Buchi NIR-Online X-One Operation Manual

Buchi NIR-Online X-One Operation Manual

Process analyser

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Process Analyser X-One
Operation Manual
NIR-Online
®

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Summary of Contents for Buchi NIR-Online X-One

  • Page 1 Process Analyser X-One Operation Manual NIR-Online ®...
  • Page 2 NIR-Online GmbH Altrottstrasse 31 D-69190 Walldorf E-mail: info.nir-online@buchi.com NIR-Online reserves the right to make changes to this manual as required on the basis of future insights, especially with respect to layout, illustrations and technical detail. This manual is copyright. Information from it may not be reproduced, distributed, or used for competi- tive purposes, nor made available to third parties.
  • Page 3: Table Of Contents

    NIR-Online GmbH Table of contents Contents About this document...................... 5 Warning notices in this document.................. 5 Symbols.......................... 5 1.2.1 Warning symbols ...................... 5 1.2.2 Mandatory directive symbols .................. 5 Mark-ups and symbols ...................... 6 Safety............................ 7 Proper use .......................... 7 Use other than that intended .................... 7 Location of safety notices and warning signs on the product .......... 7 Residual risks ........................ 8 2.4.1 Risk of explosion from opening up the sensor............ 8 2.4.2 Risk of explosion from unplugging the device power plug.......... 8...
  • Page 4 Table of contents NIR-Online GmbH Operation.......................... 27 Journal button........................ 27 Entering reference data in the journal .................  27 Cleaning and servicing ..................... 28 Notes on servicing ....................... 28 Regular maintenance work.................... 28 Taking out of service and disposal..................  29 Disposal.......................... 29 Returning the instrument ..................... 29 Appendix .......................... 30 Certificates........................... 30 9.1.1 ATEX certificate ...................... 30 9.1.2 CE certificate ...................... 31...
  • Page 5: About This Document

    If you have any questions after reading this operation manual: Contact NIR-Online GmbH Customer Service. service.nir-online@buchi.com Warning notices in this document Warning notices warn you of dangers that can occur when handling the device.
  • Page 6: Mark-Ups And Symbols

    1 | About this document NIR-Online GmbH Mark-ups and symbols NOTE This symbol draws attention to useful and important information. R This character draws attention to a requirement that must be met before the in- structions below are carried out. This character indicates an instruction that must be carried out by the user.
  • Page 7: Safety

    NIR-Online GmbH Safety | 2 Safety Proper use The sensor is used to analyze substances and samples in production and in the labo- ratory. The sensor is intended exclusively for that purpose. The sensor can be used in laboratories and production facilities for the following op- erations: —...
  • Page 8: Residual Risks

    2 | Safety NIR-Online GmbH Fig. 1: Location of safety notices and warning signs on the product General warning General warning Clean Unit when dust exceeds 5 Do not separate when energized mm thickness Do not open in hazardous area. Residual risks The device has been developed and manufactured using the latest technological ad- vances.
  • Page 9: Personal Protective Equipment (Production)

    — Safety-related incidents that occur while operating the instrument are to be re- ported to the manufacturer. service.nir-online@buchi.com NIR-Online service technicians Service technicians authorized by NIR-Online have attended special training courses and are authorized by NIR-Online GmbH to carry out special servicing and repair measures.
  • Page 10: Product Description

    3 | Product description NIR-Online GmbH Product description Description of function The sensor is an optical instrument for nondestructive determination of substances and concentrations in a sample. A sample absorbs and reflects light across the entire wavelength spectrum according to its color and chemical composition. The signal reflected by the sample is recorded and analyzed by a spectrometer.
  • Page 11: Configuration

    NIR-Online GmbH Product description | 3 Configuration 3.2.1 Front view Fig. 2: Front View Measurement window Flange Heat sink 3.2.2 Rear view Fig. 3: Rear view Power and signal connector Video cable connection Journal Button Type plate Power and scanning indicator light Ground connection (Equipotential bonding) Operation Manual Process Analyser X-One...
  • Page 12: Type Plate

    3 | Product description NIR-Online GmbH Type plate The type plate identifies the instrument. The type plate is attached to the rear panel. See Chapter 3.2.2 "Rear view", page 11 NOTE Labeling Instruments without mark. Instruments without ATEX mark are not suitable for ATEX operation. See Chap- ter 3.4 "ATEX rating", page 13 Fig. 4: Type plate Company name and address...
  • Page 13: Atex Rating

    NIR-Online GmbH Product description | 3 Letter Option FEEDER/X-ROT (without ATEX certification) CAMERA Gold reflector (X-One) Silver reflector (X-Two/X-Four (diffusion lamps), X-Three) Lamp position rev. 1.3.2 Lamp position rev. 1.3.6 (X-Two/X-Four/X-View (diffusion lamps)) Camera setting flange (0 mm) Camera setting X-ROT (15 mm) Camera setting (20 mm (X-Cell+X-Cool))
  • Page 14: Scope Of Delivery

    3 | Product description NIR-Online GmbH Rating Meaning according to Directive 2014/34/EU Explosion-safe Protection class protected by enclosure [op is Da] Intrinsically safe optical radiation approved for dust zone 20 IIIC Dust group conductive dusts T80 °C Temperature classification max. surface temperature = 80° C Device safety level zone 21, adequate safety in event of fore- seeable faults Scope of delivery...
  • Page 15: Installation Box

    NIR-Online GmbH Product description | 3 Specifications X-One Power consumption 30 W Temperature stabiliza- ASDC (Advanced Spectral Drift Control): active tempera- tion ture control to ±1°C from set system operating tempera- ture. Deviations will lead to automatic white reference measurement to account for spectral drifts. ATEX Dust: II 2 D Ex tb [op is Da] IIIC T80°C Db Gas: II 2 G Ex pxb [op ist Ga] IIC T4 Gb...
  • Page 16: Software

    3 | Product description NIR-Online GmbH Screen resolution At least 1280x1024 At least 1 x 100 Mbit/s LAN USB 2.0/3.0 At least 1 USB connection per sensor and 1x USB per Data- Lab I/O box PCI/PCIe 1 slot for Profibus card (for Profibus connection) Software Word and Microsoft Excel 2003 or later...
  • Page 17 NIR-Online GmbH Product description | 3 Name Description Typical usage User Occurence SX-Backup Data backup Automated NIR admin During installa- scheduler backup of mea- tion surement data, results and cali- brations Operation Manual Process Analyser X-One 17/36...
  • Page 18: Transport And Storage

    4 | Transport and storage NIR-Online GmbH Transport and storage Transport NOTICE Risk of breakage due to incorrect transportation Make sure that all parts of the device are safely packed in such a way as to pre- vent breakage, ideally in the original box. Avoid sharp movements during transit.
  • Page 19: Installation

    NIR-Online GmbH Installation | 5 Installation Installation site (production) Make sure that the installation site meets the following requirements: — Minimum space requirements: 230 mm x 280 mm x 140 mm (W x D x H). — At least 100 mm clearance on all sides. The clearance ensures air circulation and prevents the instrument from overheating.
  • Page 20: Establishing Installation Point

    5 | Installation NIR-Online GmbH Establishing installation point The fixing points or bolts conform to M6 A2-70/7.3 Nm. Establish the installation point according to the specified data of the flange. Fig. 5: Dimensions of flange 20/36 Operation Manual Process Analyser X-One...
  • Page 21: Installation Point In Piping System (Example)

    NIR-Online GmbH Installation | 5 Installation point in piping system (example) < 1 m Fig. 6: Configuration Flow restrictor Bypass Analyser Sample removal point Flow restrictor Operation Manual Process Analyser X-One 21/36...
  • Page 22: Installation (Example)

    5 | Installation NIR-Online GmbH Installation (example) Production Server/Control room Control center Zone 21 Product flow Process control system Zone 20 Video/Frame grabber card Optional Video interfaces: filter -Profibus -4-20 mA Sensor cables USB converter -TCP/IP (power supply, -OPC Video cable RS 422) -Modbus Remote access via Ethernet...
  • Page 23: Sensor Installation

    NIR-Online GmbH Installation | 5 Sensor installation DANGER Use of an unsuitable flange in potentially explosive atmospheres. The use of an unsuitable flange may cause an explosion. In potentially explosive atmospheres use a double flange. The following installation positions are possible: Fig. 7: Fixing sensor with screws Tools required: —...
  • Page 24: Connecting The Sensor

    5 | Installation NIR-Online GmbH Connecting the sensor Tools required: — Torque wrench, size 7 mm AF — Torque wrench, size Torx T20 NOTE Make sure that the power is not switched on when connecting the sensor. NOTE Loss of performance due to use of unsuitable device cables Max.
  • Page 25: Connecting The Video Cable (Optional Accessory)

    NIR-Online GmbH Installation | 5 Tightening torque: 2 Nm ± 0.5 Fix the ground cable to the sensor. Connecting the video cable (optional accessory) Tools required — Torque wrench, size 7 mm AF Slide the cable guard over the video ca- ble connector.
  • Page 26: Establishing The Electrical Connection To The Installation Box

    5 | Installation NIR-Online GmbH Establishing the electrical connection to the installation box WARNING Death or serious burns by electric current. Have the installation carried out by an electrician or a person with similar expert knowledge. After installation, check electrical safety. NOTE Observe the legal requirements when connecting the instrument to the power sup- ply.
  • Page 27: Operation

    NIR-Online GmbH Operation | 6 Operation The instrument is operated via the SX-Suite software on a computer. See "SX-Suite User Manual " and "SX-Plus User Manual ". Journal button Pressing the button generates a journal entry. Entering reference data in the journal To perform a calibration and continuously check the calibration, reference data is re- quired.
  • Page 28: Cleaning And Servicing

    7 | Cleaning and servicing NIR-Online GmbH Cleaning and servicing NOTE Users may only carry out the servicing and cleaning operations described in this sec- tion. Any servicing and repair work which involves opening up the casing may only be carried out by NIR-Online service technicians.
  • Page 29: Taking Out Of Service And Disposal

    When disposing, observe the disposal regulations of the materials used. Materials used see Chapter 3.6 "Technical data", page 14 Returning the instrument Before returning the instrument, contact the NIR-Online GmbH Service Department. service.nir-online@buchi.com and ask for an RMA number. Operation Manual Process Analyser X-One 29/36...
  • Page 30: Appendix

    9 | Appendix NIR-Online GmbH Appendix Certificates 9.1.1 ATEX certificate NOTE Labeling Instruments without mark. Instruments without ATEX mark are not suitable for ATEX operation. See Chap- ter 3.4 "ATEX rating", page 13 30/36 Operation Manual Process Analyser X-One...
  • Page 31: Ce Certificate

    NIR-Online GmbH Appendix | 9 9.1.2 CE certificate Declaration of conformity Konformitätserklärung Déclaration de conformité Dichiarazione di conformita Declaración de conformidad Büchi NIR-Online GmbH Altrottstr. 31 69190 Walldorf Germany Declares, that the products / Erklärt, dass die Produkte / Déclare par la présente que les produits / Dichiara che i prodotti / Declara que los productos: Process Analyzer X-One comply with the requirements of the European Directives / den Anforderungen der Europäischen...
  • Page 32: Spare Parts And Accessories

    9 | Appendix NIR-Online GmbH Spare parts and accessories NOTE Any modifications of spare parts or assemblies are only allowed with the prior writ- ten permission of NIR-Online GmbH. 9.2.1 Accessories Order no. USB-RS422 interface 11060741 Analog interface (DataLabIO) 11060742 PC video card ( Frame-grabber) 11060746 PCI express, High Profile...
  • Page 33 NIR-Online GmbH Appendix | 9 Specification Max. peak-to-peak residual ripple: 200 mV Device cables NOTE Loss of performance due to use of unsuitable device cables Max. cable length between installation box and sensor 10 m. Sensor Cable Pin assignment on device connector viewed from rear of instrument: Fig. 8: Pin assignment PIN 1- blue, ground PIN 2- red, 12.7 VDC...
  • Page 34 9 | Appendix NIR-Online GmbH When using the supplied Moxa D-Sub 9-pole connector, swap the cables on pin 1 and 2. 34/36 Operation Manual Process Analyser X-One...
  • Page 36 T +971 4 313 2860 T +52 55 9001 5386 F +66 2 862 08 54 F +971 4 313 2861 latinoamerica@buchi.com bacc@buchi.com middleeast@buchi.com www.buchi.com/es-es www.buchi.com/th-th www.buchi.com We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com...

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