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Summary of Contents for Rigaku XtaLAB mini
- Page 1 Cat. No. 2366A201 XtaLAB mini Cryogenic gas suction attachment Instruction manual Manual No. ME12973A02...
- Page 2 This manual described in it may not be disclosed to a third party or copied, in whole or in part, without the written consent of Rigaku Corporation. In no event will Rigaku Corporation be responsible for the results of the use of this manual. As a rule, one set of the instruction manual has to be purchased for each product.
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Page 3: Table Of Contents
ME12973A－i Table of Contents 1. Overview ..............................1 2. Cryogenic gas suction attachment - installation and adjustment............2 2.1 Wiring the electric power supply cable ..................... 2 2.2 Fine alignment of the cryogenic gas suction pipe ................5 2.3 Evaluate operation and performance ....................6 2012. -
Page 5: Overview
ME12973A 1. Overview The cryogenic gas suction unit has been developed as an attachment for the XtaLAB mini. The unit aims at reducing the ice buildup on the sample while at cryogenic temperatures. The role of the unit is to redirect the cold gas, flow and reduce the amount of ice accumulation. -
Page 6: Cryogenic Gas Suction Attachment - Installation And Adjustment
(5) Move the Omega axis to 90 degrees. (6) Close the CrystalClear software and turn off power to the XtaLAB mini and the water chiller systems. (7) Remove the collimator and beam stop from the XtaLAB mini and mount the protective cover on to the face of the detector (Fig.2). - Page 7 － 3 － ME12973A (11) Locate the cable from the gonio cover for cryogenic gas suction unit. Pass the cable through the hole at the center of the Omega axis to reach the back side of the goniometer (Fig.4). Next attach the gonio cover for cryogenic gas suction and the cryogenic gas suction tube.
- Page 8 － 4 － ME12973A (14)Connect the adapter cable to the power outlet. (15)Mount the suction pipe into the cryogenic gas suction. Refer to the Fig.7, the cooling gas alignment guide must be positioned at the bottom of the suction pipe when switching on the cryogenic gas suction at the left.
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Page 9: Fine Alignment Of The Cryogenic Gas Suction Pipe
(18)Mount the X-ray enclosure of the XtaLAB mini. (19)Mount the nozzle of Low-Temperature Gas Cooler to the XtaLAB mini main body. (20)Remove the protective cover on the detector. Mount the collimator and beam stop. -
Page 10: Evaluate Operation And Performance
－ 6 － ME12973A (10) Adjust the position of cryogenic gas suction tube to direct the flow toward the sample center, as illustrated in Fig.11. From the view point at the front of the equipment, adjust the center of the cryogenic gas suction pipe to be aligned with the sample. Sample pin Sample center Cooling gas... - Page 11 Differential Scanning Calorimeters Specifications Subject to Change without Notice Rigaku Corporation Tokyo Branch 4-14-4, Sendagaya, Shibuya-ku, Tokyo 151-0051, Japan www.rigaku.com Phone: +81-3-3479-0618 Fax: +81-3-3479-6112 e-mail: rinttyo@rigaku.co.jp Rigaku Corporation Rigaku Americas Corporation Rigaku Europe SE Head Office 9009 New Trails Drive,...
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