give anything by mouth to an unconscious person. If breathing is irregular or stopped, administer artificial respiration. If symptoms persist, call a physician. Inhalation May cause asphyxiation at high concentrations. Symptoms may include loss of mobility/consciousness. Victim may not be aware of asphyxiation. Remove victim to an uncontaminated area, wearing self‐contained breathing apparatus. Keep person warm and at rest. Seek medical assistance. Apply artificial respiration if breathing has stopped. Skin/eye contact Compressed gas directed at the skin can enter the body through small wounds or even penetrate the skin, causing serious or fatal injuries. Seek medical advice immediately. Ingestion Ingestion is not considered a potential route of exposure. SECTION 5: Fire‐fighting measures Suitable extinguishing media All known extinguishants can be used. Specific methods If possible, stop flow of product. Move container away or cool with water from a protected position. Specific hazards during firefighting Pressure buildup Fire of intense heat may cause violent rupture of containers. No hazardous combustion products. Advice for fire fighters In confined spaces use self‐contained breathing apparatus. Use personal protective equipment. SECTION 6: Accidental release measures Personal precautions Evacuate personnel to safe areas. Ventilate area, especially low or enclosed places where the mixture might collect. Refer to protective measures listed in sections 7 and 8. Environmental precautions Provided it is safe to do so, try to stop release. Prevent from entering sewers, basements and work pits or any place where accumulation can be dangerous. Methods for cleaning up Ventilate area. Disposal Refer to section 13 for disposal instructions. PAGE / A‐6 ...
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SECTION 7: Handling and storage Handling Substance is heavier than air and may spread along floors. Compressed gas cylinders are heavy and contain considerable stored energy. Use suitable equipment and handle with appropriate caution. Contact supplier if in doubt. Storage Do not drag, slide or roll containers. Never attempt to lift cylinder by its cap. Use a check valve in the discharge line to . prevent hazardous back flow into the container Storage temperature Keep containers in a dry, cool, and well‐ventilated place at a temperature of between ‐20°C and 50°C. SECTION 8: Exposure controls/personal protection Exposure limits No exposure limit specified, but the atmosphere must have a minimum of 18% free oxygen. Exposure controls Ventilation ‐ Ensure adequate ventilation, especially in confined areas. Eye protection ‐ Wear safety glasses complying with EN 166 or ANSI Z87.1 Hand protection – Wear leather gloves that are resistant to low temperature complying with EN 374 or US OSHA guidelines. The choice of the gloves also depends on other quality features other than material and is different from one manufacturer to another. Consideration must be given to specific local conditions, such as the danger of cuts, abrasion, and contact time with the substance. Skin and body protection – Wear suitable protective equipment. Protective measures – Wear a self‐contained breathing apparatus if a large release is experienced (required!). Respiratory protection – Use a self‐contained breathing apparatus for rescue. The gas can cause suffocation by reducing the oxygen concentration available for breathing. Apparatus must comply with EN 137. SECTION 9: Physical and chemical properties Physical and chemical properties Form ...
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No acute toxicity SECTION 12: Ecological information No ecological damage is caused by this product. Nitrogen is a natural component of air, constituting approximately 78% of the earth’s atmosphere. SECTION 13: Disposal considerations This product must be discharged to the atmosphere in a well‐ventilated area. Consider noise and pressure hazards when discharging this product. Do not discharge into any place where product accumulation could be dangerous. Contact your Fike Corporation supplier if guidance is required or if you are unsure of the best disposal method. SECTION 14: Transport information UN No. : 1066 Class : 2 Proper shipping name : Nitrogen, compressed. ...
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SECTION 16: Other information Refer to Section 3. H280 Contains gas under pressure; may explode if heated. The hazard of asphyxiation is often overlooked and must be stressed during operator training. Before using this product in any new processes or experiment, a thorough material compatibility and safety study should be carried out. The information provided in this document is correct at the date of publication. The information is designed only as a guide for safe handling, use, storage, transportation, disposal and release and is not to be considered as a warranty or quality specification. While great care has been taken in the preparation of this information, no liability for injury, damage or non‐compliance with any legislation or directive arising from its use can be accepted. This document does not constitute or substitute for the user’s own assessment of workplace risk as required by other health and safety legislation. PAGE / A‐9 Doc. P/N 06‐312 Rev. 11 / March 2020 ...
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A.1.3 PROINERT IG‐541 PROINERT IG‐541 SECTION 1: Identification of the substance/mixture and of the company/undertaking Product identifier PROINERT IG‐541 Use of the substance/preparation Fire extinguishing agent Company/undertaking identification Fike Corporation 704 SW 10th Street P.O. Box 610 Blue Springs Missouri 64013‐0610 USA Tel : +1‐816‐229‐3405 SECTION 2: Hazards identification Classification of the substance or mixture Gases under pressure H280 : Contains gas under pressure; may explode if heated. Label elements Warning ...
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SECTION 4: First aid measures General advice If person is unconscious, place in recovery position and seek medical advice. Never give anything by mouth to an unconscious person. If breathing is irregular or stopped, administer artificial respiration. If symptoms persist, call a physician. Inhalation May cause asphyxiation at high concentrations. Symptoms may include loss of mobility/consciousness. Victim may not be aware of asphyxiation. Remove victim to an uncontaminated area, wearing self‐contained breathing apparatus. Keep person warm and at rest. Seek medical assistance. Apply artificial respiration if breathing has stopped. Skin/eye contact Compressed gas directed at the skin can enter the body through small wounds or even penetrate the skin, causing serious or fatal injuries. Seek medical advice immediately. Ingestion Ingestion is not considered a potential route of exposure. SECTION 5: Fire‐fighting measures Suitable extinguishing media All known extinguishants can be used. Specific methods If possible stop flow of product. Move container away or cool with water from a protected position. Specific hazards during firefighting Pressure buildup Fire of intense heat may cause violent rupture of containers. No hazardous combustion products. Advice for fire fighters In confined spaces use self‐contained breathing apparatus. Use personal protective equipment. SECTION 6: Accidental release measures Personal precautions Evacuate personnel to safe areas. Ventilate area, especially low or enclosed places where the mixture might collect. Refer to protective measures listed in sections 7 and 8. Environmental precautions Provided it is safe to do so, try to stop release. Prevent from entering sewers, basements and work pits or any place where accumulation can be dangerous. Methods for cleaning up Ventilate area. Disposal Refer to section 13 for disposal instructions. PAGE / A‐11 Doc. P/N 06‐312 ...
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SECTION 7: Handling and storage Handling Substance is heavier than air and may spread along floors. Compressed gas cylinders are heavy and contain considerable stored energy. Use suitable equipment and handle with appropriate caution. Contact supplier if in doubt. Storage Do not drag, slide or roll containers. Never attempt to lift cylinder by its cap. Use a check valve in the discharge line to . prevent hazardous back flow into the container Storage temperature Keep containers in a dry, cool and well ventilated place at a temperature of between ‐20°C and 50°C. SECTION 8: Exposure controls/personal protection Exposure limits No exposure limit specified, but atmosphere must have a minimum of 18% free oxygen. Exposure controls Ensure adequate ventilation, especially in confined areas. Eye protection ‐ wear safety glasses complying with EN 166 or ANSI Z87.1 Hand protection ‐ Leather gloves that are resistant to low temperature complying with EN 374 or US OSHA guidelines. The choice of the gloves also depends on other quality features other than material and is different from one manufacturer to another. Consideration must be given to specific local conditions such as the danger of cuts, abrasion and contact time with the substance. Skin and body protection – Wear suitable protective equipment. Protective measures – Self‐contained breathing apparatus is required if a large release is experienced. Respiratory protection – For rescue use self‐contained breathing apparatus. The mixture is heavier than air and can cause suffocation by reducing the oxygen concentration available for breathing. Apparatus must comply with EN 137. SECTION 9: Physical and chemical properties Physical and Chemical Properties Form : Colorless gas Odor ...
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SECTION 11: Toxicological information General No toxicological effects from this product. Acute toxicity No acute toxicity. SECTION 12: Ecological information No ecological damage is caused by this product. Nitrogen, Argon and Carbon dioxide are natural components of air. Nitrogen constituting approximately 78%, Argon approximately 0.9% and Carbon dioxide 0.03% of the earth’s atmosphere. SECTION 13: Disposal considerations To atmosphere in a well‐ventilated area. Consider noise and pressure hazards. Do not discharge into any place where its accumulation could be dangerous. Contact your Fike Corporation supplier if guidance is required or you are unsure of the best disposal method. SECTION 14: Transport information UN No. : 1956 Class : 2 Proper shipping name : Compressed gas, N.O.S. ADR/RID Item No.1 : 2.1a Other transport information : Avoid transport on vehicles where the load space is not separated from the driver’s compartment. Ensure vehicle driver is aware of the potential hazards of the load and knows what to do in an emergency. Before transporting product containers ensure: Cylinder valve is closed and not leaking. Valve outlet cap is correctly fitted. Adequate ventilation. ...
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SECTION 16: Other information Refer to Section 3. H280 Contains gas under pressure; may explode if heated. The hazard of asphyxiation is often overlooked and must be stressed during operator training. Before using this product in any new processes or experiment, a thorough material compatibility and safety study should be carried out. The information provided in this document is correct at the date of publication. The information is designed only as a guide for safe handling, use, storage, transportation, disposal and release and is not to be considered as a warranty or quality specification. While great care has been taken in the preparation of this information, no liability for injury, damage or non‐compliance with any legislation or directive arising from its use can be accepted. This sheet does not constitute or substitute for the user’s own assessment of workplace risk as required by other health and safety legislation. PAGE / A‐14 Doc. P/N 06‐312 Rev. 11 / March 2020 ...
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A.2 Pressure/Temperature Chart for Containers Based on Fill at 59°F (15°C) A.2.1 PROINERT IG‐55 (50% Argon and 50% Nitrogen mixture) ProInert™ Containers Pressure Fill Method Developed Pressure Chart - Initial Fill with Argon ProInert™ 300 Bar - Argon Initial Fill ProInert™ 200 Bar - Argon Initial Fill Temperature (°C) 2600 2500 2400 2300 2200 2100 2000 1900 1800 1700...
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ProInert™ Containers Pressure Fill Method Developed Pressure Chart - Initial Fill with Nitrogen Temperature (°C) 2700 2600 2500 2400 2300 2200 2100 2000 1900 1800 1700 1600 1500 1400 1300 Temperature (°F) PAGE / A‐16 Doc. P/N 06‐312 Rev. 11 / March 2020 ...
Appendix B – PROINERT Valve Best Practices This appendix is intended to serve as a best practices guide for addressing problems related to the PROINERT Valve. B.1 Reporting Valve Failures After each fill session, valves failing to perform as intended should be reported back to Fike Corporation. A PROINERT Valve Failure Report (See Appendix B.4) should be filled out by the person performing the initial fill/recharge operation. The report should be emailed to proinertvalve@fike.com. B.2 Addressing Valve Neck Leaks If a valve is leaking from the neck, remove the valve from the cylinder and attempt to do the following: Clean valve threads by removing the remainder of Teflon tape and thread sealant. Make sure any hanging burrs or brass material from the threads is removed. Tape the valve and apply thread sealant as indicated in Section 3.2. Torque the valve into a cylinder. Go past the original thread depth provided it is within the min/max gauge limits. Fill the cylinder as per instructions provided in this manual. Return the valve to Fike Corporation if it leaks even after following the above mentioned procedure. B.3 Inspecting Incoming Cylinders A receiving inspection of incoming cylinders should be performed and documented using the following set of NGT plug gauges (B.3.1): L‐1 Gauge L‐9 Gauge Crest Check Gauge It is recommended that a random sample of 13 cylinders be inspected from each lot received for NGT specification conformance. A PROINERT Cylinder Inspection Report (See Appendix B.5) should be filled out by the person performing the inspection. The report should be emailed to proinertvalve@fike.com. B.3.1 NGT Plug Gauges Doc. P/N 06‐312 ...
B.4 PROINERT Valve Failure Report Form PROINERT Valve Failure Report Fill Date Total Valves Filled Fill Site Report Submitted By Failure Mode Indicators: Note: Valves that fail to close should be indicated by using the letter “J.” “A” through “I” indicate leak positions. # Cylinder Serial No. Valve Lot No. Failure Mode Fill Date 1 2 3 4 ...
B.5 PROINERT Cylinder Inspection Report Form PROINERT Cylinder Inspection Report Date Cylinder Manufacturer Fill Site Report Submitted By # Cylinder Serial No. L‐1 Gauge L‐9 Gauge Crest Check 1 2 3 4 5 ...
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REVISION HISTORY EVISION ESCRIPTION OF HANGE EVISION D .............................. J 2004 EVISION 1) Changed Valve Filling Adaptor p/n from 90032908 to p/n IG71‐064 in Section 2 Item 5 on page 4 and in Step 3 on page 8. 2) Changed p/n from IG71‐0151 to IG71‐0152 on page 8. 3) Formatting changes. E .............................. J 2011 EVISION 1) Updated Section 2 Equipment. 2) Updated Figures 2, 3, 4 & 5 6 .............................. J 2013 EVISION ANUARY 1) Replaced existing equipment list in 2.0 Equipment Section with information from Manual 06‐377. 2) Updated the Figures 2, 3, 4, 5 ...
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7) Updated nameplate in 7.0 Cylinder Identification 8) Added Safety Data Sheet and IG‐541 Pressure vs Temperature chart to Appendix A 10 .............................. M 2016 EVISION 1) Added “or Thermocouple” to Item 9 and paragraph 2.1 on page 2 2) Added Ambient Shop Temperature column to Sample Lob Book in A.3 on page 28 11 ............................... M 2020 EVISION ARCH 1) Replaced current Section A.1.2 with PROINERT IG‐100 Safety Data Sheet. 2) Renumbered former A.1.2 to A.1.3 for IG‐541. 3) Replaced current A.2.2 with IG‐100 Pressure/Temperature Chart. 4) Renumbered former A.2.2 to A.2.3 for IG‐541. 5) Inserted regulatory information in Appendix A, Section 15, for consistency. 6) Updated overall document to current Fike standard template. 7) Updated TOC, List of Figures, and List of Appendices. 8) Grammar, spelling, and/or punctuation as needed. 9) Modified text and figures to align with P/N 06‐806. Doc. P/N 06‐312 PAGE / B‐3 Rev. 11 / March 2020 ...
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B E C A U S E S O M U C H I S A T S T A K E ® CONTACT US Fike World Headquarters 704 SW 10 Street Blue Springs, Missouri 64015 USA Tel: +001 816‐229‐3405 Toll Free (US Only): 1‐800‐YES‐FIKE (1‐800‐937‐3453) www.Fike.com ...
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