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Summary of Contents for Linseis Chip-DSC 10
- Page 1 How To Low temperature measurements Chip-DSC with Linseis Messgeräte GmbH Gerlach Stand: 26.08.2021...
- Page 2 How To Low temperature measurements Index General information ................................3 2. Preparation of the Chip-DSC 10 System .......................... 3 2.1 Peltier system ................................. 3 2.2 QuenchCooling system .............................. 3 3. Preparation of the Chip-DSC 100 System ........................4 3.1 Peltier system ................................. 4 3.2 Intracooler System ...............................
- Page 3 T up to 30 K below ambient temperature is possible Δ place the cooling block on the ready to use Chip-DSC 10 tighten the screws at the blue main plate connect the Peltier cooler with power supply and turn on the cooling device 2.2 QuenchCooling system...
- Page 4 How To Low temperature measurements 3. Preparation of the Chip-DSC 100 System 3.1 Peltier system Affordable and easy to use cooling option for investigations near room temperature T up to 30 K below ambient temperature is possible Δ The system is already installed and can be turned on by the switch at the side of your Chip- DSC 100 3.2 Intracooler System Closed system and easy to use cooling option for investigations at lower temperatures...
- Page 5 How To Low temperature measurements 3.3 manual LN2 system Liquid nitrogen powered and manual cooling option for investigations at lowest temperatures investigations from -150 °C are possible open the cap of your Quench cooling reservoir Fill the reservoir with liquid nitrogen until you reach the required temperature To avoid evaporated liquid nitrogen in your lab it is possible to connect an additional tube at the outlet of your cooling option...
- Page 6 How To Low temperature measurements 3.4 Automatic LN2 system Liquid nitrogen powered and automatic cooling option for investigations at lowest temperatures investigations from -150 °C are possible adjust the level of the temperature sensor in your liquid nitrogen reservoir Connect the tube of your Dewar bottle with the inlet of your Chip-DSC 100 To avoid evaporated liquid nitrogen in your lab it is possible to connect an additional tube at the outlet of your cooling option...
- Page 7 How To Low temperature measurements 4. Calibration hints Calibrate the device starting from room temperature HowTo calibrate Chip-DSC Please follow the instructions of You can also combine different calibration measurements as described in the previously mentioned instructions For liquid calibration samples make sure they don’t evaporate when you put them from balance to the precooled measurement cell e.g.
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