PRONOVA FOS/TAC 2000 User Manual

PRONOVA FOS/TAC 2000 User Manual

Automatic titration of total anorganic carbon (tac) and volatile organic acids (fos)

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User Manual
FOS/TAC 2000
Automatic titration of total anorganic carbon (TAC) and volatile
organic acids (FOS)
Version: 812-04.2015-EN
Date revised last: April 2015

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Summary of Contents for PRONOVA FOS/TAC 2000

  • Page 1 User Manual FOS/TAC 2000 Automatic titration of total anorganic carbon (TAC) and volatile organic acids (FOS) Version: 812-04.2015-EN Date revised last: April 2015...
  • Page 3 All brands and their respective owners referred to in this manual are recognized and accepted. The manufacturer does not claim any rights with regard to such brands. Should you have any questions concerning the use or maintenance of the device, please contact the manufacturer or distributor: Pronova Analysentechnik GmbH & Co. KG Groninger Straße 25 13347 Berlin, Germany...
  • Page 5: Table Of Contents

    Start measurement CALIBRATING THE PH ELECTRODE General information Calibration procedure Calibrating the peristaltic pump MANUAL STIRRING MODE MAINTENANCE, REPAIR, CUSTOMER SERVICE Maintenance of the pH electrode Changing the hose of the peristaltic pump 10 WARRANTY CONDITIONS 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 6 FOS/TAC 2000 CONTENTS 11 APPENDIX 11.1 Technical specifications 11.2 Parts subject to wear and tear 11.3 Spare parts 11.4 Declarations of conformity & Certificate 11.5 Safety Data Sheet H 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 7: General Safety Information

    In the event that work must be performed on the live, opened device, this may only be carried out by an informed skilled technician who must be familiar with the related risks and hazards! 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 8: Introduction

    Illustration: FOS/TAC analysis diagram FOS/TAC 2000 enables plant operators to perform FOS/TAC analyses without further external assistance. The fully automated system reduces operator errors to a minimum and enables a high repeatability rate. This is important because the most recent result must always be evaluated in light of the previous results.
  • Page 9: Elements Of The Analyzer

    View of the FOS/TAC controller LC display / measured-value display Function keys The function keys of the controller are used to open the different user menus, for example, to start a measuring or cycle or a calibration process. 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 10: Scope Of Delivery, Installation And Setting Into Operation

    Scope of delivery, rating plate and test certificates Quantity Description Scope of delivery FOS/TAC 2000 analyzer with 1000-ml titration solution bottle Buffer solution pH 4, 100-ml bottle Buffer solution pH 7, 100-ml bottle Refill solution pH electrode 3 mol/l KCl, 100-ml bottle...
  • Page 11: Requirements For The Place Of Installation

    The power supply unit has a EURO plug and is designed for an input voltage range of 100-240VAC / 47-63 Hz (1A @230V). In order to set the FOS/TAC 2000 into operation, proceed as follows: Connect the plug-in power supply unit to the power supply.
  • Page 12: Menu And Function Overview

    In this menu section, the analogue inputs are shown on the display of the A/D Values controller for setting into operation and service purposes. Display of the digitised sensor signal and of the calculated pH. 5,08 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 13: Performing A Fos/Tac Measurement

    FOS and TAC values by the device! Resetting the scales Filling in the sample Weighing in 5.0g of the Topping up with distilled water Finished final sample sample 20.0g 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 14: Preparing The Device

    During transport or storage, KCl solution can leak from the protective cap and produce crystalline, white potassium chloride. This salt layer has no influence on measuring capability and can be easily rinsed off with water. 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 15: Start Measurement

    Whenever changing to the next buffer solution, always rinse the electrode with distilled water. Please note that the temperature must be the same for the two calibration fluids for pH4 and pH7. Dispose of buffer solutions after use! 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 16: Calibration Procedure

    Dispose of buffer solutions after use! Following this, rinse the electrode once again with distilled water and dry. In order to protect the membrane from drying out, we recommend always attaching the protective cap with KCl solution during measuring intervals. 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 17 Click <OK> to confirm calibration and accept the new calibration data. If the calibration process is aborted by clicking <ESC>, the old calibration data is maintained. Calibration finished pH: 7.000 T: 23.17 `C Calibration canceled Calibration completed - automatic return to main menu 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 18: Calibrating The Peristaltic Pump

    The analyzer should be checked and calibrated by the manufacturer or qualified technical personnel every two years. Defective devices must be taken out of operation and returned to the manufacturer. Pronova Analysentechnik GmbH & Co. KG Groninger Straße 25 13347 Berlin, Germany Telephone +49 (0)30 / 455 085 –0...
  • Page 19: Maintenance Of The Ph Electrode

    The process ends automatically after two minutes or it can be stopped earlier by pressing <ESC>. Measuring Calibration Calibration Calibration Calibration Peristaltic active Stirrer pH Electrode Pump with A/D Values Perist. Pump < OK > __________ 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 20: Warranty Conditions

     The device must have been operated within the specified temperature range. The warranty does not cover parts subject to wear and tear, such as various solutions, the pH electrode or the hose of the peristaltic pump. 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 21: Appendix

    FOS/TAC 2000 APPENDIX 11 Appendix Appendix 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 23: Technical Specifications

    100-240VAC / 47-63 Hz / 1A @230V / Euro plug / (included in the scope of delivery) Voltage output 24 VDC / 1 A / 24 W Connector Hollow connector 5.5x2.1x11 mm / centre positive 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 24: Parts Subject To Wear And Tear

    Replacement battery for digital sample scales 812 – 1968 Plug-in power supply unit (Euro) 24VDC/1A 812 – 1930 User manual – German 812 – 1931 User manual – English Other spare parts are available on request. 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 25: Declarations Of Conformity & Certificate

    FOS/TAC 2000 DECLARATIONS OF CONFORMITY & CERTIFICATE 11.4 Declarations of conformity & Certificate EG-Konformitätserklärung Declaration of conformity Manufacturer Pronova Analysentechnik GmbH & Co. KG Groninger Straße 25 13347 Berlin Germany Product description FOS/TAC 2000 Automatische Bestimmung des FOS/TAC-Wertes von Fermenterproben durch Titration Manufacturer No.:...
  • Page 26 FOS/TAC 2000 DECLARATIONS OF CONFORMITY & CERTIFICATE 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 27: Safety Data Sheet Hso

    Article 2 REACH Regulation (EC) No 1907/2006, the annual tonnage does not require a registration or the registration is envisaged for a later registration deadline. · Application of the substance: Laboratory chemical · Manufacteur / Supplier: Pronova Analysentechnik GmbH & Co. KG Groninger Str. 25 13347 Berlin Telefon: +49/(0)30 455085-0 Telefax: +49/(0)30 455085-90 Email: info@pronova.de ·...
  • Page 28 · Conditions for safe storage: Requirements to be met by storerooms and receptacles: Provide acid-resistant floor. Do not store in corrodible metal. Information about storage in one common storage facility: Store away from foodstuffs. Recommended storage temperature: 15-25 °C 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 29 9 Physical and chemical properties · General Information: Form: Fluid Colour: Colourless Odour: Odourless · Change in condition: Melting point/Melting range: ~0°C Boiling point/Boiling range: ~100°C · Vapour pressure at 20°C: 23 hPa · Density at 20°C: 1.002 g/cm³ 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 30 The disposal is regionally differently regulated, therefore the kind of disposal is to be inquired at the responsible authorities. · Uncleaned packaging: Recommendation: Disposal according to official regulations. Recommended cleansing agents: Water, if necessary together with cleansing agents. 812-04.2015-EN FOS/TAC 2000 User Manual...
  • Page 31 International Carriage of Dangerous Goods by Road) IMDG: International Maritime Code for Dangerous Goods IATA: International Air Transport Association GHS: Globally Harmonized System of Classification and Labelling of Chemicals LC50: Letale Konzentration, 50 Prozent LD50: Letale Dosis, 50 Prozent 812-04.2015-EN FOS/TAC 2000 User Manual...

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